CN104860645B - A kind of glazed tiles utilizing loess to prepare - Google Patents

A kind of glazed tiles utilizing loess to prepare Download PDF

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Publication number
CN104860645B
CN104860645B CN201510289561.2A CN201510289561A CN104860645B CN 104860645 B CN104860645 B CN 104860645B CN 201510289561 A CN201510289561 A CN 201510289561A CN 104860645 B CN104860645 B CN 104860645B
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parts
glazed tiles
loess
glaze
carbon fiber
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CN104860645A (en
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张国阳
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SINO RISING-SUN CONSTRUCTION GROUP Co Ltd
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Abstract

The present invention relates to a kind of glazed tiles utilizing loess to prepare, this glazed tiles base substrate is made up of loess, alumine, albite, quartz, fused magnesite, carbon fiber, phenolic resin, starch and rice husk;This glazed tiles glaze is made up of iron oxide yellow, titanium dioxide, feldspar powder, nano zine oxide, carborundum, carbon fiber, tin ash, TEOS, politef, this glazed tiles smooth surface is clean and tidy, bright in colour beautiful, there is excellent resistance to compression, the fire-resistant and performance of acid and alkali-resistance, and light weight, water absorption rate is low, good permeability, low cost.

Description

A kind of glazed tiles utilizing loess to prepare
Technical field
The invention belongs to glazed tiles field, particularly to a kind of glazed tiles utilizing loess to prepare.
Background technology
Glazed tiles are one ancient, traditional ceramic materials of China.Along with the development of tourist industry, people are for the demand of glazed tiles Also it is more and more, is also more and more higher to its requirement.
Glazed tiles, material is firm, bright in luster, glaze colours is smooth, and always as the building object of Chinese tradition, it is through the successive dynasties Development, the improvement of quality, owing to having multiple excellent function, and it is widely used in modern architecture.
Existing glazed tiles are the most all to use multiple pug mixed sintering to form, and its glaze layer is the thickest and produces stress, quality Weight, is easily caused product glaze and be full of cracks occurs, collapse the defect of stripping.The most smooth, and pug is easily generated dirt in process of production Dye, cost and energy consumption are high, and the quality of product is not sufficiently stable, and its glaze glossiness is inadequate, and colour generation is abundant not, stable, at gas Wait and easily fade under changeable area or long sunlight irradiation.
Present invention mainly solves technical problem is that: for the deficiencies in the prior art, it is provided that a kind of glazed tiles utilizing loess to prepare, This glazed tiles smooth surface is clean and tidy, bright in colour beautiful, has excellent resistance to compression, the fire-resistant and performance of acid and alkali-resistance, and light weight, Water absorption rate is low, good permeability, low cost.
Summary of the invention
It is an object of the invention to, for the problems referred to above, develop a kind of glazed tiles utilizing loess to prepare, by optimizing coloured glaze unbaked tile Body and the composition of glaze, improve the colouring effect of glazed tiles, resistance to compression, the fire-resistant and performance of acid and alkali-resistance and water absorption rate and breathe freely The physical and chemical performances such as property.
A kind of glazed tiles utilizing loess to prepare, this glazed tiles base substrate weight portion composition is as follows:
Loess 100-120 part;Alumine 20-30 part;Albite 8-10 part;Quartz 2-6 part;Fused magnesite 2-6 part; Carbon fiber 2-6 part;Phenolic resin 2-6 part;Starch 2-6 part;Rice husk 2-6 part;
This glazed tiles glaze weight portion composition is as follows:
Iron oxide yellow 40-50 part;Titanium dioxide 1-5 part;Feldspar powder 1-5 part;Nano zine oxide 1-5 part;Carborundum 1-5 part; Carbon fiber 1-5 part;Tin ash 1-5 part;TEOS 1-5 part;Politef 1-5 part;
Its preparation method is as follows:
(1) batch mixing: glazed tiles blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 3 days;
(2) pressed compact molding, compressing under 55Mpa pressure, it is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, and during kiln discharge, base substrate water content is less than 1.2wt%;
(4) glazing: added water by glaze raw material and prepare glaze, and glazing, glaze thickness is 0.2mm;After glazing and 150 Dry 24 hours at DEG C;
(5) burn till: in calcining kiln, heating rate 80 DEG C/h, after being warming up to 1500 DEG C, be incubated 2 hours, Utilize glazed tiles prepared by loess.
As preferably, the chemical composition of loess is: SiO2 55wt%, Al2O3 25wt%, Fe2O3 8%, CaO 7wt%, Other compositions 5wt%.
As preferably, the particle diameter of alumine is less than 1 μm.
As preferably, this glazed tiles base substrate weight portion composition is as follows:
Loess 110 parts;Alumine 25 parts;Albite 9 parts;2 parts of quartz;Fused magnesite 2 parts;2 parts of carbon fiber; 2 parts of phenolic resin;Starch 2 parts;2 parts of rice husk.
As preferably, this glazed tiles glaze weight portion composition is as follows:
Iron oxide yellow 45 parts;Titanium dioxide 2 parts;Feldspar powder 2 parts;Nano zine oxide 2 parts;Carborundum 2 parts;Carbon fiber 2 Part;Tin ash 2 parts;TEOS 2 parts;Politef 2 parts.
Beneficial effects of the present invention:
(1) generally speaking, by optimizing glazed tiles base substrate and the composition of glaze, improve the colouring effect of glazed tiles, resistance to compression, The performance of fire-resistant and acid and alkali-resistance and the physical and chemical performance such as water absorption rate and breathability;This glazed tiles smooth surface is clean and tidy, bright in colour bright Beautiful, there is excellent resistance to compression, the fire-resistant and performance of acid and alkali-resistance, and light weight, water absorption rate is low, good permeability, low cost.Should The water absorption rate of glazed tiles is less than 5.5%, and comprcssive strength is more than 56Mpa.
(2) in base substrate dispensing, being the first primary raw material with loess, alumine is the second primary raw material, and assists sodium long Stone, quartz, fused magnesite, carbon fiber, phenolic resin, starch and rice husk, and form by optimizing the weight portion of each component, The resistance to compression of customer service loess is strong, the imperfect deficiency of stability, and optimizes water suction and the permeability of base substrate.And due to Huang Soil has preferable viscosity, and preferable with the combination of glaze layer, therefore, glaze layer can be the thinnest, such that it is able to prevent glaze from going out Now chap, collapse the defect of stripping.Meanwhile, loess carries color, also the colour brightness that glazed tiles are overall can be produced material impact.
(3) by with the addition of titanium dioxide and carborundum in glaze, the toughness of surface layer can be improved, and nano zine oxide, The automatically cleaning effect of glazed tiles can be played;And feldspar powder can play the effect of sintering aid;And TEOS and politef Interpolation, effective surface protection can be carried out for glazed tiles, improve the smooth degree on surface.Prepared by the application out Glazed tiles smooth surface is clean and tidy, bright in colour beautiful, and has preferable stability.
Detailed description of the invention
Below in conjunction with specific embodiment, and with reference to data, the present invention is described in further detail.Should be understood that these The embodiment present invention solely for the purpose of illustration, rather than limit the scope of the present invention by any way.
Embodiment 1:
A kind of glazed tiles utilizing loess to prepare,
This glazed tiles base substrate weight portion composition is as follows:
Loess 110 parts;Alumine 25 parts;Albite 9 parts;2 parts of quartz;Fused magnesite 2 parts; 2 parts of carbon fiber;2 parts of phenolic resin;Starch 2 parts;2 parts of rice husk;
This glazed tiles glaze weight portion composition is as follows,
Iron oxide yellow 45 parts;Titanium dioxide 2 parts;Feldspar powder 2 parts;Nano zine oxide 2 parts;Carborundum 2 Part;2 parts of carbon fiber;Tin ash 2 parts;TEOS 2 parts;Politef 2 parts;
The chemical composition of loess is: SiO2 55wt%, Al2O3 25wt%, Fe2O3 8%, CaO 7wt%, Other compositions 5wt%.
The particle diameter of alumine is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: glazed tiles blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 3 days;
(2) pressed compact molding, compressing under 55Mpa pressure, it is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, and during kiln discharge, base substrate water content is less than 1.2wt %;
(4) glazing: added water by glaze raw material and prepare glaze, and glazing, glaze thickness is 0.2mm;Glazing Afterwards and dry 24 hours at 150 DEG C;
(5) burn till: in calcining kiln, heating rate 80 DEG C/h, after being warming up to 1500 DEG C, be incubated 2 Hour, utilize glazed tiles prepared by loess.
Embodiment 2:
A kind of glazed tiles utilizing loess to prepare,
This glazed tiles base substrate weight portion composition is as follows:
Loess 112 parts;Alumine 26 parts;Albite 8 parts;2 parts of quartz;Fused magnesite 4 parts; 2 parts of carbon fiber;4 parts of phenolic resin;Starch 2 parts;2 parts of rice husk;
This glazed tiles glaze weight portion composition is as follows,
Iron oxide yellow 46 parts;Titanium dioxide 2 parts;Feldspar powder 2 parts;Nano zine oxide 2 parts;Carborundum 2 Part;2 parts of carbon fiber;Tin ash 2 parts;TEOS 2 parts;Politef 2 parts;
The chemical composition of loess is: SiO2 55wt%, Al2O3 25wt%, Fe2O3 8%, CaO 7wt%, Other compositions 5wt%.
The particle diameter of alumine is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: glazed tiles blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 3 days;
(2) pressed compact molding, compressing under 55Mpa pressure, it is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, and during kiln discharge, base substrate water content is less than 1.2wt %;
(4) glazing: added water by glaze raw material and prepare glaze, and glazing, glaze thickness is 0.2mm;Glazing Afterwards and dry 24 hours at 150 DEG C;
(5) burn till: in calcining kiln, heating rate 80 DEG C/h, after being warming up to 1500 DEG C, be incubated 2 Hour, utilize glazed tiles prepared by loess.
Embodiment 3:
A kind of glazed tiles utilizing loess to prepare,
This glazed tiles base substrate weight portion composition is as follows:
Loess 109 parts;Alumine 22 parts;Albite 9 parts;5 parts of quartz;Fused magnesite 5 parts; 5 parts of carbon fiber;5 parts of phenolic resin;Starch 5 parts;5 parts of rice husk;
This glazed tiles glaze weight portion composition is as follows,
Iron oxide yellow 42 parts;Titanium dioxide 2 parts;Feldspar powder 2 parts;Nano zine oxide 2 parts;Carborundum 2 Part;2 parts of carbon fiber;Tin ash 2 parts;TEOS 2 parts;Politef 2 parts;
The chemical composition of loess is: SiO2 55wt%, Al2O3 25wt%, Fe2O3 8%, CaO 7wt%, Other compositions 5wt%.
The particle diameter of alumine is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: glazed tiles blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 3 days;
(2) pressed compact molding, compressing under 55Mpa pressure, it is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, and during kiln discharge, base substrate water content is less than 1.2wt %;
(4) glazing: added water by glaze raw material and prepare glaze, and glazing, glaze thickness is 0.2mm;Glazing Afterwards and dry 24 hours at 150 DEG C;
(5) burn till: in calcining kiln, heating rate 80 DEG C/h, after being warming up to 1500 DEG C, be incubated 2 Hour, utilize glazed tiles prepared by loess.
Embodiment 4:
A kind of glazed tiles utilizing loess to prepare,
This glazed tiles base substrate weight portion composition is as follows:
Loess 119 parts;Alumine 27 parts;Albite 9 parts;2 parts of quartz;Fused magnesite 5 parts; 2 parts of carbon fiber;2 parts of phenolic resin;Starch 2 parts;5 parts of rice husk;
This glazed tiles glaze weight portion composition is as follows,
Iron oxide yellow 47 parts;Titanium dioxide 2 parts;Feldspar powder 2 parts;Nano zine oxide 2 parts;Carborundum 2 Part;2 parts of carbon fiber;Tin ash 2 parts;TEOS 2 parts;Politef 2 parts;
The chemical composition of loess is: SiO2 55wt%, Al2O3 25wt%, Fe2O3 8%, CaO 7wt%, Other compositions 5wt%.
The particle diameter of alumine is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: glazed tiles blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 3 days;
(2) pressed compact molding, compressing under 55Mpa pressure, it is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, and during kiln discharge, base substrate water content is less than 1.2wt %;
(4) glazing: added water by glaze raw material and prepare glaze, and glazing, glaze thickness is 0.2mm;Glazing Afterwards and dry 24 hours at 150 DEG C;
(5) burn till: in calcining kiln, heating rate 80 DEG C/h, after being warming up to 1500 DEG C, be incubated 2 Hour, utilize glazed tiles prepared by loess.
Embodiment 5:
A kind of glazed tiles utilizing loess to prepare,
This glazed tiles base substrate weight portion composition is as follows:
Loess 100 parts;Alumine 20 parts;Albite 9 parts;4 parts of quartz;Fused magnesite 5 parts; 4 parts of carbon fiber;5 parts of phenolic resin;Starch 4 parts;5 parts of rice husk;
This glazed tiles glaze weight portion composition is as follows,
Iron oxide yellow 50 parts;Titanium dioxide 2 parts;Feldspar powder 2 parts;Nano zine oxide 2 parts;Carborundum 2 Part;2 parts of carbon fiber;Tin ash 2 parts;TEOS 2 parts;Politef 2 parts;
The chemical composition of loess is: SiO2 55wt%, Al2O3 25wt%, Fe2O3 8%, CaO 7wt%, Other compositions 5wt%.
The particle diameter of alumine is less than 1 μm.
Its preparation method is as follows:
(1) batch mixing: glazed tiles blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 3 days;
(2) pressed compact molding, compressing under 55Mpa pressure, it is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, and during kiln discharge, base substrate water content is less than 1.2wt %;
(4) glazing: added water by glaze raw material and prepare glaze, and glazing, glaze thickness is 0.2mm;Glazing Afterwards and dry 24 hours at 150 DEG C;
(5) burn till: in calcining kiln, heating rate 80 DEG C/h, after being warming up to 1500 DEG C, be incubated 2 Hour, utilize glazed tiles prepared by loess.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and And without departing from the spirit or essential characteristics of the present invention, it is possible to realize this in other specific forms Bright.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and be non-limiting , the scope of the present invention is limited by claims rather than described above, wants it is intended that will fall in right All changes in the implication of the equivalency asked and scope are included in the present invention.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, but the most each embodiment party Formula only comprises an independent technical scheme, and this narrating mode of description is only for clarity sake, ability Field technique personnel should be using description as an entirety, and the technical scheme in each embodiment can also be through suitable group Close, form other embodiments that it will be appreciated by those skilled in the art that.

Claims (5)

1. the glazed tiles utilizing loess to prepare, it is characterised in that:
This glazed tiles base substrate weight portion composition is as follows:
Loess 100-120 part;Alumine 20-30 part;Albite 8-10 part;Quartz 2-6 part;Fused magnesite 2-6 part;Carbon fiber 2-6 part;Phenolic resin 2-6 part;Starch 2-6 part;Rice husk 2-6 part;
This glazed tiles glaze weight portion composition is as follows:
Iron oxide yellow 40-50 part;Titanium dioxide 1-5 part;Feldspar powder 1-5 part;Nano zine oxide 1-5 part;Carborundum 1-5 part;Carbon fiber 1-5 part;Tin ash 1-5 part;TEOS 1-5 part;Politef 1-5 part;Its preparation method is as follows:
(1) batch mixing: glazed tiles blank raw material is weighed, pulverizes, sieved, add water batch mixing, and old mud 3 days;
(2) pressed compact molding, compressing under 55Mpa pressure, it is incubated 2 hours, the demoulding;
(3) base substrate is dried: dry 1 hour at 150 DEG C in drying kiln, and during kiln discharge, base substrate water content is less than 1.2wt%;
(4) glazing: added water by glaze raw material and prepare glaze, and glazing, glaze thickness is 0.2mm;Dry 24 hours after glazing and at 150 DEG C;
(5) burn till: in calcining kiln, heating rate 80 DEG C/h, after being warming up to 1500 DEG C, be incubated 2 hours, utilize glazed tiles prepared by loess.
2. one kind utilizes glazed tiles prepared by loess as claimed in claim 1, it is characterised in that the chemical composition of loess is: SiO255wt%, Al2O325wt%, Fe2O38%, CaO 7wt%, other compositions 5wt%.
3. one kind utilizes glazed tiles prepared by loess as claimed in claim 1 or 2, it is characterised in that the particle diameter of alumine is less than 1 μm.
4. one kind utilizes glazed tiles prepared by loess as claimed in claim 1, it is characterised in that this glazed tiles base substrate weight portion composition is as follows:
Loess 110 parts;Alumine 25 parts;Albite 9 parts;2 parts of quartz;Fused magnesite 2 parts;2 parts of carbon fiber;2 parts of phenolic resin;Starch 2 parts;2 parts of rice husk.
5. one kind utilizes glazed tiles prepared by loess as claimed in claim 1, it is characterised in that this glazed tiles glaze weight portion composition is as follows:
Iron oxide yellow 45 parts;Titanium dioxide 2 parts;Feldspar powder 2 parts;Nano zine oxide 2 parts;Carborundum 2 parts;2 parts of carbon fiber;Tin ash 2 parts;TEOS 2 parts;Politef 2 parts.
CN201510289561.2A 2015-06-01 2015-06-01 A kind of glazed tiles utilizing loess to prepare Expired - Fee Related CN104860645B (en)

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Publication number Priority date Publication date Assignee Title
CN107352809A (en) * 2017-07-24 2017-11-17 太仓市科教新城琉璃艺术策划中心 A kind of coloured glaze containing loess composition
CN107365076A (en) * 2017-07-24 2017-11-21 太仓市科教新城琉璃艺术策划中心 A kind of coloured glaze containing alumine composition
CN107555926A (en) * 2017-08-18 2018-01-09 寿县维东建材商贸有限公司 A kind of azulejo watt of service life length and preparation method thereof

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CN103538141B (en) * 2013-10-15 2015-08-26 常熟大象建陶有限公司 The preparation method of colored glaze ceramic tile and the method shaped device used
CN103693993A (en) * 2013-12-23 2014-04-02 宾阳县明翔新材料科技有限公司 Ceramic tile with heat-preservation and heat-insulation functions and production method of same
CN103833325B (en) * 2014-01-04 2015-05-27 安徽省含山瓷业股份有限公司 Low-cost domestic ceramic containing laterite
CN104860644A (en) * 2015-05-29 2015-08-26 苏州拓科仪器设备有限公司 Underglaze blue and underglaze red glaze ceramic

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