CN105060843A - Preparation method of reinforced jade-based porcelain and product made of reinforced jade-based porcelain - Google Patents
Preparation method of reinforced jade-based porcelain and product made of reinforced jade-based porcelain Download PDFInfo
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Abstract
The invention relates to a preparation method of reinforced jade-based porcelain and a product made of the reinforced jade-based porcelain. The reinforced jade-based porcelain comprises a blank material and a glaze material, wherein the blank material comprises the following raw materials by weight: 10 to 15 percent of Longyan kaolinite, 8 to 15 percent of Guizhou kaolinite, 5 to 10 percent of New Zealand kaolinite, 10 to 15 percent of Xingzi feldspar, 40 to 50 percent of Xingzi quartz, 5 to 10 percent of Yifeng low-temperature porcelain stone, 3 to 5 percent of Jingdezhen glaze stone, 3 to 5 percent of Heilongjiang bentonite, and 3 to 5 percent of Yunnan porcelain clay; the glaze material comprises the following raw materials by weight: 8 to 12 percent of Longyan kaolinite, 3 to 5 percent of New Zealand kaolinite, 10 to 15 percent of Xingzi feldspar, 30 to 37 percent of Xingzi quartz, 8 to 12 percent of Yifeng low-temperature porcelain stone, 15 to 20 percent of Leping dolomite, 5 to 10 percent of Leping calcite, 8 to 10 percent of Jingdezhen glaze stone, and 5 to 10 percent of Yunnan porcelain clay. The preparation method and the product have the advantages that the production method is scientific and reasonable; the production cost is relatively low; the implementation is easy; the yield is high; the product quality is good. Therefore, the market prospect is wide.
Description
Technical field
The invention belongs to ceramic (pottery) field, be specifically related to a kind ofly strengthen the preparation method of beautiful matter porcelain and obtained product thereof.
Background technology
Jingdezhen Ceramic historical origin stream is long, be called as world culture art rarity, Jing Dezhen domestic ceramics belongs to pate dure, have compared with other porcelain kinds that product whiteness is high, porcelain is fine and smooth, glaze paint is bright smooth, never fade, resistance to rapid cool shock heating, anti abrasive feature, being the high-grade porcelain kind in domestic ceramics, is the leading of domestic high-grade porcelain consumption.But the light transmission of product is not very good compared with beautiful matter porcelain, permeability is not strong, and product hardness also also has a certain distance compared with strengthening porcelain.Therefore a kind of feature both having maintained Jing Dezhen tradition domestic ceramics of research invention, and the glossiness of product is high, light transmission good, beautiful texture is strong, the beautiful matter porcelain of the strengthening that hardness of glaze surface is large just has very large realistic meaning, really represents the characteristic of Jing Dezhen domestic ceramics " thin as a piece of paper, white as a jade, bright if mirror, sound are as single sonorous stone, firmly as steel ".
Summary of the invention
The technical problem to be solved in the present invention is to provide the preparation method of the beautiful matter porcelain of strengthening that a kind of preparation technology is simple, production cost is lower, product performance are stable and obtained product thereof.
For solving above technical problem, technical scheme of the present invention is: a kind of preparation method strengthening beautiful matter porcelain, and adopt raw mineral materials and industrial chemicals, the weight percent of its blank and glaze formula consists of:
Blank: Longyan kaolin 10 ~ 15%, Guizhou kaolin 8 ~ 15%, New Zealand's kaolin 5 ~ 10%, planetesimal feldspar 10 ~ 15%, planetesimal quartz 40 ~ 50%, Yifeng low temperature porcelain stone 5 ~ 10%, Jing Dezhen glaze fruit 3 ~ 5%, Heilungkiang wilkinite 3 ~ 5%, Yunnan china clay 3 ~ 5%;
Glaze: Longyan kaolin 8 ~ 12%, New Zealand's kaolin 3 ~ 5%, planetesimal feldspar 10 ~ 15%, planetesimal quartz 30 ~ 37%, Yifeng low temperature porcelain stone 8 ~ 12%, Leping rhombspar 15 ~ 20%, Leping calcite 5 ~ 10%, Jing Dezhen glaze fruit 8 ~ 10%, Yunnan china clay 5 ~ 10%;
Through blank and glaze preparation, shaping, dry, repaired biscuit, low temperature biscuiting, glazing, the glaze firing of high temperature reduction flame, decoration firing operation acquisition goods.
Described Slug preparing operation is by material: ball: the part by weight batching dress ball mill of water=1:1.5 ~ 1.7:1, Ball-milling Time 35 ~ 40 hours, blank ball milling fineness was 300 mesh sieves, tail over and be less than 0.1 ~ 0.3%, obtain solid particulate fineness and be less than the slurry that 6 microns reach 60 ~ 70%, described slurry after deironing is sieved, then is made powder by spray-drying tower or makes roll extrusion mud bar by press filt, pugging or make grout material by changing slurry after press filt sheet.
Described glaze preparation section is by material: ball: the part by weight batching dress ball mill of water=1:1.9 ~ 2.0:1, Ball-milling Time 40 ~ 45 hours, glaze ball milling fineness was 300 mesh sieves, tailed over and was less than 0.01 ~ 0.03%, made glaze for subsequent use after sieve after glaze slip deironing.
Described molding procedure comprises isostatic pressing, roll forming, injection forming.
In described isostatic pressing process, in spray-drying tower, the proportion of pug is 1570 ~ 1600g/l, and mobility is 50 ~ 70s/100ml, and the water ratio of obtained powder is 3 ~ 4%; In described flow forming process, pug moisture content is 22 ~ 25%; In described slip-casting shaping process, the unit weight of slip casing by pressure material is 1670 ~ 1690g/l, and changing slurry mobility is 130 ~ 160s/100ml; Manual grout material unit weight is 1620 ~ 1660g/ml, and mobility is 0.3%.
Described spray-drying tower is adding additives 0.8 ~ 1.0%, thinner≤0.5% at home and abroad, and described binding agent is modified starch, and thinner is Sodium hexametaphosphate 99.
The temperature of described drying process is 40 ~ 50 DEG C.
In described glazing operation, glaze proportion is 1.25 ~ 1.29g/ml, and glazed thickness is 0.25 ~ 0.3mm.
Described low temperature biscuiting temperature is 940 ~ 960 DEG C, the biscuiting cycle is 14 ~ 16 hours, and 880 DEG C of insulations 40 minutes, top temperature was incubated 30 minutes; High temperature reduction flame temperature of glaze firing is 1320 ~ 1340 DEG C, the glaze firing cycle is 25 ~ 27 hours, the highest temperature is incubated 60 minutes; In described decoration firing step, in-glaze decoration decoration firing temperature is 1200 ~ 1290 DEG C, and over-glaze decoration decoration firing temperature is 780 ~ 880 DEG C.
The whiteness of the beautiful matter porcelain products of the strengthening that described method obtains is 92 ~ 94, glossiness is 93 ~ 95, water-intake rate is 0.05 ~ 0.07, thermostability is that 220 ~ 20 DEG C of heat exchanges are not once split, glaze paint vickers microhardness is 8.3 ~ 8.5Gpa, and center resistance to impact shock is 2.3 ~ 2.5J/cm
2, plumbous, quantity of cadmium release is 0.
The raw material that described strengthening beautiful matter porcelain base, glaze use: the chemical weight percent composition of Guizhou kaolin, New Zealand's kaolin, Longyan kaolin, planetesimal feldspar, planetesimal quartz, Yifeng low temperature porcelain stone, Leping rhombspar, Leping calcite, Jing Dezhen glaze fruit, Heilungkiang wilkinite, Yunnan china clay is as follows:
This patent is by extensively finding novel starting material, develop a kind of novel domestic ceramics---strengthen beautiful matter porcelain, main raw material selected by this patent is high grade kaolinite, feldspar, the natural environmental-protective materials such as a large amount of crystal quality fused silica and low temperature high-quality porcelain stone, strict control blank fineness, burn till the mixed phase of middle generation vitreum and crystal, form unique whiteness, glossiness, the beautiful texture of transparence perfect adaptation, bright in making porcelain body white, have whiter, more saturating, the beautiful texture of more moistening, glittering and translucent to people's one, impression as jadeware, porcelain whiteness is high, transparency is good, glossiness is high, it is " thin as a piece of paper that product has, thoroughly as mirror, sound is as single sonorous stone, white as a jade " feature, and product hardness of glaze surface is large, thermostability is high, reach the product performance of strengthening domestic ceramics.While the tradition domestic ceramics advantage of maintenance Jing Dezhen, thoroughly solve the shortcoming that product light transmission is not strong, hardness of glaze surface is not high.And its production method is scientific and reasonable, and production cost is lower, easy to implement, and yield rate is high, good product quality, therefore there are wide market outlook.
Embodiment
embodiment 1
Strengthening beautiful matter porcelain body recipe weight percent is Longyan kaolin 11%, Guizhou kaolin 12%, New Zealand's kaolin 6%, planetesimal feldspar 12%, planetesimal quartz 40%, Yifeng low temperature porcelain stone 6%, Jing Dezhen glaze fruit 5%, Heilungkiang wilkinite 4%, Yunnan china clay 4%.
Strengthening beautiful matter glaze weight percent is Longyan kaolin 9%, New Zealand's kaolin 3%, planetesimal feldspar 11%, planetesimal quartz 30%, Yifeng low temperature porcelain stone 9%, Leping rhombspar 15%, Leping calcite 6%, Jing Dezhen glaze fruit 9%, Yunnan china clay 8%.
Mix by blank formulation requirement raw materials weighing, after fragmentation, by material: ball: the part by weight batching dress ball mill of water=1:1.5:1, Ball-milling Time 36 hours, blank ball milling fineness was 300 mesh sieves, tailed over and was less than 0.1%, obtained solid particulate fineness and was less than the slurry that 6 microns reach 62%, described slurry, after deironing is sieved, makes by press filt, pugging the pug that water ratio is 23%.
Mix by glaze formula requirement raw materials weighing, by material: ball: the part by weight batching dress ball mill of water=1:1.9:1, Ball-milling Time 42 hours, glaze ball milling fineness was 300 mesh sieves, tail over and be less than 0.01%, making proportion after glaze slip deironing after sieve is that 1.26g/ml glaze is for subsequent use.
By base substrate good for roll forming after 45 DEG C of dryings, repaired biscuit, through 15 hours, biscuiting to 940 DEG C, wherein be incubated 40 minutes at 880 DEG C, top temperature is incubated 30 minutes, naturally cools to room temperature kiln discharge, then to glazing after biscuit dedusting moisturizing, glazed thickness is 0.26mm.
The base substrate loading of kiln having executed glaze burnt till, from room temperature, through 25 hours, glaze firing to 1320 DEG C, is incubated 60 minutes, naturally cools to room temperature kiln discharge and obtains ceramic whiteware tire.
Glue in note after warm marble paper at ceramic whiteware tire outside surface, loading of kiln is burnt to 1260 DEG C, naturally cools to the beautiful matter porcelain of strengthening after room temperature kiln discharge acquisition marble paper decoration.
The whiteness of the beautiful matter porcelain products of described strengthening is 92, glossiness is 93, water-intake rate is 0.05, thermostability is that 220 ~ 20 DEG C of heat exchanges are not once split, and glaze paint vickers microhardness is 8.3Gpa, and center resistance to impact shock is 2.3J/cm
2, plumbous, quantity of cadmium release is 0.
embodiment 2
Strengthening beautiful matter porcelain body recipe weight percent is Longyan kaolin 14%, Guizhou kaolin 8%, New Zealand's kaolin 5%, planetesimal feldspar 14%, planetesimal quartz 45%, Yifeng low temperature porcelain stone 5%, Jing Dezhen glaze fruit 3%, Heilungkiang wilkinite 3%, Yunnan china clay 3%.
Strengthening beautiful matter glaze weight percent is Longyan kaolin 11%, New Zealand's kaolin 4%, planetesimal feldspar 14%, planetesimal quartz 30%, Yifeng low temperature porcelain stone 8%, Leping rhombspar 15%, Leping calcite 5%, Jing Dezhen glaze fruit 8%, Yunnan china clay 5%.
Mix by blank formulation requirement raw materials weighing, after fragmentation, by material: ball: the part by weight batching dress ball mill of water=1:1.6:1, Ball-milling Time 38 hours, blank ball milling fineness was 300 mesh sieves, tail over and be less than 0.3%, obtain solid particulate fineness and be less than the slurry that 6 microns reach 65%, described slurry is after deironing is sieved, adjustment mud balance is 1580g/l, mobility be 60s/100ml and add 0.8% modified starch and 0.3% Sodium hexametaphosphate 99 after make by spray-drying tower the powder that water ratio is 3.5%.
Mix by glaze formula requirement raw materials weighing, by material: ball: the part by weight batching dress ball mill of water=1:2.0:1, Ball-milling Time 45 hours, glaze ball milling fineness was 300 mesh sieves, tail over and be less than 0.02%, making proportion after glaze slip deironing after sieve is that 1.27g/ml glaze is for subsequent use.
By base substrate good for isostatic pressing after 50 DEG C of dryings, repaired biscuit, through 16 hours, biscuiting to 960 DEG C, wherein be incubated 40 minutes at 880 DEG C, top temperature is incubated 30 minutes, naturally cools to room temperature kiln discharge, then to glazing after biscuit dedusting moisturizing, glazed thickness is 0.25mm.
The base substrate loading of kiln having executed glaze burnt till, from room temperature, through 27 hours, glaze firing to 1340 DEG C, is incubated 60 minutes, naturally cools to room temperature kiln discharge and obtains ceramic whiteware tire.
After ceramic whiteware tire outside surface glues note low temperature marble paper, loading of kiln is burnt to 860 DEG C, naturally cools to the beautiful matter porcelain of strengthening after room temperature kiln discharge acquisition marble paper decoration.
The whiteness of the beautiful matter porcelain products of described strengthening is 94, glossiness is 95, water-intake rate is 0.07, thermostability is that 220 ~ 20 DEG C of heat exchanges are not once split, and glaze paint vickers microhardness is 8.5Gpa, and center resistance to impact shock is 2.5J/cm
2, plumbous, quantity of cadmium release is 0.
embodiment 3
Strengthening beautiful matter porcelain body recipe weight percent is Longyan kaolin 10%, Guizhou kaolin 9%, New Zealand's kaolin 9%, planetesimal feldspar 10%, planetesimal quartz 48%, Yifeng low temperature porcelain stone 5%, Jing Dezhen glaze fruit 3%, Heilungkiang wilkinite 3%, Yunnan china clay 3%.
Strengthening beautiful matter glaze weight percent is Longyan kaolin 8%, New Zealand's kaolin 3%, planetesimal feldspar 10%, planetesimal quartz 36%, Yifeng low temperature porcelain stone 8%, Leping rhombspar 19%, Leping calcite 5%, Jing Dezhen glaze fruit 8%, Yunnan china clay 8%.
Mix by blank formulation requirement raw materials weighing, after fragmentation, by material: ball: the part by weight batching dress ball mill of water=1:1.7:1, Ball-milling Time 36 hours, blank ball milling fineness was 300 mesh sieves, tailed over and was less than 0.3%, obtain solid particulate fineness and be less than the slurry that 6 microns reach 69%, described slurry is after deironing is sieved, and by changing slurry after press filt sheet, to make unit weight be 1670g/l, changes the slip casing by pressure material that slurry mobility is 140s/100ml.
Mix by glaze formula requirement raw materials weighing, by material: ball: the part by weight batching dress ball mill of water=1:2.0:1, Ball-milling Time 44 hours, glaze ball milling fineness was 300 mesh sieves, tail over and be less than 0.01%, making proportion after glaze slip deironing after sieve is that 1.28g/ml glaze is for subsequent use.
By base substrate good for pressure after 50 DEG C of dryings, repaired biscuit, through 14 hours, biscuiting to 940 DEG C, wherein be incubated 40 minutes at 880 DEG C, top temperature is incubated 30 minutes, naturally cools to room temperature kiln discharge, then to glazing after biscuit dedusting moisturizing, glazed thickness is 0.3mm.
The base substrate loading of kiln having executed glaze burnt till, from room temperature, through 27 hours, glaze firing to 1330 DEG C, is incubated 60 minutes, naturally cools to room temperature kiln discharge and obtains the beautiful matter porcelain of strengthening.
The whiteness of the beautiful matter porcelain products of described strengthening is 93, glossiness is 94, water-intake rate is 0.06, thermostability is that 220 ~ 20 DEG C of heat exchanges are not once split, and glaze paint vickers microhardness is 8.4Gpa, and center resistance to impact shock is 2.5J/cm
2, plumbous, quantity of cadmium release is 0.
embodiment 4
Strengthening beautiful matter porcelain body recipe weight percent is Longyan kaolin 10%, Guizhou kaolin 14%, New Zealand's kaolin 5%, planetesimal feldspar 10%, planetesimal quartz 40%, Yifeng low temperature porcelain stone 10%, Jing Dezhen glaze fruit 3%, Heilungkiang wilkinite 4%, Yunnan china clay 4%.
Strengthening beautiful matter glaze weight percent is Longyan kaolin 8%, New Zealand's kaolin 3%, planetesimal feldspar 10%, planetesimal quartz 32%, Yifeng low temperature porcelain stone 11%, Leping rhombspar 15%, Leping calcite 8%, Jing Dezhen glaze fruit 8%, Yunnan china clay 5%.
Mix by blank formulation requirement raw materials weighing, after fragmentation, by material: ball: the part by weight batching dress ball mill of water=1:1.5:1, Ball-milling Time 39 hours, blank ball milling fineness was 300 mesh sieves, tailed over and was less than 0.2%, obtain solid particulate fineness and be less than the slurry that 6 microns reach 63%, described slurry is after deironing is sieved, and by changing slurry after press filt sheet, to make unit weight be 1640g/ml, and mobility is the manual grout material of 0.3%.
Mix by glaze formula requirement raw materials weighing, by material: ball: the part by weight batching dress ball mill of water=1:2.0:1, Ball-milling Time 45 hours, glaze ball milling fineness was 300 mesh sieves, tail over and be less than 0.03%, making proportion after glaze slip deironing after sieve is that 1.27g/ml glaze is for subsequent use.
By base substrate good for manual injection forming after 47 DEG C of dryings, repaired biscuit, through 15 hours, biscuiting to 940 DEG C, wherein be incubated 40 minutes at 880 DEG C, top temperature is incubated 30 minutes, naturally cools to room temperature kiln discharge, then to glazing after biscuit dedusting moisturizing, glazed thickness is 0.29mm.
The base substrate loading of kiln having executed glaze burnt till, from room temperature, through 25 hours, glaze firing to 1330 DEG C, is incubated 60 minutes, naturally cools to room temperature kiln discharge and obtains the beautiful matter porcelain of strengthening.
The whiteness of the beautiful matter porcelain products of described strengthening is 92, glossiness is 93, water-intake rate is 0.05, thermostability is that 220 ~ 20 DEG C of heat exchanges are not once split, and glaze paint vickers microhardness is 8.3Gpa, and center resistance to impact shock is 2.3J/cm
2, plumbous, quantity of cadmium release is 0.
Claims (10)
1. strengthen a preparation method for beautiful matter porcelain, adopt raw mineral materials and industrial chemicals, the weight percent of its blank and glaze formula consists of:
Blank: Longyan kaolin 10 ~ 15%, Guizhou kaolin 8 ~ 15%, New Zealand's kaolin 5 ~ 10%, planetesimal feldspar 10 ~ 15%, planetesimal quartz 40 ~ 50%, Yifeng low temperature porcelain stone 5 ~ 10%, Jing Dezhen glaze fruit 3 ~ 5%, Heilungkiang wilkinite 3 ~ 5%, Yunnan china clay 3 ~ 5%;
Glaze: Longyan kaolin 8 ~ 12%, New Zealand's kaolin 3 ~ 5%, planetesimal feldspar 10 ~ 15%, planetesimal quartz 30 ~ 37%, Yifeng low temperature porcelain stone 8 ~ 12%, Leping rhombspar 15 ~ 20%, Leping calcite 5 ~ 10%, Jing Dezhen glaze fruit 8 ~ 10%, Yunnan china clay 5 ~ 10%;
Through blank and glaze preparation, shaping, dry, repaired biscuit, low temperature biscuiting, glazing, the glaze firing of high temperature reduction flame, decoration firing operation acquisition goods.
2. preparation method according to claim 1, it is characterized in that: described Slug preparing operation is by material: ball: the part by weight batching dress ball mill of water=1:1.5 ~ 1.7:1, Ball-milling Time 35 ~ 40 hours, blank ball milling fineness was 300 mesh sieves, tail over and be less than 0.1 ~ 0.3%, obtain solid particulate fineness and be less than the slurry that 6 microns reach 60 ~ 70%, described slurry after deironing is sieved, then is made powder by spray-drying tower or makes roll extrusion mud bar by press filt, pugging or make grout material by changing slurry after press filt sheet.
3. preparation method according to claim 1, it is characterized in that: described glaze preparation section is by material: ball: the part by weight batching dress ball mill of water=1:1.9 ~ 2.0:1, Ball-milling Time 40 ~ 45 hours, glaze ball milling fineness was 300 mesh sieves, tail over and be less than 0.01 ~ 0.03%, make glaze after glaze slip deironing after sieve for subsequent use.
4. preparation method according to claim 1, is characterized in that: described molding procedure comprises isostatic pressing, roll forming, injection forming.
5. preparation method according to claim 4, is characterized in that: in described isostatic pressing process, in spray-drying tower, the proportion of pug is 1570 ~ 1600g/l, and mobility is 50 ~ 70s/100ml, and the water ratio of obtained powder is 3 ~ 4%; In described flow forming process, pug moisture content is 22 ~ 25%; In described slip-casting shaping process, the unit weight of slip casing by pressure material is 1670 ~ 1690g/l, and changing slurry mobility is 130 ~ 160s/100ml; Manual grout material unit weight is 1620 ~ 1660g/ml, and mobility is 0.3%.
6. preparation method according to claim 5, is characterized in that: described spray-drying tower is adding additives 0.8 ~ 1.0%, thinner≤0.5% at home and abroad, and described binding agent is modified starch, and thinner is Sodium hexametaphosphate 99.
7. preparation method according to claim 1, is characterized in that: the temperature of described drying process is 40 ~ 50 DEG C.
8. preparation method according to claim 1, is characterized in that: in described glazing operation, glaze proportion is 1.25 ~ 1.29g/ml, and glazed thickness is 0.25 ~ 0.3mm.
9. preparation method according to claim 1, is characterized in that: described low temperature biscuiting temperature is 940 ~ 960 DEG C, the biscuiting cycle is 14 ~ 16 hours, and 880 DEG C of insulations 40 minutes, top temperature was incubated 30 minutes; High temperature reduction flame temperature of glaze firing is 1320 ~ 1340 DEG C, the glaze firing cycle is 25 ~ 27 hours, the highest temperature is incubated 60 minutes; In described decoration firing step, in-glaze decoration decoration firing temperature is 1200 ~ 1290 DEG C, and over-glaze decoration decoration firing temperature is 780 ~ 880 DEG C.
10. the beautiful matter porcelain products of strengthening that method is obtained according to claim 1, it is characterized in that: the whiteness of described product is 92 ~ 94, glossiness is 93 ~ 95, water-intake rate is 0.05 ~ 0.07, thermostability is that 220 ~ 20 DEG C of heat exchanges are not once split, glaze paint vickers microhardness is 8.3 ~ 8.5Gpa, and center resistance to impact shock is 2.3 ~ 2.5J/cm
2, plumbous, quantity of cadmium release is 0.
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| CN106278337A (en) * | 2016-08-11 | 2017-01-04 | 德化县毅术陶瓷研究所 | Oryza glutinosa tire high density mercerising jade porcelain and processing technology thereof |
| CN107056263A (en) * | 2017-04-27 | 2017-08-18 | 湖南港鹏实业有限公司 | A kind of preparation method of middle temperature feldspathic bone china |
| CN108947571A (en) * | 2018-09-19 | 2018-12-07 | 上海大实新型材料科技有限公司 | A kind of tourmaline ceramic product and preparation method thereof |
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| CN110981418A (en) * | 2019-12-30 | 2020-04-10 | 景德镇市望龙陶瓷有限公司 | Preparation method of colored glaze exquisite porcelain |
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| CN106278337A (en) * | 2016-08-11 | 2017-01-04 | 德化县毅术陶瓷研究所 | Oryza glutinosa tire high density mercerising jade porcelain and processing technology thereof |
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| CN108947571A (en) * | 2018-09-19 | 2018-12-07 | 上海大实新型材料科技有限公司 | A kind of tourmaline ceramic product and preparation method thereof |
| CN110171986A (en) * | 2019-07-01 | 2019-08-27 | 广东易成陶瓷实业有限公司 | A kind of production method of garland ceramics colouring |
| CN110981418A (en) * | 2019-12-30 | 2020-04-10 | 景德镇市望龙陶瓷有限公司 | Preparation method of colored glaze exquisite porcelain |
| CN110981417A (en) * | 2019-12-30 | 2020-04-10 | 景德镇市望龙陶瓷有限公司 | Preparation method of five-color exquisite porcelain |
| CN110981418B (en) * | 2019-12-30 | 2021-12-14 | 景德镇市望龙陶瓷有限公司 | Preparation method of colored glaze exquisite porcelain |
| CN110981417B (en) * | 2019-12-30 | 2022-04-22 | 景德镇市望龙陶瓷有限公司 | Preparation method of five-color exquisite porcelain |
| CN115321944A (en) * | 2022-06-27 | 2022-11-11 | 广西三环陶瓷小镇发展有限公司 | High-temperature hard in-glaze color porcelain and preparation method thereof |
| CN115321944B (en) * | 2022-06-27 | 2023-10-13 | 广西三环陶瓷小镇发展有限公司 | High-temperature hard in-glaze color porcelain and preparation method thereof |
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