CN106278337B - Glutinous rice tire high density mercerising jade porcelain and its manufacture craft - Google Patents
Glutinous rice tire high density mercerising jade porcelain and its manufacture craft Download PDFInfo
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- CN106278337B CN106278337B CN201610654679.5A CN201610654679A CN106278337B CN 106278337 B CN106278337 B CN 106278337B CN 201610654679 A CN201610654679 A CN 201610654679A CN 106278337 B CN106278337 B CN 106278337B
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
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- C04B33/00—Clay-wares
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/131—Inorganic additives
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- C04B33/32—Burning methods
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
Abstract
The present invention relates to ceramic fabrication technique field, it is specifically related to a kind of glutinous rice tire high density mercerising jade porcelain and its manufacture craft.This kind of glutinous rice tire high density mercerising jade porcelain, including Longyan kaolin, Yunnan kaolin, Guangxi kaolin, Guizhou kaolin, Jiangxi kaolin, Australia kaolin, Dehua kaolin, Afghan white jade, florisil silica, albite.Above-mentioned glutinous rice tire high density mercerising jade porcelain, it selects unique raw material components and unique burning process is used according to the characteristic of raw material, there are a large amount of Free quartz crystal and glass phases in made mercerising jade porcelain body body, secondary mullite needle, colour generation is gentle as beautiful, with sparkling and crystal-clear gloss, carcass density is high, water absorption rate and the porosity are low, it can be not required to when use plus color, glazing, the fine and soft hard cause of tire bone, sense of touch silk is sliding, the sound kowtowed such as single sonorous stone, with the color of traditional glutinous rice tire Dehua ceramic whiteware, romantic charm is very close, it is the recovery to traditional Dehua ceramic whiteware, have the function of for the popularization of Dehua ceramic whiteware positive.
Description
Technical field
The present invention relates to ceramic fabrication technique field, it is specifically related to a kind of glutinous rice tire high density mercerising jade porcelain and its production
Technique.
Background technique
For Dehua ceramic whiteware because its production is fine, quality heavily fortified point is close, and sparkling and crystal-clear as beautiful, glaze is moistened like rouge, therefore has " ivory
White ", " lard white ware ", " goose down is white " etc. laudatory titles, there is unique style in China's ceramic whiteware system, occupy in Chinaware Progression history
Critical role has the reputation of " oriental art " in the world.
Traditional Dehua ceramic whiteware is divided into " my child is red ", " ivory white ", " lard white ware ", " green onion root is white ", " goose down is white " etc., closely
As the reputation of Dehua ceramic whiteware increasingly improves over year, also more and more being paid close attention to for traditional Dehua ceramic whiteware is restored, is such as applied public
Accuse and number disclose a kind of composition of raw materials of lard ceramic whiteware for an application for a patent for invention of CN201310265837.4, composition of raw materials by
Silica, aluminum oxide, di-iron trioxide, calcium oxide, magnesia, potassium oxide, sodium oxide molybdena, titanium dioxide, barium monoxide, oxygen
Change strontium composition.This kind of lard white ware porcelain formula changes existing can only become by cellar once in a while and obtains the status of lard ceramic whiteware,
Lard ceramic whiteware can be made by conventional method for cooking in composition of raw materials according to the invention.
Existing Dehua ceramic whiteware be more pursue surface, similar on color, and really the romantic charm of Dehua ceramic whiteware be from
It embodies, is commonly called as " glutinous rice tire " in tire, the fine and soft hard cause of tire bone, with sparkling and crystal-clear gloss, colour generation is gentle as beautiful, exquisitely carved smooth, body
In the case where light shines, can reflect and see finger shadow, the sound kowtowed please clearly it is melodious, like tap metal, it is loud and clear to make a sound.And traditional Dehua is white
Porcelain must use Dehua kaolin as raw material, just be able to achieve glutinous rice tire, and Dehua as non-renewable resources is high
Ridge soil, has developed totally now, it is rare and expensive to deposit generation amount.In recent years, the reputation of Dehua ceramic whiteware increasingly improves, with
Dehua County be cited as world's town of porcelain, pass through improvement composition of raw materials and production technology restore Dehua ceramic whiteware closest to traditional romantic charm
Not only there is economic significance, have more social effect and historic significance.
Summary of the invention
For overcome the deficiencies in the prior art, the present invention provides a kind of glutinous rice tire high density mercerising jade porcelain and its preparation sides
Method and its manufacture craft.
To achieve the above object, glutinous rice tire high density mercerising jade porcelain, which is characterized in that the high density mercerising jade porcelain includes
Component is as follows: kaolin 15-20 parts of Longyan, kaolin 10-15 parts of Yunnan, kaolin 10-15 parts of Guangxi, Guizhou kaolin 10-
15 parts, kaolin 10-15 parts of Jiangxi, kaolin 10-15 parts of Australia, kaolin 0-5 parts of Dehua, Afghan white jade 5-10
Part, 1-10 parts of florisil silica, 1-5 parts of albite.
Optimization, 16 parts of Longyan kaolin, 14 parts of Yunnan kaolin, 12 parts of Guangxi kaolin, 13 parts of Guizhou kaolin, river
10 parts of western kaolin, 13 parts of Australia kaolin, 1 part of Dehua kaolin, Afghan 8 parts of white jade, 8 parts of florisil silica, sodium
5 parts of feldspar.
Optimization, 20 parts of Longyan kaolin, 10 parts of Yunnan kaolin, 11 parts of Guangxi kaolin, 10 parts of Guizhou kaolin, river
13 parts of western kaolin, 14 parts of Australia kaolin, Afghan 10 parts of white jade, 9 parts of florisil silica, 3 parts of albite.
Optimization, 15 parts of Longyan kaolin, 12 parts of Yunnan kaolin, 14 parts of Guangxi kaolin, 14 parts of Guizhou kaolin, river
11 parts of western kaolin, 12 parts of Australia kaolin, 5 parts of Dehua kaolin, Afghan 6 parts of white jade, 7 parts of florisil silica, sodium
4 parts of feldspar.
Optimization, 18 parts of Longyan kaolin, 13 parts of Yunnan kaolin, 11 parts of Guangxi kaolin, 14 parts of Guizhou kaolin, river
12 parts of western kaolin, 13 parts of Australia kaolin, 3 parts of Dehua kaolin, Afghan 7 parts of white jade, 6 parts of florisil silica, sodium
3 parts of feldspar.
A kind of manufacture craft of glutinous rice tire high density mercerising jade porcelain prepares glutinous rice described in claim 1-5 any one
Tire high density mercerising jade porcelain, the specific steps are as follows:
Step 1, it is matched according to the raw material of high glutinous rice tire high density mercerising jade porcelain, chinaware body is made；
Step 2, blank is made；
Step 3, it is put into kiln after body drying；
Step 4, kiln was warming up to 350-450 DEG C by room temperature through 1-2 hours；
Step 5, kiln continues to heat up, and is at the uniform velocity warming up to 800 DEG C by 450 DEG C through 2-3 hours；
Step 6, furnace heating-up is kept for 20-40 minutes to 1200 DEG C；
Step 7, kiln continues to heat up, and when being warming up to 1335-1350 DEG C, keeps the temperature 1-2 hours；
Step 8, blow-on after kiln slow cooling to room temperature obtains glutinous rice tire high density mercerising jade porcelain.
Further, in step 6 kiln by 800 DEG C be warming up to 1200 DEG C pass through 1-2 hours.
Further, kiln by 1200 DEG C is warming up to 1335-1350 DEG C through 2-3 hours in step 7.
Further, step 8 kiln is at the uniform velocity cooled to 1100 DEG C by 1335-1350 DEG C, keeps the temperature 20-30 minutes.
Further, kiln is at the uniform velocity cooled to 800 DEG C by 1100 DEG C, keeps the temperature 20-30 minutes.
By the above-mentioned description of this invention it is found that glutinous rice tire high density mercerising jade porcelain provided by the invention, is selected unique
Raw material components simultaneously use unique burning process according to the characteristic of raw material, exist in made mercerising jade porcelain body body a large amount of free
Quartz crystal and glass phase, secondary mullite needle, colour generation it is gentle as it is beautiful, with sparkling and crystal-clear gloss, carcass density is high, water absorption rate
Low with the porosity, when use, can be not required to plus color, glazing, tire bone it is fine and soft it is hard cause, sense of touch silk it is sliding, the sound kowtowed such as single sonorous stone is and traditional
The color of glutinous rice tire Dehua ceramic whiteware, romantic charm are very close, are the recoveries to traditional Dehua ceramic whiteware, have for the popularization of Dehua ceramic whiteware
Play the role of positive.
Specific embodiment
Below by way of specific embodiment, the invention will be further described.
Glutinous rice tire high density mercerising jade porcelain, which is characterized in that the high density mercerising jade porcelain includes that component is as follows: Longyan is high
Soil 15-20 parts of ridge, kaolin 10-15 parts of Yunnan, kaolin 10-15 parts of Guangxi, kaolin 10-15 parts of Guizhou, Jiangxi kaolin
10-15 parts, kaolin 10-15 parts of Australia, kaolin 0-5 parts of Dehua, Afghan 5-10 parts of white jade, florisil silica 1-10
Part, 1-5 parts of albite.
A kind of manufacture craft of glutinous rice tire high density mercerising jade porcelain prepares above-mentioned glutinous rice tire high density mercerising jade porcelain, tool
Steps are as follows for body:
Step 1, it is matched according to the raw material of high glutinous rice tire high density mercerising jade porcelain, chinaware body is made；
Step 2, blank is made；
Step 3, it is put into kiln after body drying；
Step 4, kiln was warming up to 350-450 DEG C by room temperature through 1-2 hours；
Step 5, kiln continues to heat up, and is at the uniform velocity warming up to 800 DEG C by 450 DEG C through 2-3 hours；
Step 6, kiln was warming up to 1200 DEG C by 1-2 hours, was kept for 20-40 minutes；
Step 7, when kiln is warming up to 1335-1350 DEG C in 2-3 hours, 1-2 hours are kept the temperature；
Step 8, kiln is at the uniform velocity cooled to 1100 DEG C by 1335-1350 DEG C, keeps the temperature 20-30 minutes；
Step 9, kiln is at the uniform velocity cooled to 800 DEG C by 1100 DEG C, keeps the temperature 20-30 minutes, after continue to open after being cooled to room temperature
Furnace obtains glutinous rice tire high density mercerising jade porcelain.
Specific embodiment one:
16 parts of Longyan kaolin, 14 parts of Yunnan kaolin, 12 parts of Guangxi kaolin, 13 parts of Guizhou kaolin, Jiangxi kaolinite
10 parts of soil, 13 parts of Australia kaolin, 1 part of Dehua kaolin, Afghan 8 parts of white jade, 8 parts of florisil silica, albite 5
Part.
When firing, temperature control is as follows:
A: through 1 hour, 360 DEG C are warming up to by room temperature；
B: kiln continues to heat up, and is at the uniform velocity warming up to 800 DEG C by 360 DEG C through 2.3 hours；
C: kiln was warming up to 1200 DEG C by 1.5 hours, was kept for 30 minutes；
D: when kiln is warming up to 1340 DEG C in 3 hours, 1 hour is kept the temperature；
E: kiln is at the uniform velocity cooled to 1100 DEG C by 1340 DEG C, keeps the temperature 30 minutes；
F: kiln is at the uniform velocity cooled to 800 DEG C by 1100 DEG C, keeps the temperature 25 minutes, after continue to be cooled to blow-on after room temperature, obtain
Glutinous rice tire high density mercerising jade porcelain.
Specific embodiment two:
20 parts of Longyan kaolin, 10 parts of Yunnan kaolin, 11 parts of Guangxi kaolin, 10 parts of Guizhou kaolin, Jiangxi kaolinite
13 parts of soil, 14 parts of Australia kaolin, Afghan 10 parts of white jade, 9 parts of florisil silica, 3 parts of albite.
When firing, temperature control is as follows:
A: kiln is warming up to 430 DEG C through 2 hours, by room temperature；
B: kiln continues to heat up, and is at the uniform velocity warming up to 800 DEG C by 430 DEG C through 2.5 hours；
C: kiln was warming up to 1200 DEG C by 1.5 hours, was kept for 25 minutes；
D: when kiln is warming up to 1350 DEG C in 3 hours, 2 hours are kept the temperature；
E: kiln is at the uniform velocity cooled to 1100 DEG C by 1350 DEG C, keeps the temperature 28 minutes；
F: kiln is at the uniform velocity cooled to 800 DEG C by 1100 DEG C, keeps the temperature 20 minutes, after continue to be cooled to blow-on after room temperature, obtain
Glutinous rice tire high density mercerising jade porcelain.
Specific embodiment three:
15 parts of Longyan kaolin, 12 parts of Yunnan kaolin, 14 parts of Guangxi kaolin, 14 parts of Guizhou kaolin, Jiangxi kaolinite
11 parts of soil, 12 parts of Australia kaolin, 5 parts of Dehua kaolin, Afghan 6 parts of white jade, 7 parts of florisil silica, albite 4
Part.
When firing, temperature control is as follows:
A: kiln is warming up to 400 DEG C through 1.8 hours, by room temperature；
B: kiln continues to heat up, and is at the uniform velocity warming up to 800 DEG C by 400 DEG C through 2 hours；
C: kiln was warming up to 1200 DEG C by 1 hour, was kept for 40 minutes；
D: when kiln is warming up to 1345 DEG C in 3 hours, 2 hours are kept the temperature；
E: kiln is at the uniform velocity cooled to 1100 DEG C by 1345 DEG C, keeps the temperature 30 minutes；
F: kiln is at the uniform velocity cooled to 800 DEG C by 1100 DEG C, keeps the temperature 25 minutes, after continue to be cooled to blow-on after room temperature, obtain
Glutinous rice tire high density mercerising jade porcelain.
Specific embodiment four:
18 parts of Longyan kaolin, 13 parts of Yunnan kaolin, 11 parts of Guangxi kaolin, 14 parts of Guizhou kaolin, Jiangxi kaolinite
12 parts of soil, 13 parts of Australia kaolin, 3 parts of Dehua kaolin, Afghan 7 parts of white jade, 6 parts of florisil silica, albite 3
Part.
When firing, temperature control is as follows:
A: kiln is warming up to 450 DEG C through 2 hours, by room temperature；
B: kiln continues to heat up, and is at the uniform velocity warming up to 800 DEG C by 450 DEG C through 2.8 hours；
C: kiln was warming up to 1200 DEG C by 2 hours, was kept for 40 minutes；
D: when kiln is warming up to 1335 DEG C in 3 hours, 2 hours are kept the temperature；
E: kiln is at the uniform velocity cooled to 1100 DEG C by 1335 DEG C, keeps the temperature 30 minutes；
F: kiln is at the uniform velocity cooled to 800 DEG C by 1100 DEG C, keeps the temperature 25 minutes, after continue to be cooled to blow-on after room temperature, obtain
Glutinous rice tire high density mercerising jade porcelain.
It above are only the specific embodiment of the present invention, but the design concept of the present invention is not limited to this, all benefits
It is made a non-material change to the present invention, should all be belonged to behavior that violates the scope of protection of the present invention with this design.
Claims (9)
1. glutinous rice tire high density mercerising jade porcelain, which is characterized in that the high density mercerising jade porcelain includes that component is as follows: Longyan kaolinite
15-20 parts native, kaolin 10-15 parts of Yunnan, kaolin 10-15 parts of Guangxi, kaolin 10-15 parts of Guizhou, Jiangxi kaolin 10-
15 parts, kaolin 10-15 parts of Australia, kaolin 0-5 parts of Dehua, Afghan 5-10 parts of white jade, 1-10 parts of florisil silica,
1-5 parts of albite；
The preparation process of the glutinous rice tire high density mercerising jade porcelain, the specific steps are as follows:
Step 1, it is matched according to the raw material of high glutinous rice tire high density mercerising jade porcelain, chinaware body is made；
Step 2, blank is made；
Step 3, it is put into kiln after body drying；
Step 4, kiln was warming up to 350-450 DEG C by room temperature through 1-2 hours；
Step 5, kiln continues to heat up, and is at the uniform velocity warming up to 800 DEG C by 350-450 DEG C through 2-3 hours；
Step 6, furnace heating-up is kept for 20-40 minutes to 1200 DEG C；
Step 7, kiln continues to heat up, and when being warming up to 1335-1350 DEG C, keeps the temperature 1-2 hours；
Step 8, blow-on after kiln slow cooling to room temperature obtains glutinous rice tire high density mercerising jade porcelain.
2. glutinous rice tire high density mercerising jade porcelain according to claim 1, it is characterised in that: 16 parts of Longyan kaolin,
14 parts of Yunnan kaolin, 12 parts of Guangxi kaolin, 13 parts of Guizhou kaolin, 10 parts of Jiangxi kaolin, 13 parts of Australia kaolin, moral
Change local 1 part of kaolin, Afghan 8 parts of white jade, 8 parts of florisil silica, 5 parts of albite.
3. glutinous rice tire high density mercerising jade porcelain according to claim 1, it is characterised in that: 20 parts of Longyan kaolin,
10 parts of Yunnan kaolin, 11 parts of Guangxi kaolin, 10 parts of Guizhou kaolin, 13 parts of Jiangxi kaolin, 14 parts of Australia kaolin, Ah
10 parts of rich sweat white jade, 9 parts of florisil silica, 3 parts of albite.
4. glutinous rice tire high density mercerising jade porcelain according to claim 1, it is characterised in that: 15 parts of Longyan kaolin,
12 parts of Yunnan kaolin, 14 parts of Guangxi kaolin, 14 parts of Guizhou kaolin, 11 parts of Jiangxi kaolin, 12 parts of Australia kaolin, moral
Change local 5 parts of kaolin, Afghan 6 parts of white jade, 7 parts of florisil silica, 4 parts of albite.
5. glutinous rice tire high density mercerising jade porcelain according to claim 1, it is characterised in that: 18 parts of Longyan kaolin,
13 parts of Yunnan kaolin, 11 parts of Guangxi kaolin, 14 parts of Guizhou kaolin, 12 parts of Jiangxi kaolin, 13 parts of Australia kaolin, moral
Change local 3 parts of kaolin, Afghan 7 parts of white jade, 6 parts of florisil silica, 3 parts of albite.
6. glutinous rice tire high density mercerising jade porcelain according to claim 1, which is characterized in that kiln is risen by 800 DEG C in step 6
Temperature is to 1200 DEG C by 1-2 hours.
7. glutinous rice tire high density mercerising jade porcelain according to claim 1, it is characterised in that: in the step 7 kiln by
1200 DEG C were warming up to 1335-1350 DEG C through 2-3 hours.
8. glutinous rice tire high density mercerising jade porcelain according to claim 1, it is characterised in that: step 8 kiln is by 1335-
1350 DEG C are at the uniform velocity cooled to 1100 DEG C, keep the temperature 20-30 minutes.
9. glutinous rice tire high density mercerising jade porcelain according to claim 8, it is characterised in that: the kiln by 1100 DEG C at the uniform velocity
800 DEG C are cooled to, keeps the temperature 20-30 minutes.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107216127B (en) * | 2017-06-21 | 2019-09-03 | 泉州市陶瓷科学技术研究所 | Dehua pearl white porcelain and its preparation process |
| CN107216119B (en) * | 2017-06-21 | 2019-09-20 | 泉州市陶瓷科学技术研究所 | Ceramic whiteware and its preparation process are built in Dehua |
| CN107337432B (en) * | 2017-06-21 | 2019-09-27 | 泉州市陶瓷科学技术研究所 | Dehua glutinous rice tire ceramic whiteware and its preparation process |
| CN110776306A (en) * | 2019-12-11 | 2020-02-11 | 福建省德化县飞天陶瓷艺术研究所 | Solid jade porcelain and preparation process thereof |
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| CN101913843A (en) * | 2010-07-23 | 2010-12-15 | 华南理工大学 | Preparation method of emerald ceramic |
| CN102336563A (en) * | 2011-06-24 | 2012-02-01 | 黄丽君 | Processing method for five colored jade porcelain |
| CN103833329A (en) * | 2014-03-12 | 2014-06-04 | 于国泉 | Preparation method of reinforced bone china and product prepared therefrom |
| CN105060843A (en) * | 2015-08-17 | 2015-11-18 | 景德镇红叶陶瓷股份有限公司 | Preparation method of reinforced jade-based porcelain and product made of reinforced jade-based porcelain |
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