CN105417953A - Ceramic jade white glaze and glaze application method - Google Patents
Ceramic jade white glaze and glaze application method Download PDFInfo
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- CN105417953A CN105417953A CN201511010557.4A CN201511010557A CN105417953A CN 105417953 A CN105417953 A CN 105417953A CN 201511010557 A CN201511010557 A CN 201511010557A CN 105417953 A CN105417953 A CN 105417953A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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Abstract
The invention discloses ceramic jade white glaze. The comprises the following ingredients, by weight, 48-52 parts of albite, 5-8 parts of calcium carbonate, 7-9 parts of kaolin, 33-36 parts of quartz, 5-7 parts of barium carbonate, 0.4-0.6 part of calcium borate, 1-3 parts of strontium carbonate, 0.5-1.5 parts of bentonite and 0.01-0.02 part of methyl cellulose. Glazing modes comprise glaze soaking and glaze spraying twice. The sintering curve comprises four stages of 1 DEG C-300 DEG C, 300 DEG C-600 DEG C, 600 DEG C -1000 DEG C and 600 DEG C-1330 DEG C. The ceramic jade white glaze has a low cost and a wide adaptability, the saying is changed that Dehua ceramic whiteware only depends on good porcelain clay in history, a ceramic product made from the provided ceramic jade white glaze and through the glaze application method is oily and fleshy like Hetian jade and is ivory, and a layer of brightness appears on the glaze surface. Especially, when thickening is carried out during glaze application of a green body especially, the glaze flows vertically when high temperature sintering and when the glaze fluid flows and deposits, the Hetian jade texture is strong and the lightspot is shown.
Description
Technical field
The present invention relates to the field of domestic ceramics and art ceramics, be specifically related to a kind of ceramic beautiful white glaze material and enameling method thereof.
Background technology
Blacn de chine, is called for short " Chinese white ", and " Chinese white " pottery has long history in China, the Northern Wei Dynasty ceramic whiteware discovery, in the age occurred the earliest by ceramic whiteware, advanceed to the Northern Wei Dynasty from the Northern Qi Dynasty, rewrite Chinese pottery history, the ceramic whiteware of the ivory white i.e. pure transparent of Ming Dynasty's Dahua ware.Because ferric oxide content in glaze is low especially, and the content of potassium oxide is not high especially, adds when burning till and adopts neutral atmosphere, so color is pure especially.From the appearance bright in luster bright; Under illumination, dimly visible pink or milky white in glaze, therefore there are lard white ware, ivory white title.European is characterized as also known as this pottery that goose down is white, Chinese white.Occurred countless outstanding ceramic works and technique in the evolution of several thousand, most of product and technique are also common people's succession so far, are the contribution of mankind's happiness.
Dehua County, Fujian Province is quite well-known local kiln.Its glaze colours is white as congealed fat, and Dehua ceramic whiteware, also known as ivory white, as Song, the powder box, little vase, tea set etc. in first period, also have most typical porcelain carving to be foremost goods in the porcelain of Dehua, just has the people such as famous artist He Chaozong, Lin Chaojing, Zhang Shoushan during the Ming Dynasty.Dehua ceramic whiteware is just well-known at home and abroad with its peculiar " ivory white ", " Chinese white " early than the period of Ming and Qing.
Ming Dynasty's Dehua ceramic whiteware has the style of its uniqueness, and it is not only different from the ceramic whiteware in Tang, other areas of Song Shidai, and the ceramic whiteware produced with the Jing Dezhen contemporaneously is also peculiar.Its (1) porcelain body is fine and close, and printing opacity is extremely good, less than other regional ceramic whitewares of Tang and Song Dynasty.Tang and Song Dynasty north ceramic whiteware, be fire with the clay that alumina content is higher, it is few that clay includes flux material, therefore device tire inadequate between difference mainly contain: fine and close, transparence is poor.Dehua ceramic whiteware then uses potassium oxide, and content is up to 6%, and it is more to burn till the rear glassiness, and thus its porcelain body is fine and close, and transparence is good especially.
(2) from glaze paint, Dehua white glaze is pure white glaze (belonging to pure transparent), and the white ceramic glaze in north epoch Tang and Song Dynasty is then general faint yellow.Slight general green grass or young crops in the ceramic whiteware that Jing Dezhen of first, bright epoch produces is white, has obvious difference with Dehua ceramic whiteware.Cause the reason of this difference, not only relevant, also relevant with the character of firing atmosphere with the content of the chemical constitution, particularly ferric oxide of raw material, titanium oxide.The feature of north ceramic whiteware is that in tire, glaze, Tio, Aio comparision contents is high, adopt oxidizing atmosphere, therefore porcelain presents the tone of white middle yellowing when burning till; The feature of Jing Dezhen ceramic whiteware is that in tire glaze, Fe, Tio, Aio content is all more moderate, adopt reducing atmosphere, therefore porcelain presents the tone of white inner general green grass or young crops when burning till; The feature of Dehua ceramic whiteware is that the Feo content in tire glaze is high especially, adopts neutral atmosphere when burning till, so Dehua ceramic whiteware is just purer than the ceramic whiteware glaze colours of Tang and Song Dynasty north ceramic whiteware and the Jing Dezhen production same period.From the appearance, Ming Dynasty's Dehua ceramic whiteware is bright in luster bright, milky white as congealed fat, under illumination, dimly visible pink or milky white in glaze.Therefore the title of " lard white ware ", " ivory white ", " maiden is white " is had.Spread behind Europe, the foreigner is referred to as again " goose down is white ".Up to now, Frenchman also directly exhales Dahua ware ceramic whiteware with " Chinese white ".
(3) from the transparency that porcelain, glaze combine, Dehua ceramic whiteware is all the saying of " tire starved glaze is thin " from ancient times to the present, and the transparency of adding Dehua china clay is good, seems glittering and translucent especially, but the not plump sense of glaze colours, glossy not, resistance toly not sees.
But " Chinese white " in Dehua from ancient times to the present, be all carry out color development well by selected china clay quality, so Dehua ceramic whiteware can not talk about the change of glaze skill with other kilneye, can only talk china clay fine at all.Ceramic product to manufacture with glaze preparation composition, special glazing technology and firing process thereof be important key problem in technology, and in order to " Chinese white " in Dehua is promoted, just need to make in the technique such as glaze formula, firing condition and explore and innovation, can go up by common china clay quality " beautiful white glaze ", both saved the superfine kaolin resource of " rare ", and can reduce costs again.
Summary of the invention
The technical problem to be solved in the present invention is the superfine kaolin that the making of " Chinese white " in the Dehua overcoming prior art needs to rely on selected " rare ", the defect high to china clay specification of quality, provides a kind of ceramic beautiful white glaze material and enameling method thereof.
In order to solve the problems of the technologies described above, the invention provides following technical scheme:
A kind of ceramic beautiful white glaze material, comprises each component of following parts by weight: albite 48 ~ 52 parts, 5 ~ 8 parts, calcium carbonate, kaolin 7 ~ 9 parts, 33 ~ 36 parts, quartz, barium carbonate 5 ~ 7 parts, lime borate 0.4 ~ 0.6 part, Strontium carbonate powder 1 ~ 3 part, bentonite 0.5 ~ 1.5 part, methylcellulose gum 0.01 ~ 0.02 part.
Further, a kind of ceramic beautiful white glaze material, comprises each component of following parts by weight: albite 50 parts, 6 parts, calcium carbonate, kaolin 8 parts, 35 parts, quartz, barium carbonate 6 parts, lime borate 0.5 part, Strontium carbonate powder 2 parts, bentonite 1 part, methylcellulose gum 0.015 part.
An enameling method for the beautiful white glaze material of pottery, comprises following step:
(1), by recipe configuration pottery 100 kilograms, beautiful white glaze material, add water 110 kilograms, stir, obtained glaze slip;
(2), by the biscuiting 4 ~ 5 hours at 800 DEG C of shaping porcelain base, naturally cooling is stand-by;
(3), porcelain base is dipped in glaze slip by leaching glaze, and control porcelain base glaze layer at 0.2 ~ 0.5 ㎜, surface is dried;
(4), glaze slip is sprayed onto on base substrate by glaze spraying, and first time glaze spraying thickness is 0.1mm ~ 0.2mm, and surface is dried, and then carries out second time glaze spraying, and the thickness of glaze spraying is for the second time 0.15mm ~ 0.3mm, dries;
(5), converter is fired base substrate to send in tunnel furnace and is sintered
First stage at the uniform velocity heats up from 1 DEG C ~ 300 DEG C, 90 minutes time;
Subordinate phase 300 DEG C ~ 600 DEG C at the uniform velocity heats up, 100 minutes time;
Phase III 600 DEG C ~ 1000 DEG C at the uniform velocity heats up, 100 minutes time;
Fourth stage 600 DEG C at the uniform velocity heats up to the highest 1330 DEG C of furnace temperature, 200 minutes time;
(6), cooling per minute of coming out of the stove lowers the temperature 8 DEG C ~ 10 DEG C; In 240 minutes, 800 DEG C are cooled to from 1330 DEG C; Then Temperature fall is to kiln discharge quality inspection.
Further, the firing atmosphere that in described step (5), converter is fired is pure zirconia flame.
The beautiful white glaze material of pottery of the present invention, cost is low, wide adaptability, having only had by the good saying of china clay since changing Dehua ceramic whiteware history, is performance Chinese white equally, can with other ceramic producing region than glaze skill, than beautiful texture, world-famous " Chinese white " is more stepped to a new level.Adopt the ceramic product that glaze of the present invention and enameling method thereof are made, just as glossy plumpness as " Khotan jade ", in ivory white, one deck that glaze paint rises is bright.Particularly when base substrate glazing thickeies especially, when high temperature burns till, glaze can hang down stream, along with glaze juice trickling accumulation, stronger in " Khotan jade " texture, embodies bright spot.
Embodiment
Below the preferred embodiments of the present invention are described, should be appreciated that preferred embodiment described herein is only for instruction and explanation of the present invention, is not intended to limit the present invention.
embodiment 1
A kind of ceramic beautiful white glaze material, comprises each component of following parts by weight: albite 48 parts, 5 parts, calcium carbonate, kaolin 7 parts, 33 parts, quartz, barium carbonate 5 parts, lime borate 0.4 part, Strontium carbonate powder 1 part, bentonite 0.5 part, methylcellulose gum 0.01 part.
An enameling method for the beautiful white glaze material of pottery, comprises following step:
(1), by recipe configuration pottery 100 kilograms, beautiful white glaze material, add water 110 kilograms, stir, obtained glaze slip;
(2), by the biscuiting 4 hours at 800 DEG C of shaping porcelain base, naturally cooling is stand-by;
(3), porcelain base is dipped in glaze slip by leaching glaze, and control porcelain base glaze layer at 0.5 ㎜, surface is dried;
(4), glaze slip is sprayed onto on base substrate by glaze spraying, and first time glaze spraying thickness is 0.2mm, and surface is dried, and then carries out second time glaze spraying, and the thickness of glaze spraying is for the second time 0.3mm, dries;
(5), converter is fired base substrate to send in tunnel furnace and is sintered
First stage at the uniform velocity heats up from 1 DEG C ~ 300 DEG C, 90 minutes time;
Subordinate phase 300 DEG C ~ 600 DEG C at the uniform velocity heats up, 100 minutes time;
Phase III 600 DEG C ~ 1000 DEG C at the uniform velocity heats up, 100 minutes time;
Fourth stage 600 DEG C at the uniform velocity heats up to the highest 1330 DEG C of furnace temperature, 200 minutes time;
(6), cooling per minute of coming out of the stove lowers the temperature 8 DEG C DEG C; In 240 minutes, 800 DEG C are cooled to from 1330 DEG C; Then Temperature fall is to kiln discharge quality inspection.
embodiment 2
A kind of ceramic beautiful white glaze material, comprises each component of following parts by weight: albite 52 parts, 8 parts, calcium carbonate, kaolin 9 parts, 36 parts, quartz, barium carbonate 7 parts, lime borate 0.6 part, Strontium carbonate powder 3 parts, bentonite 1.5 parts, methylcellulose gum 0.02 part.
An enameling method for the beautiful white glaze material of pottery, comprises following step:
(1), by recipe configuration pottery 100 kilograms, beautiful white glaze material, add water 110 kilograms, stir, obtained glaze slip;
(2), by the biscuiting 5 hours at 800 DEG C of shaping porcelain base, naturally cooling is stand-by;
(3), porcelain base is dipped in glaze slip by leaching glaze, and control porcelain base glaze layer at 0.2 ㎜, surface is dried;
(4), glaze slip is sprayed onto on base substrate by glaze spraying, and first time glaze spraying thickness is 0.1mmmm, and surface is dried, and then carries out second time glaze spraying, and the thickness of glaze spraying is for the second time 0.15mmmm, dries;
(5), converter is fired base substrate to send in tunnel furnace and is sintered
First stage at the uniform velocity heats up from 1 DEG C ~ 300 DEG C, 90 minutes time;
Subordinate phase 300 DEG C ~ 600 DEG C at the uniform velocity heats up, 100 minutes time;
Phase III 600 DEG C ~ 1000 DEG C at the uniform velocity heats up, 100 minutes time;
Fourth stage 600 DEG C at the uniform velocity heats up to the highest 1330 DEG C of furnace temperature, 200 minutes time;
(6), cooling per minute of coming out of the stove lowers the temperature 10 DEG C; In 240 minutes, 800 DEG C are cooled to from 1330 DEG C; Then Temperature fall is to kiln discharge quality inspection.
embodiment 3
A kind of ceramic beautiful white glaze material, comprises each component of following parts by weight: albite 50 parts, 6 parts, calcium carbonate, kaolin 8 parts, 35 parts, quartz, barium carbonate 6 parts, lime borate 0.5 part, Strontium carbonate powder 2 parts, bentonite 1 part, methylcellulose gum 0.015 part.
An enameling method for the beautiful white glaze material of pottery, comprises following step:
(1), by recipe configuration pottery 100 kilograms, beautiful white glaze material, add water 110 kilograms, stir, obtained glaze slip;
(2), by the biscuiting 4.5 hours at 800 DEG C of shaping porcelain base, naturally cooling is stand-by;
(3), porcelain base is dipped in glaze slip by leaching glaze, and control porcelain base glaze layer at 0.4 ㎜, surface is dried;
(4), glaze slip is sprayed onto on base substrate by glaze spraying, and first time glaze spraying thickness is 0.15mm, and surface is dried, and then carries out second time glaze spraying, and the thickness of glaze spraying is for the second time 0.2mm, dries;
(5), converter is fired base substrate to send in tunnel furnace and is sintered
First stage at the uniform velocity heats up from 1 DEG C ~ 300 DEG C, 90 minutes time;
Subordinate phase 300 DEG C ~ 600 DEG C at the uniform velocity heats up, 100 minutes time;
Phase III 600 DEG C ~ 1000 DEG C at the uniform velocity heats up, 100 minutes time;
Fourth stage 600 DEG C at the uniform velocity heats up to the highest 1330 DEG C of furnace temperature, 200 minutes time;
(6), cooling per minute of coming out of the stove lowers the temperature 9 DEG C; In 240 minutes, 800 DEG C are cooled to from 1330 DEG C; Then Temperature fall is to kiln discharge quality inspection.
The firing atmosphere that in step (5), converter is fired is pure zirconia flame.
Last it is noted that the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.
Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (4)
1. the beautiful white glaze material of pottery, it is characterized in that, comprise each component of following parts by weight: albite 48 ~ 52 parts, 5 ~ 8 parts, calcium carbonate, kaolin 7 ~ 9 parts, 33 ~ 36 parts, quartz, barium carbonate 5 ~ 7 parts, lime borate 0.4 ~ 0.6 part, Strontium carbonate powder 1 ~ 3 part, bentonite 0.5 ~ 1.5 part, methylcellulose gum 0.01 ~ 0.02 part.
2. a kind of ceramic beautiful white glaze material as claimed in claim 1, it is characterized in that, comprise each component of following parts by weight: albite 50 parts, 6 parts, calcium carbonate, kaolin 8 parts, 35 parts, quartz, barium carbonate 6 parts, lime borate 0.5 part, Strontium carbonate powder 2 parts, bentonite 1 part, methylcellulose gum 0.015 part.
3. an enameling method for the beautiful white glaze material of a kind of pottery as claimed in claim 1, is characterized in that, comprise following step:
(1), by recipe configuration pottery 100 kilograms, beautiful white glaze material, add water 110 kilograms, stir, obtained glaze slip;
(2), by the biscuiting 4 ~ 5 hours at 800 DEG C of shaping porcelain base, naturally cooling is stand-by;
(3), porcelain base is dipped in glaze slip by leaching glaze, and control porcelain base glaze layer at 0.2 ~ 0.5 ㎜, surface is dried;
(4), glaze slip is sprayed onto on base substrate by glaze spraying, and first time glaze spraying thickness is 0.1mm ~ 0.2mm, and surface is dried, and then carries out second time glaze spraying, and the thickness of glaze spraying is for the second time 0.15mm ~ 0.3mm, dries;
(5), converter is fired base substrate to send in tunnel furnace and is sintered
First stage at the uniform velocity heats up from 1 DEG C ~ 300 DEG C, 90 minutes time;
Subordinate phase 300 DEG C ~ 600 DEG C at the uniform velocity heats up, 100 minutes time;
Phase III 600 DEG C ~ 1000 DEG C at the uniform velocity heats up, 100 minutes time;
Fourth stage 600 DEG C at the uniform velocity heats up to the highest 1330 DEG C of furnace temperature, 200 minutes time;
(6), cooling per minute of coming out of the stove lowers the temperature 8 DEG C ~ 10 DEG C; In 240 minutes, 800 DEG C are cooled to from 1330 DEG C; Then Temperature fall is to kiln discharge quality inspection.
4. the enameling method of the beautiful white glaze material of a kind of a kind of pottery as claimed in claim 1 as claimed in claim 1, is characterized in that, the firing atmosphere that in described step (5), converter is fired is pure zirconia flame.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107216127A (en) * | 2017-06-21 | 2017-09-29 | 泉州市陶瓷科学技术研究所 | Dehua pearl white porcelain and its preparation technology |
| CN107673611A (en) * | 2017-10-25 | 2018-02-09 | 福建省德化县福金兴陶瓷有限责任公司 | One kind profit white glaze and its preparation technology |
| CN108249887A (en) * | 2018-03-22 | 2018-07-06 | 福建省德化县中国白陶瓷有限责任公司 | A kind of ivory white ceramic of high brightness and its manufacture craft |
| CN108821591A (en) * | 2018-07-30 | 2018-11-16 | 赵红刚 | A kind of jade white glaze material and preparation method thereof |
| CN112552019A (en) * | 2020-12-11 | 2021-03-26 | 江西省金海利陶瓷有限公司 | Formula of slip glaze for high-temperature firing of bone domestic porcelain |
| CN113149599A (en) * | 2021-03-17 | 2021-07-23 | 李玉桃 | High-strength light egg white enamel |
| CN115286245A (en) * | 2022-07-26 | 2022-11-04 | 姚剑锋 | Hetian jade glaze and glazing method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107216127A (en) * | 2017-06-21 | 2017-09-29 | 泉州市陶瓷科学技术研究所 | Dehua pearl white porcelain and its preparation technology |
| CN107216127B (en) * | 2017-06-21 | 2019-09-03 | 泉州市陶瓷科学技术研究所 | Dehua pearl white porcelain and its preparation process |
| CN107673611A (en) * | 2017-10-25 | 2018-02-09 | 福建省德化县福金兴陶瓷有限责任公司 | One kind profit white glaze and its preparation technology |
| CN108249887A (en) * | 2018-03-22 | 2018-07-06 | 福建省德化县中国白陶瓷有限责任公司 | A kind of ivory white ceramic of high brightness and its manufacture craft |
| CN108249887B (en) * | 2018-03-22 | 2021-04-02 | 福建省德化县中国白陶瓷有限责任公司 | High-brightness ivory ceramic product and manufacturing process thereof |
| CN108821591A (en) * | 2018-07-30 | 2018-11-16 | 赵红刚 | A kind of jade white glaze material and preparation method thereof |
| CN112552019A (en) * | 2020-12-11 | 2021-03-26 | 江西省金海利陶瓷有限公司 | Formula of slip glaze for high-temperature firing of bone domestic porcelain |
| CN113149599A (en) * | 2021-03-17 | 2021-07-23 | 李玉桃 | High-strength light egg white enamel |
| CN113149599B (en) * | 2021-03-17 | 2022-10-25 | 福建省德化县鹏明陶瓷有限公司 | High-strength light egg white enamel |
| CN115286245A (en) * | 2022-07-26 | 2022-11-04 | 姚剑锋 | Hetian jade glaze and glazing method thereof |
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Application publication date: 20160323 |