CN105254275A - Ge kiln porcelain formula and manufacturing process - Google Patents

Ge kiln porcelain formula and manufacturing process Download PDF

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CN105254275A
CN105254275A CN201510776550.7A CN201510776550A CN105254275A CN 105254275 A CN105254275 A CN 105254275A CN 201510776550 A CN201510776550 A CN 201510776550A CN 105254275 A CN105254275 A CN 105254275A
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glaze
kiln
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王军港
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王军港
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Abstract

The invention relates to a ge kiln porcelain formula and a manufacturing process. The ge kiln porcelain formula comprises soil and glaze, wherein the soil is mainly composed of, by weight, 85 parts of Zijin clay and15 parts of aluminium oxide; the glaze is mainly composed of 30 parts of pine needle ash, 35 parts of quick lime, 10 parts of albite, 20 parts of white mud and 5 parts of Zijin clay. The ge kiln porcelain manufacturing process includes the four steps of sintering biscuit firing billets, preparing ceramic glaze, glazing and sintering. The ge kiln porcelain formula and the manufacturing process have the advantages that by the adoption of the technical scheme, the white line process of ge kiln porcelain in the Song dynasty can reappear, the continuously increasing requirements of consumers can be met, and the ge kiln porcelain formula and the manufacturing process have extremely high industrial and commercial value.

Description

A kind of brother's kiln porcelain formula and manufacturing process
Technical field
The invention belongs to porcelain field, be specifically related to a kind of brother's kiln porcelain formula and manufacturing process.
Background technology
Brother's kiln, with famous official, you, fixed, an ancient unit of weight be called Song dynasty five your name's kiln, the feature of brother's kiln porcelain is " tire is thin as a piece of paper, and glaze is thick in beautiful, and glaze paint is covered with line sheet, purple mouth iron foot, and tire look greyish black ".This series products is won victory with moulding, glaze colours and crackle glaze, is difficult to manual control because hacking, and crackle is not intended to and nature, is that the work of nature is brought up, more meets nature honesty, antique esthetic sentiment.Brother's kiln porcelain is distinguished from color and luster, the kind such as have bluish white, sallow, pale blue, ash green grass or young crops, putty, the depth cream-coloured.The most significant feature of brother's kiln porcelain is the rich exquisiteness of glaze colours, and gloss jade-like stone profit, as congealed fat; If put under microscope, the bubble contained in visible enamel is as poly-foam beading, splitting between solidifying greasy glaze paint, there have to be not of uniform size, or close circle or scattered ice crack shape reticulate pattern, the look pale yellow person of its reticulate pattern is as if spun gold, thin black person is as iron wire, and the two interweaves mutually, and thus by name is " spun gold ", " iron wire ".
But, due to of the remote past, brother's kiln porcelain formula and manufacturing process lost already, be meet the consumer demand that day by day increases, someone attempts recovering brother's kiln porcelain formula and manufacturing process in recent years, but effect is not fully up to expectations.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides a kind of brother's kiln porcelain formula and manufacturing process.Use described brother's kiln porcelain formula and manufacturing process can obtain " shallow white disconnected line " effect of Song dynasty brother kiln porcelain.
The technical solution adopted in the present invention is: a kind of brother's kiln porcelain formula, comprises ridging and glaze, wherein:
Ridging is made primarily of following raw material: Zijin soil, aluminum oxide;
Glaze is made primarily of following raw material: pine needle ash, unslaked lime, albite, white clay and Zijin soil.
Preferably, described brother's kiln porcelain formula, comprises ridging and glaze, wherein:
Described ridging is made primarily of the raw material of following weight part: Zijin soil 80-90 part, aluminum oxide 10-20 part;
Described glaze is made primarily of the raw material of following weight part: pine needle ash 25-35 part, unslaked lime 30-40 part, albite 7-13 part, white clay 15-25 part and Zijin soil 2-8 part.
Further, described brother's kiln porcelain formula, comprises ridging and glaze, wherein:
Described ridging is made primarily of the raw material of following weight part: Zijin soil 85 parts, 15 parts, aluminum oxide;
Described glaze is made primarily of following raw material: pine needle ash 30 parts, unslaked lime 35 parts, albite 10 parts, white clay 20 parts and 5 parts, Zijin soil.
It should be noted that, because when manufacturing china, needing to add water and mixing, but the water of the overwhelming majority can run off in sintering procedure, and in amount of water and final porcelain water content number belong to prior art completely, for sake of convenience, for all not writing the content of water exactly in above-mentioned formula.
Below, the raw material in the present invention is further elaborated:
Zijin soil is gained the name because of preparation Zijin glaze, and be a kind of iron content soil block stock, outward appearance is the colour of loess, reddle, dark red isochrome, and its component difference is comparatively large, and mineral composition complexity differs.Because its impure mineral are more, through pulverizing, must sieve before using, washing in a pan drift.General Zijin soil is after eluriating and removing slag, and be about 6%-7% containing ferric oxide, it is the pale blue preparing ashen glaze, plum green, Chinese ilex, Geware glaze and Zijin, and the raw material of the high temperature coloured glazes such as tea dust, is mainly distributed on the hillside in Thunder God Mountain, Jindezhen City and the suburbs.
Aluminum oxide, chemical formula Al 2o 3, in traditional glaze, aluminum oxide is commonly used for whitening agent.
Pine needle ash, the one of plant ash, is the ashes after being burned by pine needle, pulverizes and remove slag and get final product.
Unslaked lime, main component is calcium oxide, and usual method for making is be the natural rock of calcium carbonate by main component, at high temperature calcines, and namely decomposable asymmetric choice net generates carbonic acid gas and calcium oxide, and chemical formula: CaO, i.e. unslaked lime, also known as marble.
Albite, albite is the one of feldspar, is common spectra, is the aluminosilicate of sodium.Albite, mainly for the manufacture of pottery, soap, ceramic tile, floor tile, glass, grinding materials and grinding tool etc., pottery is mainly used in glaze.
White clay, also known as kaolin, is a kind of nonmetallic minerals, is a kind of based on the clay of kaolinite race clay mineral and tonstein.Gain the name because of Jing Dezhen, Jiangxi Province Gao Lingcun.The pure kaolin of matter is pure white exquisiteness, soft earthy, has the physico-chemical properties such as good plasticity-and resistivity against fire.Kaolin is mainly for the manufacture of pottery.
Proportioning raw materials in the present invention, be contriver on the basis that traditional lacquer is filled a prescription, creatively choose the raw materials such as pine needle ash, unslaked lime, and essence chooses fine-pointed finish to play the effect of reappearing Song dynasty brother kiln porcelain " shallow white disconnected line " in the proportioning of raw material.
Present invention also offers the above-mentioned brother's kiln porcelain formula taxi driver brother kiln porcelain manufacturing process of a kind of use, comprise the following steps:
A, fire biscuit: being added water by all raw materials of described ridging mixes, and makes base mud, and after described base mud shaping and drying, kiln-firing, makes biscuit;
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, adds water for ball milling, after sieving, namely obtain ceramic glaze;
C, glazing: imposed on by described ceramic glaze on described biscuit, form the uniform glaze layer of thickness after dry, obtain base substrate;
D, to fire: after the glaze layer on base substrate parches naturally, kiln-firing, fires rear kiln discharge and get product; Wherein sintering procedure passes through following several stage successively: the stage that is rapidly heated, slowly temperature rise period, persistently overheating stage, reduction phase, holding stage, chilling stage, slow cooling stage and rapid cooling stage.
Preferably, with ballstone in step B, preparation ceramic glaze: glaze: water weight ratio example is 2:1:1, carry out ball milling in loading ball-grinding machine, and cross 160-200 mesh sieve.During ball milling, the ratio of ballstone, glaze and water is through the result that contriver's multilayer is explored, and can ensure outstanding grinding quality, meanwhile, the particle diameter of ceramic glaze is conveniently follow-up glazing process, ensures the even of glaze layer.
Preferably, form the uniform glaze layer of thickness after dry in step C, glazing, the thickness of described glaze layer is 0.6-1.2mm.Whether suitable the thickness of glaze layer is is one of important factor in order in firing in the later stage, and contriver finds, in the scope of 0.6-1.2mm, the yield rate after firing is higher and closer to Song dynasty brother kiln porcelain.
Preferably, step D, fire middle start-stop temperature and be room temperature, the division points of wantonly one or two adjacent phases is followed successively by: arbitrary value in arbitrary value in arbitrary value in arbitrary value in arbitrary value in arbitrary value in arbitrary value in 400-500 DEG C, 650-750 DEG C, 900-1000 DEG C, 1200-1300 DEG C, 1200-1300 DEG C, 650-750 DEG C, 400-500 DEG C.
Further, step D, to fire: the heat-up rate in the stage that is rapidly heated is 40-50 DEG C/h, the heat-up rate of slow temperature rise period is 20-30 DEG C/h, the heat-up rate of persistently overheating stage and reduction phase is 30-40 DEG C/h, the time length of holding stage is 3-4 hour, the cooling rate in chilling stage is 100-140 DEG C/h, and the cooling rate in slow cooling stage is 80-90 DEG C/h, and the cooling rate in rapid cooling stage is 100-120 DEG C/h.Different heat-up rates or cooling rate are adopted to the different stages, that the different steps experienced in kiln according to base substrate determines, in the stage of being rapidly heated, absorption evaporation of water and organic burning are all carried out at this one-phase, and the speed of intensification can be relatively quicker; In the slow temperature rise period, quartz crystal transforms, the easy craze and transfiguration of base substrate, so heat-up rate needs slow; When persistently overheating stage and reduction phase, Main Function makes kiln internal gas pressure higher than the outer air pressure of kiln, allows kiln atmosphere become reducing atmosphere, therefore require that heat-up rate is comparatively slow, ensure the carrying out that the sufficient time is beneficial to reduction reaction; Keep temperature to ensure fully carrying out of reduction reaction at holding stage; Enter the chilling stage afterwards, quenching is ftractureed to impel glaze layer, to reach the effect of " crackle ".
Preferably, step D, fire: use blower to be blown into cold wind in kiln in the chilling stage, lower the temperature.Blower is used to be blown into cold wind, simple and fast, easy handling.
Further, step D, to fire: the heat-up rate in the stage that is rapidly heated is 45 DEG C/h, the heat-up rate of slow temperature rise period is 25 DEG C/h, the heat-up rate of persistently overheating stage and reduction phase is 35 DEG C/h, the time length of holding stage is 3.5 hours, the cooling rate in chilling stage is 120 DEG C/h, and the cooling rate in slow cooling stage is 85 DEG C/h, and the cooling rate in rapid cooling stage is 110 DEG C/h.
Beneficial effect of the present invention is:
The invention provides a kind of brother's kiln porcelain formula and manufacturing process, contriver on the basis of traditional lacquer formula and manufacturing process, through reasonably attempting and improving, the technical scheme found out, because the crackle on Song dynasty brother kiln porcelain surface is originally white line, adopt the technical scheme in the present invention, the white line technique of Song dynasty brother kiln porcelain can be reappeared, the consumer demand day by day increased can be met, there is high industry and commercial value.
Embodiment
Below in conjunction with embodiment, further illustrate content of the present invention.Should be appreciated that enforcement of the present invention is not limited to the following examples, any pro forma accommodation make the present invention and/or change all will fall into scope.
In the present invention, if not refer in particular to, all parts, per-cent are weight unit, and all equipment and raw material etc. all can be buied from market or the industry is conventional.Method in following embodiment, if no special instructions, is the ordinary method of this area.
Embodiment 1
Brother's kiln porcelain formula, comprises ridging and glaze, wherein:
Described ridging is made primarily of following raw material: Zijin soil 80kg, aluminum oxide 10kg;
Described glaze is made primarily of following raw material: pine needle ash 25kg, unslaked lime 30kg, albite 7kg, white clay 15kg and Zijin soil 2kg.
The present embodiment additionally provides the above-mentioned brother's kiln porcelain formula taxi driver brother kiln porcelain manufacturing process of a kind of use, comprises the following steps:
A, fire biscuit: being added water by all raw materials of described ridging mixes, and makes base mud, and after described base mud shaping and drying, kiln-firing, makes biscuit;
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, with ballstone: glaze: water weight ratio example is 2:1:1, load in ball-grinding machine and carry out ball milling, and cross 160 mesh sieves, after sieving, namely obtain ceramic glaze;
C, glazing: imposed on by described ceramic glaze on described biscuit, form the uniform glaze layer of thickness after dry, the thickness of described glaze layer is 0.6mm.Obtain base substrate;
D, to fire: after the glaze layer on base substrate parches naturally, kiln-firing, fires rear kiln discharge and get product; Wherein sintering procedure passes through following several stage successively: the stage that is rapidly heated, slowly temperature rise period, persistently overheating stage, reduction phase, holding stage, chilling stage, slow cooling stage and rapid cooling stage.Wherein, fire middle start-stop temperature and be room temperature, the division points of wantonly one or two adjacent phases is followed successively by: 400 DEG C, 650 DEG C, 900 DEG C, 1200 DEG C, 1200 DEG C, 650 DEG C, 400 DEG C; And, the heat-up rate in stage of being rapidly heated is 40 DEG C/h, the heat-up rate of slow temperature rise period is 20 DEG C/h, the heat-up rate of persistently overheating stage and reduction phase is 30 DEG C/h, and the time length of holding stage is 3 hours, and the cooling rate in chilling stage is 100 DEG C/h, the chilling stage uses blower to be blown into cold wind in kiln, lower the temperature, the cooling rate in slow cooling stage is 80 DEG C/h, and the cooling rate in rapid cooling stage is 100 DEG C/h.
Embodiment 2
Brother's kiln porcelain formula, comprises ridging and glaze, wherein:
Described ridging is made primarily of following raw material: Zijin soil 85kg, aluminum oxide 15kg;
Described glaze is made primarily of following raw material: pine needle ash 30kg, unslaked lime 35kg, albite 10kg, white clay 20kg and Zijin soil 5kg.
The present embodiment additionally provides the above-mentioned brother's kiln porcelain formula taxi driver brother kiln porcelain manufacturing process of a kind of use, comprises the following steps:
A, fire biscuit: being added water by all raw materials of described ridging mixes, and makes base mud, and after described base mud shaping and drying, kiln-firing, makes biscuit;
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, with ballstone: glaze: water weight ratio example is 2:1:1, load in ball-grinding machine and carry out ball milling, and cross 180 mesh sieves, after sieving, namely obtain ceramic glaze;
C, glazing: imposed on by described ceramic glaze on described biscuit, form the uniform glaze layer of thickness after dry, the thickness of described glaze layer is 0.9mm.Obtain base substrate;
D, to fire: after the glaze layer on base substrate parches naturally, kiln-firing, fires rear kiln discharge and get product; Wherein sintering procedure passes through following several stage successively: the stage that is rapidly heated, slowly temperature rise period, persistently overheating stage, reduction phase, holding stage, chilling stage, slow cooling stage and rapid cooling stage.Wherein, fire middle start-stop temperature and be room temperature, the division points of wantonly one or two adjacent phases is followed successively by: 450 DEG C, 700 DEG C, 950 DEG C, 1250 DEG C, 1250 DEG C, 700 DEG C, 450 DEG C; And, the heat-up rate in stage of being rapidly heated is 45 DEG C/h, the heat-up rate of slow temperature rise period is 25 DEG C/h, the heat-up rate of persistently overheating stage and reduction phase is 35 DEG C/h, and the time length of holding stage is 3.5 hours, and the cooling rate in chilling stage is 120 DEG C/h, the chilling stage uses blower to be blown into cold wind in kiln, lower the temperature, the cooling rate in slow cooling stage is 85 DEG C/h, and the cooling rate in rapid cooling stage is 110 DEG C/h.
Embodiment 3
Brother's kiln porcelain formula, comprises ridging and glaze, wherein:
Described ridging is made primarily of following raw material: Zijin soil 90kg, aluminum oxide 20kg;
Described glaze is made primarily of following raw material: pine needle ash 35kg, unslaked lime 40kg, albite 13kg, white clay 25kg and Zijin soil 8kg.
The present embodiment additionally provides the above-mentioned brother's kiln porcelain formula taxi driver brother kiln porcelain manufacturing process of a kind of use, comprises the following steps:
A, fire biscuit: being added water by all raw materials of described ridging mixes, and makes base mud, and after described base mud shaping and drying, kiln-firing, makes biscuit;
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, with ballstone: glaze: water weight ratio example is 2:1:1, load in ball-grinding machine and carry out ball milling, and cross 200 mesh sieves, after sieving, namely obtain ceramic glaze;
C, glazing: imposed on by described ceramic glaze on described biscuit, form the uniform glaze layer of thickness after dry, the thickness of described glaze layer is 1.2mm.Obtain base substrate;
D, to fire: after the glaze layer on base substrate parches naturally, kiln-firing, fires rear kiln discharge and get product; Wherein sintering procedure passes through following several stage successively: the stage that is rapidly heated, slowly temperature rise period, persistently overheating stage, reduction phase, holding stage, chilling stage, slow cooling stage and rapid cooling stage.Wherein, fire middle start-stop temperature and be room temperature, the division points of wantonly one or two adjacent phases is followed successively by: 500 DEG C, 750 DEG C, 1000 DEG C, 1300 DEG C, 1300 DEG C, 750 DEG C, 500 DEG C; And, the heat-up rate in stage of being rapidly heated is 50 DEG C/h, the heat-up rate of slow temperature rise period is 30 DEG C/h, the heat-up rate of persistently overheating stage and reduction phase is 40 DEG C/h, and the time length of holding stage is 4 hours, and the cooling rate in chilling stage is 140 DEG C/h, the chilling stage uses blower to be blown into cold wind in kiln, lower the temperature, the cooling rate in slow cooling stage is 90 DEG C/h, and the cooling rate in rapid cooling stage is 120 DEG C/h.
It should be noted last that; above embodiment is only in order to illustrate technical scheme of the present invention and unrestricted; although with reference to preferred embodiment to invention has been detailed description; be understood that; the foregoing is only the specific embodiment of the present invention, the protection domain be not intended to limit the present invention, within the spirit and principles in the present invention all; any amendment of making, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (10)

1. brother's kiln porcelain formula, is characterized in that, comprise ridging and glaze, wherein:
Ridging is made primarily of following raw material: Zijin soil, aluminum oxide;
Glaze is made primarily of following raw material: pine needle ash, unslaked lime, albite, white clay and Zijin soil.
2. brother's kiln porcelain formula according to claim 1, is characterized in that,
Described ridging is made primarily of the raw material of following weight part: Zijin soil 80-90 part, aluminum oxide 10-20 part;
Described glaze is made primarily of the raw material of following weight part: pine needle ash 25-35 part, unslaked lime 30-40 part, albite 7-13 part, white clay 15-25 part and Zijin soil 2-8 part.
3. brother's kiln porcelain formula according to claim 1, is characterized in that,
Described ridging is made primarily of the raw material of following weight part: Zijin soil 85 parts, 15 parts, aluminum oxide;
Described glaze is made primarily of the raw material of following weight part: pine needle ash 30 parts, unslaked lime 35 parts, albite 10 parts, white clay 20 parts and 5 parts, Zijin soil.
4., according to the arbitrary described brother's kiln porcelain formula taxi driver brother kiln porcelain manufacturing process of claim 1-3, it is characterized in that, comprise the following steps:
A, fire biscuit: being added water by all raw materials of described ridging mixes, and makes base mud, and after described base mud shaping and drying, kiln-firing, makes biscuit;
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, adds water for ball milling, after sieving, namely obtain ceramic glaze;
C, glazing: imposed on by described ceramic glaze on described biscuit, form the uniform glaze layer of thickness after dry, obtain base substrate;
D, to fire: after the glaze layer on base substrate parches naturally, kiln-firing, fires rear kiln discharge and get product; Wherein sintering procedure passes through following several stage successively: the stage that is rapidly heated, slowly temperature rise period, persistently overheating stage, reduction phase, holding stage, chilling stage, slow cooling stage and rapid cooling stage.
5. brother's kiln porcelain manufacturing process according to claim 4, is characterized in that, with ballstone in step B, preparation ceramic glaze: glaze: water weight ratio example is 2:1:1, loads in ball-grinding machine and carry out ball milling, and crosses 160-200 mesh sieve.
6. brother's kiln porcelain manufacturing process according to claim 4, is characterized in that, form the uniform glaze layer of thickness after dry in step C, glazing, the thickness of described glaze layer is 0.6-1.2mm.
7. brother's kiln porcelain manufacturing process according to claim 4, it is characterized in that, step D, fire middle start-stop temperature and be room temperature, the division points of wantonly one or two adjacent phases is followed successively by: arbitrary value in arbitrary value in arbitrary value in arbitrary value in arbitrary value in arbitrary value in arbitrary value in 400-500 DEG C, 650-750 DEG C, 900-1000 DEG C, 1200-1300 DEG C, 1200-1300 DEG C, 650-750 DEG C, 400-500 DEG C.
8. brother's kiln porcelain manufacturing process according to claim 7, it is characterized in that, step D, to fire: the heat-up rate in the stage that is rapidly heated is 40-50 DEG C/h, the heat-up rate of slow temperature rise period is 20-30 DEG C/h, the heat-up rate of persistently overheating stage and reduction phase is 30-40 DEG C/h, the time length of holding stage is 3-4 hour, the cooling rate in chilling stage is 100-140 DEG C/h, the cooling rate in slow cooling stage is 80-90 DEG C/h, and the cooling rate in rapid cooling stage is 100-120 DEG C/h.
9. brother's kiln porcelain manufacturing process according to claim 8, is characterized in that, step D, fires: use blower to be blown into cold wind in kiln in the chilling stage, lower the temperature.
10. brother's kiln porcelain manufacturing process according to claim 8, it is characterized in that, step D, to fire: the heat-up rate in the stage that is rapidly heated is 45 DEG C/h, the heat-up rate of slow temperature rise period is 25 DEG C/h, the heat-up rate of persistently overheating stage and reduction phase is 35 DEG C/h, and the time length of holding stage is 3.5 hours, and the cooling rate in chilling stage is 120 DEG C/h, the cooling rate in slow cooling stage is 85 DEG C/h, and the cooling rate in rapid cooling stage is 110 DEG C/h.
CN201510776550.7A 2015-11-13 2015-11-13 A kind of brother's kiln porcelain and manufacturing process Active CN105254275B (en)

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CN106316129A (en) * 2016-08-18 2017-01-11 云南坤尚科技有限公司 Manufacturing process of ceramic base glaze
CN108751708A (en) * 2018-06-04 2018-11-06 浙江上木木陶瓷文化有限公司 The pure matting glaze of high temperature more kiln, using the matting glaze kiln secret colour ware and its method for cooking
CN109020219A (en) * 2018-10-09 2018-12-18 汝州市宣和坊汝瓷有限公司 A kind of Ruyao tea-dust glaze and preparation method thereof
CN109437836A (en) * 2018-12-24 2019-03-08 王晶 A kind of celadon pen and its preparation process

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106316129A (en) * 2016-08-18 2017-01-11 云南坤尚科技有限公司 Manufacturing process of ceramic base glaze
CN106316129B (en) * 2016-08-18 2019-02-22 云南坤尚科技有限公司 A kind of manufacture craft of the basic glaze of ceramics
CN108751708A (en) * 2018-06-04 2018-11-06 浙江上木木陶瓷文化有限公司 The pure matting glaze of high temperature more kiln, using the matting glaze kiln secret colour ware and its method for cooking
CN109020219A (en) * 2018-10-09 2018-12-18 汝州市宣和坊汝瓷有限公司 A kind of Ruyao tea-dust glaze and preparation method thereof
CN109437836A (en) * 2018-12-24 2019-03-08 王晶 A kind of celadon pen and its preparation process

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