CN107417107A - A kind of blue glaze modelled after an antique and preparation method thereof - Google Patents
A kind of blue glaze modelled after an antique and preparation method thereof Download PDFInfo
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- CN107417107A CN107417107A CN201710381618.0A CN201710381618A CN107417107A CN 107417107 A CN107417107 A CN 107417107A CN 201710381618 A CN201710381618 A CN 201710381618A CN 107417107 A CN107417107 A CN 107417107A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Dispersion Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of blue glaze modelled after an antique and preparation method thereof, blue glaze modelled after an antique includes ground-coat enamel and cover-coat enamel, and the ground-coat enamel is prepared by following parts by weight：37 parts 30 36 parts of melilite, 26 34 parts of this medicine, 8 16 parts of calcite, 12 16 parts of quartz, 0.7 1.3 parts of iron oxide red, 0.8 1.2 parts of bovine bone powder, 35 parts of talcum of burning, 24 parts of zinc oxide, tin oxide 1.5 2.5 of Fen, Celadon alkali；The cover-coat enamel is prepared by following parts by weight：36 44 parts of melilite, 13 19 parts of quartz, 11 15 parts of calcite, 46 parts of blue or green alkali, 13 17 parts of frit, 0.8 1.2 parts of ox bone, 2.5 3.5 parts of tin oxide, 3.5 4.5 parts of zinc oxide, 23 parts of talcum, 0.4 0.6 parts of cupric oxide.Obtained blue glaze modelled after an antique has Song Jun glaze colours and red speckle, and glaze colours jade-like stone profit, and crackle is few, and resistance to mechanical ability is strong.
Description
Technical field
The present invention relates to pottery manufacturing technology field, and in particular to a kind of blue glaze modelled after an antique.
Background technology
Pottery is using glaze thickness as this, and in its color or heavy glaze bottom or outstanding glaze or floating glaze table, the thick muddy work of glaze, glaze layer opalescence jade-like stone moisten,
Work of being administrations with multiplied departments is intended to drip, and third dimension is extremely strong.Traditional blue glaze in pottery, using natural earthy cobalt as colouring agent, except containing cobalt oxide
Outside, also containing iron oxide and manganese oxide.Blue glaze is seen in tri-coloured glazed pottery earliest.But at this moment or low temperature orchid glaze, only beautiful sense,
Lack calm tone.The appearance of high temperature orchid glaze is in the Yuan Dynasty.Enter it is bright after, particularly at Xuande, blue glaze implements are more and matter is beautiful,
Pushed away as the top grade of Xuande porcelain.During to clear Kangxu, more occur spilling a variety of new varieties such as blue glaze, sky blue.
In the prior art, formula of pottery orchid glaze and preparation method thereof is also seldom, and obtained pottery orchid glaze surface has and split
Line, glaze paint wearability and resistance to mechanical ability are poor, and color is single.
The content of the invention
Lacked the invention provides a kind of blue glaze modelled after an antique and preparation method thereof with solving existing formula and preparation method thereof, imitated
Ancient blue glaze surface has crackle, glaze paint wearability and resistance to mechanical ability poor and the problem of color is single.
The purpose of the present invention is realized with following technical proposals：
A kind of blue glaze modelled after an antique, including ground-coat enamel and cover-coat enamel, the ground-coat enamel are prepared by the raw material of following parts by weight：Melilite
30-36 parts, this medicine 26-34 parts, calcite 8-16 parts, quartzy 12-16 parts, iron oxide red 0.7-1.3 parts, bovine bone powder 0.8-1.2 parts,
Burn talcum 3-5 parts, zinc oxide 2-4 parts, tin oxide 1.5-2.5 Fen, Celadon alkali 3-7 parts；The cover-coat enamel by following parts by weight raw material
It is prepared：Melilite 36-44 parts, quartzy 13-19 parts, calcite 11-15 parts, blue or green alkali 4-6 parts, frit 13-17 parts, ox bone
0.8-1.2 parts, tin oxide 2.5-3.5 parts, zinc oxide 3.5-4.5 parts, talcum 2-3 parts, cupric oxide 0.4-0.6 parts.
Preferably, the ground-coat enamel is prepared by the raw material of following parts by weight：33 parts of melilite, 30 parts of this medicine, calcite
12 parts, quartz 14 parts, 1 part of iron oxide red, 1 part of bovine bone powder, burn 4 parts of talcum, 3 parts of zinc oxide, 5 parts of the Fen, Celadon alkali of tin oxide 2.
Preferably, the cover-coat enamel is prepared by the raw material of following parts by weight：40 parts of melilite, quartzy 16 parts, calcite
13 parts, 5 parts of blue or green alkali, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.
The preparation method of described blue glaze modelled after an antique comprises the following steps：
(1) add water to mix above-mentioned raw materials, ball milling, obtain glaze slip；
(2) ground-coat enamel is applied；
(3) cover-coat enamel is applied；
(4) burn till, firing temperature is 1280-1300 DEG C.
Preferably, firing process specifically comprises the following steps in the preparation method step (4) of described blue glaze modelled after an antique：
1. the heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, makes temperature uniform in 2.5-3.5h
Rise to 1000-1080 DEG C；
2. under reducing atmosphere, temperature is set to be ramped up 1280-1300 DEG C in 11-13h；
3. 2.5-3h under reducing atmosphere, is kept under the conditions of 1280-1300 DEG C；
4. being cooled to room temperature, it is made.
The present invention has following beneficial effect：By testing for many years, obtained blue glaze modelled after an antique has Song Jun glaze colours and red
Speckle, color is no longer dull, and glaze colours jade-like stone profit, crackle is few, and resistance to mechanical ability is strong.It is in using blue glaze modelled after an antique made from the technique
Reveal blue or green blueing color translucent as jade, color and luster is gentle, simple and elegant, elegant, simple and easy, so as to produce a kind of brand-new regard
Feel impact and artistic effect, improve the artistry, added value, occupation rate of market and impulsive force of this product.
Brief description of the drawings
Fig. 1 is the blue glaze uranium face figure modelled after an antique that the embodiment of the present invention 2 is prepared.
Embodiment
Embodiment 1
A kind of blue glaze modelled after an antique, including ground-coat enamel and cover-coat enamel, the ground-coat enamel are prepared by the raw material of following parts by weight：Melilite
30-36 parts, this medicine 26-34 parts, calcite 8-16 parts, quartzy 12-16 parts, iron oxide red 0.7-1.3 parts, bovine bone powder 0.8-1.2 parts, burning
Talcum 3-5 parts, zinc oxide 2-4 parts, tin oxide 1.5-2.5 Fen, Celadon alkali 3-7 parts；The cover-coat enamel by following parts by weight raw material system
It is standby to form：Melilite 36-44 parts, quartzy 13-19 parts, calcite 11-15 parts, blue or green alkali 4-6 parts, frit 13-17 parts, ox bone 0.8-
1.2 parts, tin oxide 2.5-3.5 parts, zinc oxide 3.5-4.5 parts, talcum 2-3 parts, cupric oxide 0.4-0.6 parts.
The preparation method of above-mentioned blue glaze modelled after an antique comprises the following steps：
The preparation method of described blue glaze modelled after an antique comprises the following steps：
(1) add water to mix above-mentioned raw materials, ball milling, obtain glaze slip；
(2) ground-coat enamel is applied；
(3) cover-coat enamel is applied in a manner of glaze spraying；
(4) burn till, firing temperature is 1280-1300 DEG C.
Firing process specifically comprises the following steps in step (4)：
1. the heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, makes temperature uniform in 2.5-3.5h
Rise to 1000-1080 DEG C；
2. under reducing atmosphere, temperature is set to be ramped up 1280-1300 DEG C in 11-13h；
3. 2.5-3h under reducing atmosphere, is kept under the conditions of 1280-1300 DEG C；
4. being cooled to room temperature, it is made.
Using melilite and this medicine as primary solvent in ground-coat enamel of the present invention, melilite dioxide-containing silica is 77% or so, oxygen
Change aluminium 13% or so, iron oxide 0.6%, magnesia 0.16%；This medicine be Yuzhou a kind of natural feldspar, iron-holder compared with
It is high；Calcite plays hydrotropy, and quartz can improve the mobility of glaze, the main calcic of bovine bone powder and phosphorus, can improve the milkiness of glaze
Degree, texture being improved, blue or green alkali is a kind of trona stone of Yuzhou, belongs to kaolinite class clay mineral, and silicon, aluminium content are higher,
Outward appearance is in cyan, can reduce firing temperature, promotes to melt other raw mineral materials, beneficial to and cover-coat enamel combination, tin oxide, oxidation
It is material after talcum high-temperature calcination that zinc, which is assistant toner, burns talcum, and impurity is few, can combine tire glaze preferable.Iron oxide red plays colour generation
Colouring agent effect.
Using melilite as primary solvent in cover-coat enamel, melilite is compared to for example white feldspar of other feldspars, red feldspar, silicon, iron content
It is higher, the glossiness on chun glaze surface can be improved, calcite plays hydrotropy, and quartz can improve the mobility of glaze, add in cover-coat enamel
Add blue or green alkali can equally promote glaze melting be beneficial to and ground-coat enamel combination；Frit is cosolvent, preferably main with zinc frit, bovine bone powder
Calcic and phosphorus, the opacity of glaze can be improved, talcum is natural hydrous magnesium silicate mineral, is the cosolvent of glaze, by increasing capacitance it is possible to increase an ancient unit of weight
The opaque of glaze；Cosolvent and assistant toner of the zinc oxide during high-temperature firing as glaze, reduce the firing temperature of glaze, have
Help the color development of glaze and cause glaze paint rich in change, while the opaque effect of glaze colours can be increased, tin oxide is assistant toner；Oxidation
Copper is photoghraphic coupler；The present invention applies red glaze on the basis of the ground-coat enamel in blue, and both combine preferably, obtained modelled after an antique after firing
Blue glaze has Song Jun glaze colours and red speckle, has very high artistic value.
Embodiment 2
A kind of blue glaze modelled after an antique, ground-coat enamel are prepared by the raw material of following parts by weight：33 parts of melilite, 30 parts of this medicine, Fang Xie
5 parts 12 parts of stone, 14 parts of quartz, 1 part of iron oxide red, 1 part of bovine bone powder, 4 parts of talcum of burning, 3 parts of zinc oxide, tin oxide 2 of Fen, Celadon alkali.Cover-coat enamel
It is prepared by the raw material of following parts by weight：40 parts of melilite, quartz 16 parts, 13 parts of calcite, 5 parts of blue or green alkali, 15 parts of frit,
1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.
The preparation method of above-mentioned blue glaze modelled after an antique comprises the following steps：
(1) add water to mix above-mentioned raw materials, ball milling, cross 250 mesh sieves, obtain glaze slip；
(2) ground-coat enamel is applied；
(3) cover-coat enamel is applied；
(4) burn till, specifically comprise the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, under oxidizing atmosphere
Fire, temperature is ramped up 1050 DEG C in 3.5h；2. temperature under reducing atmosphere, is set to be ramped up 1290 DEG C in 12h；3.
Under reducing atmosphere, 3h is kept under the conditions of 1290 DEG C；4. being cooled to room temperature, it is made.
The blue glaze modelled after an antique obtained using said ratio and method is as shown in figure 1, by rational proportion and control sintering process
In atmosphere, time and temperature, the blue glaze glaze colours jade-like stone profit modelled after an antique prepared, color and luster is gentle, simple and elegant, simple and easy, and crackle is few.Into
Product blue glaze modelled after an antique has natural flammulation, adds its ornamental value.
Comparative example 1
A kind of blue glaze modelled after an antique, ground-coat enamel are prepared by the raw material of following parts by weight：33 parts of melilite, 30 parts of this medicine, Fang Xie
12 parts of stone, 14 parts of quartz, burn 5 parts 4 parts of talcum, 3 parts of zinc oxide, tin oxide 2 of Fen, Celadon alkali.Cover-coat enamel by following parts by weight raw material
It is prepared：40 parts of melilite, quartz 16 parts, 13 parts of calcite, 5 parts of blue or green alkali, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide,
4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.Preparation method is the same as the preparation method in embodiment 2.This example and the phase of embodiment 2
Compare, iron oxide red is not used in ground-coat enamel raw material and bovine bone powder, the flammulation color that the blue glaze modelled after an antique being fired into is showed be not fresh
It is gorgeous, and firing glaze paint texture is poor, yield rate only has 55% or so.
Comparative example 2
A kind of blue glaze modelled after an antique, ground-coat enamel are prepared by the raw material of following parts by weight：33 parts of melilite, 30 parts of this medicine, Fang Xie
5 parts 12 parts of stone, 14 parts of quartz, 1 part of iron oxide red, 1 part of bovine bone powder, 4 parts of talcum of burning, zinc oxide 3 of Fen, Celadon alkali.Cover-coat enamel is by following weight
The raw material of part is prepared：40 parts of melilite, 16 parts of quartz, 13 parts of calcite, 5 parts of blue or green alkali, 15 parts of frit, 1 part of ox bone, oxygen
Change 3 parts of tin, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.Preparation method is the same as embodiment 2.This example is compared with Example 2
Compared with unused tin oxide, the blue glaze color and luster yellowing modelled after an antique being fired into, yield rate only have 65% in ground-coat enamel raw material.
Comparative example 3
A kind of blue glaze modelled after an antique, ground-coat enamel are prepared by the raw material of following parts by weight：45 parts of melilite, 30 parts of this medicine, Fang Xie
5 parts 12 parts of stone, 6 parts of quartz, 1 part of iron oxide red, 1 part of bovine bone powder, 4 parts of talcum of burning, 3 parts of zinc oxide, tin oxide 2 of Fen, Celadon alkali.Cover-coat enamel by
The raw material of following parts by weight is prepared：40 parts of melilite, 16 parts of quartz, 13 parts of calcite, 5 parts of blue or green alkali, 15 parts of frit, ox
1 part of bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.Preparation method is the same as embodiment 2.This example is with implementing
Example 2 compares, and the parts by weight of melilite in ground-coat enamel raw material is increased to 45 parts, quartzy parts by weight are reduced to 3 parts, this example and reality
Apply example 2 and compare and pinprick is more readily formed in sintering procedure, yield rate only has 58%.
The ground-coat enamel formula for the blue glaze modelled after an antique that 3-25 of the embodiment of the present invention is provided is shown in Table 1-4, and the cover-coat enamel formula of blue glaze modelled after an antique is shown in
Table 5-8, its preparation method are same as Example 2.
Table 1
Table 2
Table 3
Table 4
Table 5
Table 6
Table 7
Table 8
Claims (5)
1. a kind of blue glaze modelled after an antique, including ground-coat enamel and cover-coat enamel, it is characterised in that：The ground-coat enamel by following parts by weight raw material prepare and
Into：Melilite 30-36 parts, this medicine 26-34 parts, calcite 8-16 parts, quartzy 12-16 parts, iron oxide red 0.7-1.3 parts, bovine bone powder
0.8-1.2 parts, burn talcum 3-5 parts, zinc oxide 2-4 parts, tin oxide 1.5-2.5 Fen, Celadon alkali 3-7 parts；The cover-coat enamel is by following heavy
The raw material of amount part is prepared：Melilite 36-44 parts, quartzy 13-19 parts, calcite 11-15 parts, blue or green alkali 4-6 parts, frit 13-
17 parts, ox bone 0.8-1.2 parts, tin oxide 2.5-3.5 parts, zinc oxide 3.5-4.5 parts, talcum 2-3 parts, cupric oxide 0.4-0.6 parts.
2. blue glaze modelled after an antique according to claim 1, it is characterised in that：The ground-coat enamel by following parts by weight raw material prepare and
Into：33 parts of melilite, 30 parts of this medicine, 12 parts of calcite, 14 parts of quartz, 1 part of iron oxide red, 1 part of bovine bone powder, 4 parts of talcum of burning, zinc oxide
5 parts 3 parts, tin oxide 2 of Fen, Celadon alkali.
3. blue glaze modelled after an antique according to claim 1, it is characterised in that：The cover-coat enamel by following parts by weight raw material prepare and
Into：40 parts of melilite, 16 parts of quartz, 13 parts of calcite, 5 parts of blue or green alkali, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, zinc oxide 4
Part, 2.5 parts of talcum, 0.5 part of cupric oxide.
4. the preparation method of a kind of blue glaze modelled after an antique as described in claim 1,2 or 3, it is characterised in that comprise the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Apply ground-coat enamel；
（3）Apply cover-coat enamel；
（4）Burn till, firing temperature is 1280-1300 DEG C.
5. the preparation method of blue glaze modelled after an antique as claimed in claim 4, it is characterised in that step（4）Middle firing process specifically includes
Following steps：
1. the heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is ramped up in 2.5-3.5h
1000-1080℃；
2. under reducing atmosphere, temperature is set to be ramped up 1280-1300 DEG C in 11-13h；
3. 2.5-3h under reducing atmosphere, is kept under the conditions of 1280-1300 DEG C；
4. being cooled to room temperature, it is made.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109081582A (en) * | 2018-09-14 | 2018-12-25 | 张自军 | A kind of orchid chun glaze pottery and preparation method thereof |
| CN109369152A (en) * | 2018-12-12 | 2019-02-22 | 福建省德化业美陶瓷有限公司 | A kind of high intensity is resistance to fall sky blue glaze ceramic and preparation method thereof |
| CN109384478A (en) * | 2018-12-19 | 2019-02-26 | 禹州市正玉钧窑有限公司 | A kind of red glaze of band spot an ancient unit of weight |
| CN113121114A (en) * | 2020-06-18 | 2021-07-16 | 季友泉 | Longquan kiln snow melting glaze and manufacturing method thereof |
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| CN104909838A (en) * | 2015-06-12 | 2015-09-16 | 佛山科学技术学院 | Guangdong Jun Blue glaze prepared from commonly used raw materials in ceramics factory and preparation method of Guangdong Jun Blue glaze |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109081582A (en) * | 2018-09-14 | 2018-12-25 | 张自军 | A kind of orchid chun glaze pottery and preparation method thereof |
| CN109369152A (en) * | 2018-12-12 | 2019-02-22 | 福建省德化业美陶瓷有限公司 | A kind of high intensity is resistance to fall sky blue glaze ceramic and preparation method thereof |
| CN109384478A (en) * | 2018-12-19 | 2019-02-26 | 禹州市正玉钧窑有限公司 | A kind of red glaze of band spot an ancient unit of weight |
| CN113121114A (en) * | 2020-06-18 | 2021-07-16 | 季友泉 | Longquan kiln snow melting glaze and manufacturing method thereof |
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