CN104833734A - 食品包装材料中邻苯二甲酸酯类物质迁移量的检测方法 - Google Patents
食品包装材料中邻苯二甲酸酯类物质迁移量的检测方法 Download PDFInfo
- Publication number
- CN104833734A CN104833734A CN201510143016.2A CN201510143016A CN104833734A CN 104833734 A CN104833734 A CN 104833734A CN 201510143016 A CN201510143016 A CN 201510143016A CN 104833734 A CN104833734 A CN 104833734A
- Authority
- CN
- China
- Prior art keywords
- food
- phthalate
- phthalic acid
- food sample
- acetonitrile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
Description
通道 | 时间(tR/min) | 选择离子(m/z) |
1 | 10.5 | 77,135,163,194 |
2 | 12.4 | 149,177,121,222 |
3 | 14.5 | 149,167,209, |
4 | 16.2 | 104,132,149,189 |
5 | 17.7 | 76,149,191,209 |
6 | 19.1 | 149,167,205,223 |
7 | 21.5 | 121,149,223,205 |
8 | 23.2 | 59,104,149,207 |
9 | 24.7 | 69,85,104,149,167,251 |
10 | 26.4 | 72,149,176,193 |
11 | 27.4 | 104,149,219,237 |
12 | 30.1 | 76,91,149,104,206,251 |
13 | 33.7 | 85,101,149,193 |
14 | 35.4 | 104,149,167,247,249,265,279 |
15 | 36.4 | 77,104,153,225 |
16 | 38.7 | 149,167,261,279 |
17 | 40.9 | 85,127,141,149,167,261,279,293,307 |
相对离子丰度 | >50% | >20%至50% | >10%至20% | ≤10% |
允许的相对偏差 | ±10% | ±15% | ±20% | ±50% |
相对离子丰度 | >50% | >20%至50% | >10%至20% | ≤10% |
允许的相对偏差 | ±20% | ±25% | ±30% | ±50% |
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510143016.2A CN104833734A (zh) | 2015-03-30 | 2015-03-30 | 食品包装材料中邻苯二甲酸酯类物质迁移量的检测方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510143016.2A CN104833734A (zh) | 2015-03-30 | 2015-03-30 | 食品包装材料中邻苯二甲酸酯类物质迁移量的检测方法 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN104833734A true CN104833734A (zh) | 2015-08-12 |
Family
ID=53811748
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510143016.2A Pending CN104833734A (zh) | 2015-03-30 | 2015-03-30 | 食品包装材料中邻苯二甲酸酯类物质迁移量的检测方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN104833734A (zh) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105203373A (zh) * | 2015-09-10 | 2015-12-30 | 上海安谱实验科技股份有限公司 | 一种简单快速高效稳定测定食品中苯并芘的方法 |
CN105911172A (zh) * | 2016-04-14 | 2016-08-31 | 北京工商大学 | 一种快速检测高粱中塑化剂的方法 |
CN107655991A (zh) * | 2017-09-21 | 2018-02-02 | 国家烟草质量监督检验中心 | 土壤中6种邻苯二甲酸酯的测定方法 |
CN107703236A (zh) * | 2017-09-26 | 2018-02-16 | 广东工业大学 | 一种土壤中邻苯二甲酸酯的提取检测方法 |
CN108709947A (zh) * | 2018-07-10 | 2018-10-26 | 中国检验检疫科学研究院 | 食品接触材料中邻苯二甲酸酯类增塑剂迁移量的测定方法 |
CN109633020A (zh) * | 2018-12-29 | 2019-04-16 | 上海微谱化工技术服务有限公司 | 一种盐酸阿芬太尼中添加剂的检测方法 |
CN113030299A (zh) * | 2021-02-22 | 2021-06-25 | 广州海关技术中心 | 食品接触用再生pet制品中非有意或有意添加物迁移量的筛查及安全评估方法 |
CN113655148A (zh) * | 2021-08-31 | 2021-11-16 | 南京西默思博检测技术有限公司 | 一种测定异丙托溴铵吸入剂中邻苯二甲酸二丁酯和邻苯二甲酸二异丁酯的方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101493440A (zh) * | 2008-08-06 | 2009-07-29 | 通标标准技术服务(天津)有限公司 | 脂肪食品接触材料中邻苯二甲酸酯和己二酸二乙基己酯的迁移量的测定方法 |
CN101551363A (zh) * | 2009-05-14 | 2009-10-07 | 江南大学 | 一种同时检测牛奶中多种酞酸酯的液质联用测定方法 |
CN101858897A (zh) * | 2010-07-05 | 2010-10-13 | 深圳出入境检验检疫局玩具检测技术中心 | 邻苯二甲酸酯类增塑剂的检测方法 |
CN102998381A (zh) * | 2012-10-17 | 2013-03-27 | 国家烟草质量监督检验中心 | 一种烟用接装纸中邻苯二甲酸酯含量的测定方法 |
CN103808814A (zh) * | 2012-11-13 | 2014-05-21 | 云南健牛生物科技有限公司 | 一种检测食品中邻苯二甲酸酯的方法 |
-
2015
- 2015-03-30 CN CN201510143016.2A patent/CN104833734A/zh active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101493440A (zh) * | 2008-08-06 | 2009-07-29 | 通标标准技术服务(天津)有限公司 | 脂肪食品接触材料中邻苯二甲酸酯和己二酸二乙基己酯的迁移量的测定方法 |
CN101551363A (zh) * | 2009-05-14 | 2009-10-07 | 江南大学 | 一种同时检测牛奶中多种酞酸酯的液质联用测定方法 |
CN101858897A (zh) * | 2010-07-05 | 2010-10-13 | 深圳出入境检验检疫局玩具检测技术中心 | 邻苯二甲酸酯类增塑剂的检测方法 |
CN102998381A (zh) * | 2012-10-17 | 2013-03-27 | 国家烟草质量监督检验中心 | 一种烟用接装纸中邻苯二甲酸酯含量的测定方法 |
CN103808814A (zh) * | 2012-11-13 | 2014-05-21 | 云南健牛生物科技有限公司 | 一种检测食品中邻苯二甲酸酯的方法 |
Non-Patent Citations (2)
Title |
---|
中华人民共和国国家质量监督检验检疫总局: "《SN/T 3147-2012 出口食品中邻苯二甲酸酯的测定》", 7 May 2012 * |
尹鹏: "邻苯二甲酸酯类化合物在茶叶上的污染水平及其迁移规律的研究", 《中国优秀硕士学位论文全文数据库》 * |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105203373A (zh) * | 2015-09-10 | 2015-12-30 | 上海安谱实验科技股份有限公司 | 一种简单快速高效稳定测定食品中苯并芘的方法 |
CN105911172A (zh) * | 2016-04-14 | 2016-08-31 | 北京工商大学 | 一种快速检测高粱中塑化剂的方法 |
CN105911172B (zh) * | 2016-04-14 | 2018-06-26 | 北京工商大学 | 一种快速检测高粱中塑化剂的方法 |
CN107655991A (zh) * | 2017-09-21 | 2018-02-02 | 国家烟草质量监督检验中心 | 土壤中6种邻苯二甲酸酯的测定方法 |
CN107703236A (zh) * | 2017-09-26 | 2018-02-16 | 广东工业大学 | 一种土壤中邻苯二甲酸酯的提取检测方法 |
CN108709947A (zh) * | 2018-07-10 | 2018-10-26 | 中国检验检疫科学研究院 | 食品接触材料中邻苯二甲酸酯类增塑剂迁移量的测定方法 |
CN109633020A (zh) * | 2018-12-29 | 2019-04-16 | 上海微谱化工技术服务有限公司 | 一种盐酸阿芬太尼中添加剂的检测方法 |
CN109633020B (zh) * | 2018-12-29 | 2022-07-01 | 上海微谱化工技术服务有限公司 | 一种盐酸阿芬太尼中添加剂的检测方法 |
CN113030299A (zh) * | 2021-02-22 | 2021-06-25 | 广州海关技术中心 | 食品接触用再生pet制品中非有意或有意添加物迁移量的筛查及安全评估方法 |
CN113655148A (zh) * | 2021-08-31 | 2021-11-16 | 南京西默思博检测技术有限公司 | 一种测定异丙托溴铵吸入剂中邻苯二甲酸二丁酯和邻苯二甲酸二异丁酯的方法 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104833734A (zh) | 食品包装材料中邻苯二甲酸酯类物质迁移量的检测方法 | |
CN106124653B (zh) | 虾中5种硝基呋喃类代谢物和氯霉素多残留的检测方法 | |
Xian et al. | Dispersive micro solid phase extraction (DMSPE) using polymer anion exchange (PAX) as the sorbent followed by UPLC–MS/MS for the rapid determination of four bisphenols in commercial edible oils | |
Maragou et al. | Determination of bisphenol A in milk by solid phase extraction and liquid chromatography–mass spectrometry | |
CN102175784B (zh) | 固相萃取-液相色谱-质谱/质谱法同时测定猪肉中54种药物残留的方法 | |
CN106324144B (zh) | 亲水作用色谱-串联质谱法检测乳粉及婴幼儿配方乳粉中氯酸盐、高氯酸盐和溴酸盐的方法 | |
Llop et al. | Automated determination of aliphatic primary amines in wastewater by simultaneous derivatization and headspace solid-phase microextraction followed by gas chromatography–tandem mass spectrometry | |
CN106153801A (zh) | 一种同时检测白酒原辅料中七种真菌毒素的方法 | |
CN107782824A (zh) | 一种pet塑料瓶中多种紫外稳定剂的快速检测方法 | |
CN105758945A (zh) | 一种检测金枪鱼罐头中双酚类化合物的方法 | |
Song et al. | A selective and sensitive pre-column derivatization HPLC method for the trace analysis of genotoxic impurity hydroxylamine in active pharmaceutical ingredients | |
CN104820030A (zh) | 一种液质联用检测饮用水中六种邻苯二甲酸酯的方法 | |
CN109342633A (zh) | 尿液中苯、甲苯和二甲苯代谢物的检测方法 | |
CN105372340A (zh) | 高效液相色谱-串联质谱法测定低含量帕立骨化醇的方法及其应用 | |
CN109192652B (zh) | 一种基于介质阻挡放电离子源的磺酸酯类基因毒性杂质的质谱检测方法 | |
Katteboina et al. | LC-MS/MS Method Development and Validation of Montelukast in human plasma and its clinical application | |
Volpe et al. | High-performance liquid chromatography of two peripheral vasodilators, nylidrin hydrochloride and isoxsuprine hydrochloride, in pharmaceutical dosage forms | |
Lin et al. | Determination of Four Types of Hazardous Chemicals in Food Contact Materials by UHPLC‐MS/MS | |
Ryska | How to deal with the “matrix effect” as an unavoidable phenomenon | |
Wang et al. | Determination of eight Sudan dyes in chili powder by UPLC-MS/MS | |
Lin et al. | An LC-MS/MS method for determination of novel fungicide pyraoxystrobin in rat plasma and tissues: Toxicokinetics and tissue distribution study | |
Driffield et al. | A method of test for residual isophorone diisocyanate trimer in new polyester-polyurethane coatings on light metal packaging using liquid chromatography with tandem mass spectrometric detection | |
Fan et al. | Simultaneous determination of 20 phthalate esters in oil-free food by UPLC/MS/MS | |
Khan et al. | Application of Validated UPLC/Q-TOF-MS Method for Simultaneous Determination of Telmisartan, Hydrochlorothiazide and their Degradation Products in Tablets | |
Zhang et al. | Fast simultaneous determination of multiple water-soluble vitamins and vitamin-like compounds in infant formula by UPLC-MS/MS |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Qiang Wei Inventor after: Qu Li Inventor after: Cao Chen Inventor after: Zhou Yao Inventor after: Deng Xiaojun Inventor after: Shi Yiyin Inventor before: Qiang Wei Inventor before: Qu Li Inventor before: Cao Chen Inventor before: Zhou Yao Inventor before: Deng Xiaojun |
|
COR | Change of bibliographic data | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20151211 Address after: 201609 Shanghai Songjiang District Yexie town leaves 451 Lane 39, room 504, Zheng Lu Applicant after: Shanghai Anpu Experimental Technology Co., Ltd. Applicant after: Shanghai Bureau of Emigration &. Engression Examination &. Quarantine People's R Address before: 201609 Shanghai Songjiang District Yexie town leaves 451 Lane 39, room 504, Zheng Lu Applicant before: Shanghai Anpu Experimental Technology Co., Ltd. Applicant before: Shanghai inspection and quarantining for import/export animals and plants and Food Inspection Quarantine Techniques center |
|
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150812 |