CN104804701A - 一种醇溶性聚氨酯胶粘剂及其制备方法 - Google Patents
一种醇溶性聚氨酯胶粘剂及其制备方法 Download PDFInfo
- Publication number
- CN104804701A CN104804701A CN201510215972.7A CN201510215972A CN104804701A CN 104804701 A CN104804701 A CN 104804701A CN 201510215972 A CN201510215972 A CN 201510215972A CN 104804701 A CN104804701 A CN 104804701A
- Authority
- CN
- China
- Prior art keywords
- alcohol
- prepared
- polyurethane adhesive
- host
- soluble polyurethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000853 adhesive Substances 0.000 title claims abstract description 27
- 230000001070 adhesive effect Effects 0.000 title claims abstract description 27
- 239000004814 polyurethane Substances 0.000 title claims abstract description 26
- 229920002635 polyurethane Polymers 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 35
- 239000000178 monomer Substances 0.000 claims abstract description 12
- 239000002262 Schiff base Substances 0.000 claims abstract description 7
- 150000004753 Schiff bases Chemical class 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims description 26
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 22
- 229920000642 polymer Polymers 0.000 claims description 20
- 230000015572 biosynthetic process Effects 0.000 claims description 18
- 238000003786 synthesis reaction Methods 0.000 claims description 16
- 239000002585 base Substances 0.000 claims description 14
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 11
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 10
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 10
- 239000007822 coupling agent Substances 0.000 claims description 10
- 239000003822 epoxy resin Substances 0.000 claims description 10
- 229920000647 polyepoxide Polymers 0.000 claims description 10
- 229920000570 polyether Polymers 0.000 claims description 10
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 10
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 10
- 229920002554 vinyl polymer Polymers 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 9
- 238000007664 blowing Methods 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000009413 insulation Methods 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 239000000047 product Substances 0.000 abstract description 6
- 239000007795 chemical reaction product Substances 0.000 abstract description 3
- 239000002131 composite material Substances 0.000 abstract description 3
- 239000002612 dispersion medium Substances 0.000 abstract description 3
- 239000012528 membrane Substances 0.000 abstract description 3
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 239000002253 acid Substances 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000002912 waste gas Substances 0.000 description 2
- DWNBOPVKNPVNQG-LURJTMIESA-N (2s)-4-hydroxy-2-(propylamino)butanoic acid Chemical compound CCCN[C@H](C(O)=O)CCO DWNBOPVKNPVNQG-LURJTMIESA-N 0.000 description 1
- KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical group NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000004848 polyfunctional curative Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
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- Adhesives Or Adhesive Processes (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510215972.7A CN104804701B (zh) | 2015-04-30 | 2015-04-30 | 一种醇溶性聚氨酯胶粘剂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510215972.7A CN104804701B (zh) | 2015-04-30 | 2015-04-30 | 一种醇溶性聚氨酯胶粘剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104804701A true CN104804701A (zh) | 2015-07-29 |
CN104804701B CN104804701B (zh) | 2017-08-08 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201510215972.7A Active CN104804701B (zh) | 2015-04-30 | 2015-04-30 | 一种醇溶性聚氨酯胶粘剂及其制备方法 |
Country Status (1)
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CN (1) | CN104804701B (zh) |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040242763A1 (en) * | 2001-11-28 | 2004-12-02 | Michel Tielemans | Radiation-curable polyurethane dispersion |
CN1970672A (zh) * | 2006-12-15 | 2007-05-30 | 成都市新津托展油墨有限公司 | 醇溶性聚氨酯双组分粘合剂及其制备工艺 |
CN101735761A (zh) * | 2009-11-12 | 2010-06-16 | 李银松 | 一种醇溶性聚氨酯双组份粘合剂 |
-
2015
- 2015-04-30 CN CN201510215972.7A patent/CN104804701B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040242763A1 (en) * | 2001-11-28 | 2004-12-02 | Michel Tielemans | Radiation-curable polyurethane dispersion |
CN1970672A (zh) * | 2006-12-15 | 2007-05-30 | 成都市新津托展油墨有限公司 | 醇溶性聚氨酯双组分粘合剂及其制备工艺 |
CN101735761A (zh) * | 2009-11-12 | 2010-06-16 | 李银松 | 一种醇溶性聚氨酯双组份粘合剂 |
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Publication number | Publication date |
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CN104804701B (zh) | 2017-08-08 |
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Effective date of registration: 20180626 Address after: 313300 Zhejiang Anji Huzhou County Modern Lake Industrial Park Patentee after: ANJI KEGUANG NEW MATERIAL TECHNOLOGY Co.,Ltd. Address before: 313300 Huzhou City, Zhejiang Province, Anji County, Shan Chuan village boat Village Patentee before: ANJI COUNTY GUANGTAI CHEMICAL PAPER Co.,Ltd. |
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TR01 | Transfer of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Alcohol soluble polyurethane adhesive and its preparation method Effective date of registration: 20210527 Granted publication date: 20170808 Pledgee: Anji green sub branch of Hangzhou United Rural Commercial Bank Co.,Ltd. Pledgor: ANJI KEGUANG NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2021330000459 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231129 Granted publication date: 20170808 Pledgee: Anji green sub branch of Hangzhou United Rural Commercial Bank Co.,Ltd. Pledgor: ANJI KEGUANG NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2021330000459 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A alcohol soluble polyurethane adhesive and its preparation method Effective date of registration: 20231202 Granted publication date: 20170808 Pledgee: Anji green sub branch of Hangzhou United Rural Commercial Bank Co.,Ltd. Pledgor: ANJI KEGUANG NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2023330002913 |