CN104737005B - 具有晶粒取向映射功能的实验室x射线微断层扫描系统 - Google Patents

具有晶粒取向映射功能的实验室x射线微断层扫描系统 Download PDF

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CN104737005B
CN104737005B CN201380054570.2A CN201380054570A CN104737005B CN 104737005 B CN104737005 B CN 104737005B CN 201380054570 A CN201380054570 A CN 201380054570A CN 104737005 B CN104737005 B CN 104737005B
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sample
light beam
detector
broadband
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CN104737005A (zh
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迈克尔·费泽
克里斯蒂安·霍尔茨纳
埃里克·迈达尔·劳里森
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Ka Er Zeiss X-Ray Microscope Co
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Ka Er Zeiss X-Ray Microscope Co
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/20Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
    • G01N23/207Diffractometry using detectors, e.g. using a probe in a central position and one or more displaceable detectors in circumferential positions
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/02Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
    • G01N23/04Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and forming images of the material
    • G01N23/046Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and forming images of the material using tomography, e.g. computed tomography [CT]
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/40Imaging
    • G01N2223/419Imaging computed tomograph
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/60Specific applications or type of materials
    • G01N2223/606Specific applications or type of materials texture

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Pulmonology (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Engineering & Computer Science (AREA)
  • Theoretical Computer Science (AREA)
  • Radiology & Medical Imaging (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Measurement Of Radiation (AREA)
CN201380054570.2A 2012-10-18 2013-10-18 具有晶粒取向映射功能的实验室x射线微断层扫描系统 Active CN104737005B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201261715696P 2012-10-18 2012-10-18
US61/715,696 2012-10-18
PCT/US2013/065584 WO2014063002A1 (en) 2012-10-18 2013-10-18 Laboratory x-ray micro-tomography system with crystallographic grain orientation mapping capabilities

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CN104737005A CN104737005A (zh) 2015-06-24
CN104737005B true CN104737005B (zh) 2017-09-29

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US (2) US9110004B2 (enExample)
EP (1) EP2909611B1 (enExample)
JP (1) JP6039093B2 (enExample)
KR (1) KR102003202B1 (enExample)
CN (1) CN104737005B (enExample)
WO (1) WO2014063002A1 (enExample)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102003202B1 (ko) * 2012-10-18 2019-07-24 칼 짜이스 엑스-레이 마이크로스코피, 인크. 결정학적 그레인 배향 맵핑 능력을 가진 실험실 x-레이 마이크로-단층촬영 시스템
US9222900B2 (en) 2013-03-05 2015-12-29 Danmarks Tekniske Universitet Of Anker Engelundsvej X-ray diffraction method of mapping grain structures in a crystalline material sample, and an X-ray diffraction apparatus
EP2775295B8 (en) * 2013-03-05 2016-05-18 Danmarks Tekniske Universitet An X-ray diffraction method of mapping grain structures in a crystalline material sample, and an X-ray diffraction apparatus.
US9222901B2 (en) 2013-03-05 2015-12-29 Danmarks Tekniske Universitet Anker Engelundsvej X-ray diffraction method of mapping grain structures in a crystalline material sample, and an X-ray diffraction apparatus
CN105612416B (zh) * 2013-07-25 2019-01-01 模拟技术公司 对象内物品的衍射特征的生成
KR102025361B1 (ko) * 2014-07-10 2019-09-25 한화테크윈 주식회사 자동 초점 조절 시스템 및 방법
GB201421837D0 (en) * 2014-12-09 2015-01-21 Reishig Peter A method of generating a fingerprint for a gemstone using X-ray imaging
EP3223002B1 (en) * 2016-03-23 2021-04-28 Carl Zeiss X-Ray Microscopy, Inc. Method, tool and computer program product for measurement and estimation of an x-ray source spectrum in computed tomography, and x-ray ct system
CN105869179A (zh) * 2016-06-06 2016-08-17 青岛晶维科创医药工程有限公司 一种晶体颗粒三维成像系统及方法
CN108376656B (zh) * 2018-02-08 2020-07-31 北京科技大学 基于二维x射线检测技术的超大晶粒尺寸的无损检测方法
US11275039B2 (en) * 2018-07-25 2022-03-15 Bruker Axs, Inc. Divergent beam two dimensional diffraction
CN109490343A (zh) * 2018-12-04 2019-03-19 西北工业大学 一种串行晶体学样品输运装置及方法
EP3987279B1 (de) * 2019-06-24 2023-11-08 SMS Group GmbH Vorrichtung und verfahren zum bestimmen der werkstoffeigenschaften eines polykristallinen produkts
WO2021209048A1 (en) * 2020-04-17 2021-10-21 Master Dynamic Limited Imaging process and system
US12209978B2 (en) 2020-07-15 2025-01-28 Danmarks Tekniske Universitet Laboratory-based 3D scanning X-ray Laue micro-diffraction system and method (Lab3DμXRD)
EP4019951A1 (en) 2020-12-24 2022-06-29 Inel S.A.S Apparatuses and methods for combined simultaneous analyses of materials
WO2023113862A2 (en) * 2021-06-16 2023-06-22 Carl Zeiss X-ray Microscopy, Inc. Laboratory crystallographic x-ray diffraction analysis system
US12436115B2 (en) * 2022-02-25 2025-10-07 Proto Patents Ltd. Transmission X-ray diffraction apparatus and related method
CN115372395A (zh) * 2022-08-30 2022-11-22 郑州轻工业大学 一种基于纳米机器人拾放操作的块材内部晶界自动表征系统和方法
CN115494542B (zh) * 2022-09-16 2024-10-18 中国科学院上海高等研究院 一种同步辐射光束带宽的检测系统及方法
CN116184479B (zh) * 2023-02-20 2025-12-05 同济大学 一种多通道空间分辨弯晶谱仪及其装调方法
US20240298988A1 (en) * 2023-03-07 2024-09-12 Mark S. Quadling X-Ray Computed Tomography (CT) scanning using a line array detector
CN120426915B (zh) * 2025-06-25 2025-09-16 安徽创谱仪器科技有限公司 一种x射线光源光斑尺寸的测试方法及系统
CN120741531B (zh) * 2025-08-28 2025-11-07 中国航发北京航空材料研究院 一种晶体取向检测方法及相关装置

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1563959A (zh) * 2004-04-06 2005-01-12 中国科学院上海光学精密机械研究所 时间分辨x射线衍射层析装置
WO2006113908A2 (en) * 2005-04-20 2006-10-26 The Regents Of The University Of California Crytomography x-ray microscope stage
US20110038457A1 (en) * 2009-02-23 2011-02-17 X-Ray Optical Systems, Inc. X-ray diffraction apparatus and technique for measuring grain orientation using x-ray focusing optic
US7978821B1 (en) * 2008-02-15 2011-07-12 The United States Of America As Represented By The Secretary Of The Air Force Laue crystallographic orientation mapping system
US20120008736A1 (en) * 2010-07-09 2012-01-12 Danmarks Tekniske Universitet X-ray diffraction contrast tomography (dct) system, and an x-ray diffraction contrast tomography (dct) method

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2312507A1 (de) 1973-03-13 1974-09-26 Max Planck Gesellschaft Geraet fuer roentgenbeugungsmessungen mittels weisser roentgenstrahlen
FR2668262B1 (fr) 1990-10-23 1994-04-01 Centre Nal Recherc Scientifique Procede d'analyse aux rayons x de pieces monocristallines.
US5491738A (en) 1993-03-15 1996-02-13 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration X-ray diffraction apparatus
JP3684745B2 (ja) * 1997-02-25 2005-08-17 Jfeスチール株式会社 結晶粒三次元表示方法
US7130375B1 (en) 2004-01-14 2006-10-31 Xradia, Inc. High resolution direct-projection type x-ray microtomography system using synchrotron or laboratory-based x-ray source
US7443953B1 (en) 2005-12-09 2008-10-28 Xradia, Inc. Structured anode X-ray source for X-ray microscopy
JP4589882B2 (ja) * 2006-02-14 2010-12-01 株式会社リガク 背面反射x線回折像観察装置
KR101061425B1 (ko) * 2006-07-12 2011-09-01 포항공과대학교 산학협력단 X-선을 이용한 명시야 촬영 방법
US20120097835A1 (en) * 2009-05-19 2012-04-26 BioNano Geneomics, Inc. Devices and methods for dynamic determination of sample position and orientation and dynamic repositioning
FR2965921B1 (fr) * 2010-10-11 2012-12-14 Commissariat Energie Atomique Procede de mesure de l'orientation et de la deformation elastique de grains dans des materiaux multicristallins
KR102003202B1 (ko) * 2012-10-18 2019-07-24 칼 짜이스 엑스-레이 마이크로스코피, 인크. 결정학적 그레인 배향 맵핑 능력을 가진 실험실 x-레이 마이크로-단층촬영 시스템
EP2775295B8 (en) 2013-03-05 2016-05-18 Danmarks Tekniske Universitet An X-ray diffraction method of mapping grain structures in a crystalline material sample, and an X-ray diffraction apparatus.

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1563959A (zh) * 2004-04-06 2005-01-12 中国科学院上海光学精密机械研究所 时间分辨x射线衍射层析装置
WO2006113908A2 (en) * 2005-04-20 2006-10-26 The Regents Of The University Of California Crytomography x-ray microscope stage
US7978821B1 (en) * 2008-02-15 2011-07-12 The United States Of America As Represented By The Secretary Of The Air Force Laue crystallographic orientation mapping system
US20110038457A1 (en) * 2009-02-23 2011-02-17 X-Ray Optical Systems, Inc. X-ray diffraction apparatus and technique for measuring grain orientation using x-ray focusing optic
US20120008736A1 (en) * 2010-07-09 2012-01-12 Danmarks Tekniske Universitet X-ray diffraction contrast tomography (dct) system, and an x-ray diffraction contrast tomography (dct) method

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
A laboratory based system for Laue micro x-ray diffraction;P. A. Lynch et al.;《Review of Scientific Instruments》;20070209;第78卷(第2期);第23904页 *
Three-dimensional grain mapping by x-ray diffraction contrast tomography and the use of Friedel pairs in diffraction data analysis;W. Ludwig et al.;《Review of Scientific Instruments》;20090319;第80卷(第3期);第33905页 *
一种测定晶体取向及其分布的简便XRD方法;郭振琪等;《无机材料学报》;20020531;第17卷(第03期);第460-464页 *

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Publication number Publication date
JP2015533415A (ja) 2015-11-24
US20150316493A1 (en) 2015-11-05
EP2909611B1 (en) 2016-04-13
KR102003202B1 (ko) 2019-07-24
WO2014063002A1 (en) 2014-04-24
US20140112433A1 (en) 2014-04-24
KR20150068436A (ko) 2015-06-19
US9110004B2 (en) 2015-08-18
EP2909611A1 (en) 2015-08-26
CN104737005A (zh) 2015-06-24
JP6039093B2 (ja) 2016-12-07
US9383324B2 (en) 2016-07-05

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