CN104640834B - 多羧酸萃取 - Google Patents

多羧酸萃取 Download PDF

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Publication number
CN104640834B
CN104640834B CN201280062774.6A CN201280062774A CN104640834B CN 104640834 B CN104640834 B CN 104640834B CN 201280062774 A CN201280062774 A CN 201280062774A CN 104640834 B CN104640834 B CN 104640834B
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China
Prior art keywords
acid
extraction
aqueous
aqueous mixture
organic
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Expired - Fee Related
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CN201280062774.6A
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English (en)
Chinese (zh)
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CN104640834A (zh
Inventor
A·B·德哈恩
J·范克里肯
T·杰基奇奇夫科维奇
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Purac Biochem BV
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Purac Biochem BV
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Expired - Fee Related legal-status Critical Current
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/44—Polycarboxylic acids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41—Preparation of salts of carboxylic acids
    • C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
    • C07C55/02—Dicarboxylic acids
    • C07C55/10—Succinic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/13—Dicarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/13—Dicarboxylic acids
    • C07C57/15—Fumaric acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C59/01—Saturated compounds having only one carboxyl group and containing hydroxy or O-metal groups
    • C07C59/08—Lactic acid
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/56—Lactic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Biotechnology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Extraction Or Liquid Replacement (AREA)
CN201280062774.6A 2011-12-23 2012-12-21 多羧酸萃取 Expired - Fee Related CN104640834B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11195691 2011-12-23
EP11195691.8 2011-12-23
PCT/EP2012/076735 WO2013093043A1 (en) 2011-12-23 2012-12-21 Polycarboxylic acid extraction

Publications (2)

Publication Number Publication Date
CN104640834A CN104640834A (zh) 2015-05-20
CN104640834B true CN104640834B (zh) 2017-02-22

Family

ID=48667768

Family Applications (3)

Application Number Title Priority Date Filing Date
CN201280062774.6A Expired - Fee Related CN104640834B (zh) 2011-12-23 2012-12-21 多羧酸萃取
CN201280062771.2A Active CN103998108B (zh) 2011-12-23 2012-12-21 从水溶液中分离羧酸的方法
CN201280062768.0A Active CN104053641B (zh) 2011-12-23 2012-12-21 乳酸萃取

Family Applications After (2)

Application Number Title Priority Date Filing Date
CN201280062771.2A Active CN103998108B (zh) 2011-12-23 2012-12-21 从水溶液中分离羧酸的方法
CN201280062768.0A Active CN104053641B (zh) 2011-12-23 2012-12-21 乳酸萃取

Country Status (20)

Country Link
US (2) US10017451B2 (https=)
EP (3) EP2794544B1 (https=)
JP (3) JP6022600B2 (https=)
KR (4) KR101650695B1 (https=)
CN (3) CN104640834B (https=)
AU (3) AU2012356848B2 (https=)
BR (3) BR112014014881B1 (https=)
CA (3) CA2859707C (https=)
DK (1) DK2794049T3 (https=)
EA (3) EA024994B1 (https=)
ES (2) ES2689554T3 (https=)
HU (2) HUE037640T2 (https=)
IN (1) IN2014CN04949A (https=)
MY (3) MY170077A (https=)
PL (3) PL2794049T3 (https=)
PT (1) PT2794544T (https=)
UA (3) UA114497C2 (https=)
VN (3) VN39714A1 (https=)
WO (3) WO2013093043A1 (https=)
ZA (2) ZA201405100B (https=)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
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CN104640834B (zh) * 2011-12-23 2017-02-22 普拉克生化公司 多羧酸萃取
DK2812304T3 (en) * 2012-02-08 2018-06-25 Purac Biochem Bv CARBOXYLATE ACID
KR101828769B1 (ko) * 2013-02-14 2018-02-13 푸락 바이오켐 비.브이. 석신산 에스테르의 제조 방법
EP2821368A1 (en) * 2013-07-03 2015-01-07 PURAC Biochem BV Method for processing magnesium chloride solutions
CN111960447A (zh) * 2014-04-01 2020-11-20 普拉克生化公司 氯化镁的热分解
WO2016016235A1 (en) 2014-07-28 2016-02-04 Purac Biochem Bv Preparation of lactic acid and/or a lactate salt from lignocellulosic material by separate saccharification and fermentation steps
DK3174988T3 (da) 2014-07-28 2022-11-28 Purac Biochem Bv Fremgangsmåde til fremstilling af mælkesyre
CN105503578B (zh) * 2014-09-26 2018-03-02 常茂生物化学工程股份有限公司 一种用萃取剂从发酵液中提取丁二酸的方法
EP3056490A1 (en) 2015-02-13 2016-08-17 PURAC Biochem BV Method for manufacturing lactide
EP3271342B1 (en) 2015-03-17 2021-08-18 Purac Biochem B.V. Method for manufacturing furan-2,5-dicarboxylic acid (fdca) from a salt solution
JP6361980B2 (ja) * 2015-05-26 2018-07-25 住友金属鉱山株式会社 有機溶液中のシュウ酸の分析方法
BR112018014591B1 (pt) * 2016-01-19 2023-04-25 Purac Biochem Bv Método para processamento de soluções de cloreto de magnésio e para fabricação de ácidos carboxílicos
JP6884802B2 (ja) * 2016-05-30 2021-06-09 ピュラック バイオケム ビー． ブイ． 固体発酵生成物からバイオマスを分離する方法
CN106220493B (zh) * 2016-07-22 2018-09-25 南京正大天晴制药有限公司 一种l-苹果酸的精制方法
CN110845326A (zh) * 2017-06-09 2020-02-28 安徽丰原发酵技术工程研究有限公司 一种通过脱水萃取制备乳酸和丙交酯的方法
CN107344911A (zh) * 2017-06-09 2017-11-14 安徽丰原发酵技术工程研究有限公司 一种提取柠檬酸/柠檬酸盐的方法
CN107353196A (zh) * 2017-06-09 2017-11-17 安徽丰原发酵技术工程研究有限公司 一种提取丁二酸/丁二酸盐的方法
CN107176907A (zh) * 2017-06-09 2017-09-19 安徽丰原发酵技术工程研究有限公司 一种提取苹果酸/苹果酸盐的方法
CN107353197A (zh) * 2017-06-09 2017-11-17 安徽丰原发酵技术工程研究有限公司 一种提取3‑羟基丙酸的方法
SG11202003616PA (en) 2017-10-26 2020-05-28 Noroo Ic Co Ltd Production and separation of 3-hydroxypropionic acid
IL282900B2 (en) 2018-11-26 2025-02-01 Triplew Ltd Magnesium lactate purification from fermentation solutions containing large amounts of impurities
CN110028402B (zh) * 2019-05-30 2022-01-25 上海泰坦科技股份有限公司 一种提取3-羟基丙酸的方法
CA3155694A1 (en) 2019-09-24 2021-04-01 Genetec Inc. Intermediary device for daisy chain and tree configuration in hybrid data/power connection
CN112745215B (zh) * 2019-10-31 2022-11-11 中国石油化工股份有限公司 一种从乳酸盐的含水原料中转化乳酸和提取乳酸相耦合的方法
EP4090443A1 (en) 2020-01-15 2022-11-23 Purac Biochem B.V. Method for purifying magnesium chloride solutions
KR102832610B1 (ko) 2020-04-20 2025-07-11 푸락 바이오켐 비.브이. 고순도 산화마그네슘 제조방법
US11770155B2 (en) 2020-05-19 2023-09-26 Genetec Inc. Power distribution and data routing in a network of devices interconnected by hybrid data/power links
CN121548561A (zh) 2023-05-12 2026-02-17 百帆科技有限责任公司 生产和回收乙酰丙酸的方法
WO2025083005A1 (en) 2023-10-17 2025-04-24 Purac Biochem B.V. Process for manufacturing high-purity magnesium oxide from magnesium chloride
CN119176749B (zh) * 2024-11-22 2025-07-18 上海金发科技发展有限公司 一种生物基丁二酸组合物及其制备方法、由其制备的聚酯

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US3786096A (en) * 1970-03-24 1974-01-15 Mitsubishi Petrochemical Co Recovery of adipic acid
US4273234A (en) * 1979-02-02 1981-06-16 Bourgeois Ronald D Conveyor storage system
WO1995003268A1 (en) * 1993-07-26 1995-02-02 A.E. Staley Manufacturing Company Process for recovering organic acids
WO2000017378A2 (en) * 1998-09-17 2000-03-30 Imi (Tami) Process for preparing lactic acid
CN101979368A (zh) * 2010-10-19 2011-02-23 大连理工大学 一种盐析萃取发酵液中有机酸的方法

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CN104640834B (zh) * 2011-12-23 2017-02-22 普拉克生化公司 多羧酸萃取
PT2794049T (pt) * 2011-12-23 2018-10-31 Purac Biochem Bv Método para isolar um ácido carboxílico a partir de uma solução aquosa
ES2531399T3 (es) * 2012-05-24 2015-03-13 Purac Biochem Nv Recuperación de ácido carboxílico de una mezcla de carboxilato de magnesio
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Patent Citations (5)

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Publication number Priority date Publication date Assignee Title
US3786096A (en) * 1970-03-24 1974-01-15 Mitsubishi Petrochemical Co Recovery of adipic acid
US4273234A (en) * 1979-02-02 1981-06-16 Bourgeois Ronald D Conveyor storage system
WO1995003268A1 (en) * 1993-07-26 1995-02-02 A.E. Staley Manufacturing Company Process for recovering organic acids
WO2000017378A2 (en) * 1998-09-17 2000-03-30 Imi (Tami) Process for preparing lactic acid
CN101979368A (zh) * 2010-10-19 2011-02-23 大连理工大学 一种盐析萃取发酵液中有机酸的方法

Also Published As

Publication number Publication date
CN104053641A (zh) 2014-09-17
BR112014014882A2 (pt) 2017-06-13
AU2012356848A8 (en) 2014-10-23
AU2012356848A1 (en) 2014-07-31
CA2859706C (en) 2020-01-28
CA2859705A1 (en) 2013-06-27
VN39373A1 (en) 2014-09-25
KR20140108696A (ko) 2014-09-12
JP6118338B2 (ja) 2017-04-19
EA201491093A1 (ru) 2014-11-28
EP2794544B1 (en) 2018-03-14
CA2859707C (en) 2019-11-12
WO2013093043A1 (en) 2013-06-27
MY165221A (en) 2018-03-09
CA2859705C (en) 2020-07-21
KR101650694B1 (ko) 2016-08-24
JP2015507623A (ja) 2015-03-12
UA113530C2 (xx) 2017-02-10
US10017451B2 (en) 2018-07-10
BR112014014883A2 (pt) 2017-06-13
CA2859707A1 (en) 2013-06-27
EP2794545A1 (en) 2014-10-29
UA114497C2 (uk) 2017-06-26
ZA201405100B (en) 2015-11-25
CN104640834A (zh) 2015-05-20
EP2794544A1 (en) 2014-10-29
IN2014CN04949A (https=) 2015-09-18
EP2794049A1 (en) 2014-10-29
WO2013093047A1 (en) 2013-06-27
US20150004663A1 (en) 2015-01-01
CA2859706A1 (en) 2013-06-27
EP2794049B1 (en) 2018-07-18
VN39714A1 (en) 2014-10-27
AU2012356770A8 (en) 2014-09-18
AU2012356774A8 (en) 2014-10-23
BR112014014882B1 (pt) 2021-02-02
KR101650695B1 (ko) 2016-08-24
EA201491113A1 (ru) 2014-11-28
JP2015500866A (ja) 2015-01-08
EA201491146A1 (ru) 2014-11-28
KR101913670B1 (ko) 2018-11-01
ZA201405104B (en) 2015-11-25
AU2012356848B2 (en) 2016-02-04
CN103998108B (zh) 2016-08-24
EA024181B1 (ru) 2016-08-31
JP6085311B2 (ja) 2017-02-22
ES2689554T3 (es) 2018-11-14
MY170077A (en) 2019-07-03
KR20140112041A (ko) 2014-09-22
BR112014014881A2 (pt) 2017-06-13
CN103998108A (zh) 2014-08-20
UA110671C2 (uk) 2016-01-25
US11299447B2 (en) 2022-04-12
KR20160106787A (ko) 2016-09-12
AU2012356770B2 (en) 2016-01-28
EA024143B1 (ru) 2016-08-31
US20140335581A1 (en) 2014-11-13
VN39713A1 (en) 2014-10-27
AU2012356774A1 (en) 2014-07-31
JP2015504044A (ja) 2015-02-05
BR112014014881B1 (pt) 2021-09-28
ES2669319T3 (es) 2018-05-24
PL2794545T3 (pl) 2021-01-25
EP2794545B1 (en) 2020-06-03
PL2794544T3 (pl) 2018-09-28
PL2794049T3 (pl) 2019-01-31
KR20140112524A (ko) 2014-09-23
HUE039459T2 (hu) 2019-01-28
WO2013093028A1 (en) 2013-06-27
PT2794544T (pt) 2018-05-18
MY176926A (en) 2020-08-26
CN104053641B (zh) 2016-11-23
EA024994B1 (ru) 2016-11-30
BR112014014883B1 (pt) 2021-02-02
JP6022600B2 (ja) 2016-11-09
AU2012356774B2 (en) 2016-03-31
DK2794049T3 (en) 2018-10-22
AU2012356770A1 (en) 2014-07-24
HUE037640T2 (hu) 2018-09-28

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