CN104529548A - Red-spot crystalline glaze and preparation method of ceramic adopting same - Google Patents
Red-spot crystalline glaze and preparation method of ceramic adopting same Download PDFInfo
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Abstract
The invention discloses a red-spot crystalline glaze and a preparation method of ceramic adopting the same, belonging to the technical field of crystalline glazes. The glaze mainly comprises the following raw materials in parts by weight: 20-40 parts of albite, 10-20 parts of quartz, 10-20 parts of calcined talc, 1-10 parts of calcite, 10-25 parts of bone ash, 1-10 parts of glass powder, 5-15 parts of barium carbonate and 5-2 parts of iron oxide. The method comprises the following steps: (1) weighing the raw materials, performing wet grinding to obtain glaze slip, and aging; (2) glazing a biscuit firing billet, and drying; and (3) firing the dried billet in a kiln, and finishing the whole firing process of heating, high temperature keeping, cooling, low temperature keeping and extinction within 230-655 minutes. The invention aims to provide a red-spot crystalline glaze which is scientific in formula and favorable in use effect and a preparation method of ceramic adopting the same, and is used for red-spot crystalline glaze and ceramic manufacturing.
Description
Technical field
The present invention relates to a kind of glaze formula, more particularly, particularly relate to a kind of erythema crystalline glaze.The present invention also relates to a kind of ceramic preparation adopting this erythema crystalline glaze simultaneously.
Background technology
Erythema crystalline substance flower artistic glaze is a kind of famous and precious crystallization artistic glaze, it is characterized in that being studded with circular erythema crystalline substance flower in brown or tan glaze paint, reflects the radiance glittered under light illumination, has strong stereoscopic sensation and artistic effect, be loved by the people.Adopt existing formula and technique, when firing, existing and burning till difficulty greatly, product poor repeatability, the shortcoming that harvest rate is low.Burn this crystalline glaze and whole kiln product particle often occurs without the phenomenon received, bring larger financial loss to enterprise.
Summary of the invention
The object of the invention is to for above-mentioned the deficiencies in the prior art, the erythema crystalline glaze that a kind of scientific formulation, result of use are good is provided.
Another object of the present invention is to provide a kind of ceramic preparation adopting above-mentioned erythema crystallization to burn.
Last technical scheme of the present invention is achieved in that a kind of erythema crystalline glaze, and this glaze forms primarily of the raw material of following weight parts: albite 20 ~ 40 parts, 10 ~ 20 parts, quartz, burning 10 ~ 20 parts, talcum, 1 ~ 10 part, calcite, 10 ~ 25 parts, bone ash, 1 ~ 10 part, glass powder, barium carbonate 5 ~ 15 parts, ferric oxide 5 ~ 20 parts;
Preferably, glaze forms primarily of the raw material of following weight parts: albite 25 ~ 35 parts, 10 ~ 15 parts, quartz, burning 10 ~ 15 parts, talcum, 2 ~ 8 parts, calcite, 10 ~ 20 parts, bone ash, 2 ~ 8 parts, glass powder, barium carbonate 5 ~ 10 parts, ferric oxide 10 ~ 15 parts.
In above-mentioned a kind of erythema crystalline glaze, glaze also comprises the raw material of following weight parts: kaolin 0.5 ~ 2 part, Fluorspar Powder 0.3 ~ 2 part; Preferably, glaze also comprises the raw material of following weight parts: kaolin 0.8 ~ 1.5 part, Fluorspar Powder 0.5 ~ 1 part.
After of the present invention, a technical scheme is achieved in that a kind of ceramic preparation adopting erythema crystalline glaze described in above-mentioned arbitrary claim, comprise the steps: that (1) takes each raw material by glaze formula, put into ball mill wet-milling and obtain glaze slip, old rear for subsequent use; (2) glazing on biscuit, glazing thickness is 0.8 ~ 1.2mm, carries out drying treatment after glazing; (3) dried base substrate loading of kiln is fired, when firing, from room temperature to 90 ~ 240 minutes 500 DEG C of used times, 1250 DEG C ~ 1280 DEG C are risen to rapidly after 1200 DEG C, soak is after 10 ~ 50 minutes, slowly be down to 1150 DEG C ~ 1180 DEG C and be incubated 20 ~ 120 minutes, last powered-down naturally cooling, whole firing time is 230 ~ 655 minutes.
In above-mentioned ceramic preparation, material during step (1) described wet-milling: ball: the weight ratio of water is 1: 2: 0.6 ~ 1, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, and glaze slip water ratio is 45 ~ 48%.
In above-mentioned ceramic preparation, in step (3), the concrete technology fired is from room temperature to 90 ~ 240 minutes 500 DEG C of used times, 60 ~ 120 minutes used times from 500 DEG C to 950 DEG C, 10 ~ 40 minutes used times from 950 DEG C to 1100 DEG C, 10 ~ 25 minutes used times from 1100 DEG C to 1200 DEG C, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C of 10 ~ 20 minutes used times, be incubated and be cooled to 1150 DEG C ~ 1180 DEG C after 10 ~ 50 minutes, be down to 20 ~ 40 minutes preset temperature used times and be incubated 20 ~ 120 minutes at preset temperature, last powered-down naturally cooling, whole firing time is 230 ~ 655 minutes.
In above-mentioned ceramic preparation, when firing, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C, be incubated after 10-50 minute, be cooled to 1150 DEG C ~ 1160 DEG C and be incubated 20 ~ 60 minutes.
In above-mentioned ceramic preparation, when firing, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C, be incubated after 10-50 minute, be cooled to 1160 DEG C ~ 1180 DEG C and be incubated 60 ~ 120 minutes.
The present invention adopts above-mentioned glaze formula, by the amount of reasonably combined each component, especially the content of bone ash and ferric oxide, ferric oxide is main crystallizing agent and tinting material in formula, very big on the artistic effect impact of erythema crystalline substance flower artistic glaze, add very little, glaze paint does not have circular brilliant flower, the mottled mixed and disorderly distribution in yellow-green colour; Add too many, crystallization is easily linked to be sheet, skewness, and glaze is faint in color, and crystalline substance spends tarnish, affects attractive in appearance.This formula adopts the ox bone ash of high-quality as main phase-splitting agent, makes crystalline glaze surface luster fine and smooth, makes to cool the spherical molten group formed and seems more clear bright, thus makes erythema crystalline substance flower artistic glaze Be very effective be better than similar crystalline product.
Simultaneously, the ceramic product that process for calcining of the present invention is produced, circular erythema crystalline substance flower is studded with in brown or tan glaze paint, reflect the radiance glittered under light illumination, there is strong stereoscopic sensation and artistic effect, have reserve value, both developed local characteristic product, increase this producing region pottery assortment, enrich again the market requirement.According to preresearch estimates, formula of the present invention and technique will increase by the income of more than 1,000,000 after going into operation to local manufacturing enterprises.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail, but do not form any limitation of the invention.
A kind of erythema crystalline glaze of the present invention, this glaze forms primarily of the raw material of following weight parts: albite 20 ~ 40 parts, 10 ~ 20 parts, quartz, burning 10 ~ 20 parts, talcum, 1 ~ 10 part, calcite, 10 ~ 25 parts, bone ash, 1 ~ 10 part, glass powder, barium carbonate 5 ~ 15 parts, ferric oxide 5 ~ 20 parts.Preferably, glaze forms primarily of the raw material of following weight parts: albite 25 ~ 35 parts, 10 ~ 15 parts, quartz, burning 10 ~ 15 parts, talcum, 2 ~ 8 parts, calcite, 10 ~ 20 parts, bone ash, 2 ~ 8 parts, glass powder, barium carbonate 5 ~ 10 parts, ferric oxide 10 ~ 15 parts.
Bone ash and Fe in formula
2o
3play vital effect, Fe
2o
3main crystallizing agent and tinting material, very big on the artistic effect impact of erythema crystalline substance flower artistic glaze, Fe
2o
3add-on optimum range is 12 ~ 15%, adds very little, and glaze paint does not have circular brilliant flower, the mottled mixed and disorderly distribution in yellow-green colour; Add too many, crystallization is easily linked to be sheet, skewness, and glaze is faint in color, and crystalline substance spends tarnish, affects attractive in appearance.
Meanwhile, the application adopts high-quality ox bone ash as main phase-splitting agent, the P in ox bone ash
2o
5can liquid-liquid separation be promoted, be conducive to forming the Continuous Liquid Phase of poor iron and the isolated liquid phase of Fu Tie.Crystalline glaze surface luster can be made fine and smooth containing higher CaO in ox bone ash simultaneously, make to cool the spherical molten group formed and seem more clear bright, thus make erythema crystalline substance flower artistic glaze Be very effective be better than similar crystalline product.
The present invention also controls by the rational proportion of ferric oxide and these two kinds of raw materials of talcum powder brilliant floral shape and the artistic effect that erythema crystalline substance spends artistic glaze, ferric oxide is main tinting material and crystallizing agent, also be the basis of formation two kinds of liquid phase separation, in the MgO that talcum powder provides and glaze, CaO composition forms CaO-Fe
2o
3-MgO ternary phase, CaO and MgO containing very strong crystallization ability, rationally adds Fe in crystalline glaze
2o
3, easily separate out α-Fe
2o
3, and then form the crystalline substance flower of circular rule, poor iron external phase and Fu Tie are isolated and balances each other, make erythema crystalline substance flower artistic glaze crystalline substance spend rule nature, the spot of other colors that undope.
Further, above-mentioned glaze also comprises the raw material of following weight parts: kaolin 0.5 ~ 2 part, Fluorspar Powder 0.3 ~ 2 part; Preferably, glaze also comprises the raw material of following weight parts: kaolin 0.8 ~ 1.5 part, Fluorspar Powder 0.5 ~ 1 part.
A small amount of interpolation Fluorspar Powder, fluorite had active fluxing capabilities and certain milkiness effect before melting temperature (1423 DEG C), erythema crystalline substance flower artistic glaze milkiness is not only made during a small amount of interpolation, can also contribute to improving glaze paint glossiness, simultaneously, the optical characteristics (as low in specific refractory power, dispersion is little) of fluorite can make the crystalline substance flower of erythema crystalline substance flower artistic glaze produce special opal effect, and the effect of the radiance that make to glitter is more obvious.
A kind of ceramic preparation adopting erythema crystalline glaze described in above-mentioned arbitrary claim of the present invention, comprises the steps:
(1) each raw material is taken by glaze formula, put into ball mill wet-milling, material during wet-milling: ball: the weight ratio of water is 1: 2: 0.6 ~ 1, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, glaze slip water ratio is 45 ~ 48%, old rear for subsequent use; The impact on erythema crystalline substance flower artistic glaze product of glaze fineness and glazing thickness is comparatively large, and glaze meticulous being unfavorable for forms nucleus, burns till rear glaze paint and only has several crystalline substances to spend at randomly to be distributed in glaze surface.Glazing is too thin, and the crystalline substance occurred is spent little, the crystalline substance flower size of not easily growing up needed for being formed, the artistic effect of the brilliant flower of impact.
(2) glazing on biscuit, glazing thickness is 0.8 ~ 1.2mm, carries out drying treatment after glazing; Biscuit is household china or display china base substrate, and 1250 DEG C ~ 1300 DEG C to burn till rear porcelain degree good, is applicable to erythema crystalline substance flower artistic glaze.
(3) dried base substrate loading of kiln is fired, when firing, from room temperature to 90 ~ 240 minutes 500 DEG C of used times, 60 ~ 120 minutes used times from 500 DEG C to 950 DEG C, 10 ~ 40 minutes used times from 950 DEG C to 1100 DEG C, 10 ~ 25 minutes used times from 1100 DEG C to 1200 DEG C, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C of 10 ~ 20 minutes used times, be incubated and be cooled to 1150 DEG C ~ 1180 DEG C after 10 ~ 50 minutes, be down to 1150 DEG C ~ 1180 DEG C 20 ~ 40 minutes used times and be incubated 20 ~ 120 minutes at 1150 DEG C ~ 1180 DEG C, last powered-down naturally cooling, whole firing time is 230 ~ 655 minutes.Calcining system has the greatest impact to the formation of erythema crystalline substance flower, the circle crystalline substance flower that the higher or on the low side all unfavorable formation of firing temperature is good, temperature drift, easy sagging forms the fancy glaze of yellow-green colour spot, firing temperature is on the low side, then brilliant flower is not full, and gradation sense is not strong, and easily form black sandstone glass mark, affect artistic effect equally.
Preferably, when firing, as the brilliant flower diameter 0.5mm-5mm of needs, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C, be incubated after 10-50 minute, be cooled to 1150 DEG C ~ 1160 DEG C and be incubated 20 ~ 60 minutes.
As the brilliant flower diameter 0.5cm-2cm of needs, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C, be incubated after 10-50 minute, be cooled to 1160 DEG C ~ 1180 DEG C and be incubated 60 ~ 120 minutes.
Embodiment 1
Glaze formula:
Albite 20 parts, 10 parts, quartz, burning 10 parts, talcum, 1 part, calcite, 10 parts, bone ash, 1 part, glass powder, barium carbonate 5 parts, ferric oxide 5 parts of, Gao Ling soil 0.5 part, Fluorspar Powder 0.3 part.
Preparation method:
(1) take each raw material by glaze formula, put into ball mill wet-milling, material during wet-milling: ball: the weight ratio of water is 1: 2: 0.6, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, and glaze slip water ratio is 45 ~ 48%, old rear for subsequent use;
(2) glazing on biscuit, glazing thickness is 0.8mm, carries out drying treatment after glazing;
(3) dried base substrate loading of kiln is fired, when firing, from room temperature to 90 minutes 500 DEG C of used times, 60 minutes used times from 500 DEG C to 950 DEG C, 10 minutes used times from 950 DEG C to 1100 DEG C, 10 minutes used times from 1100 DEG C to 1200 DEG C, 10 minutes used times from 1200 DEG C to 1250 DEG C, be incubated and be cooled to 1150 DEG C after 10 minutes, be down to 40 minutes 1150 DEG C of used times and 1150 DEG C of temperature 20 minutes, last powered-down naturally cooling, whole firing time is 250 minutes.The brilliant flower diameter 0.5mm of gained erythema.
Embodiment 2
Glaze formula:
Albite 25 parts, 10 parts, quartz, burning 10 parts, talcum, 2 parts, calcite, 12 parts, bone ash, 2 parts, glass powder, barium carbonate 8 parts, ferric oxide 10 parts of, Gao Ling soil 0.8 part, Fluorspar Powder 0.5 part.
Preparation method:
(1) take each raw material by glaze formula, put into ball mill wet-milling, material during wet-milling: ball: the weight ratio of water is 1: 2: 0.6, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, and glaze slip water ratio is 45 ~ 48%, old rear for subsequent use;
(2) glazing on biscuit, glazing thickness is 0.8mm, carries out drying treatment after glazing;
(3) dried base substrate loading of kiln is fired, when firing, from room temperature to 100 minutes 500 DEG C of used times, 75 minutes used times from 500 DEG C to 950 DEG C, 15 minutes used times from 950 DEG C to 1100 DEG C, 12 minutes used times from 1100 DEG C to 1200 DEG C, 12 minutes used times from 1200 DEG C to 1255 DEG C, be incubated and be cooled to 1160 DEG C after 25 minutes, be down to 35 minutes 1160 DEG C of used times and be incubated 60 minutes at 1160 DEG C, last powered-down naturally cooling, whole firing time is 334 minutes.The brilliant flower diameter 0.5cm of gained erythema.
Embodiment 3
Glaze formula:
Albite 30 parts, 12 parts, quartz, burning 12 parts, talcum, 5 parts, calcite, 15 parts, bone ash, 5 parts, glass powder, barium carbonate 10 parts, ferric oxide 12 parts.
Preparation method:
(1) take each raw material by glaze formula, put into ball mill wet-milling, material during wet-milling: ball: the weight ratio of water is 1: 2: 0.8, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, and glaze slip water ratio is 45 ~ 48%, old rear for subsequent use;
(2) glazing on biscuit, glazing thickness is 1mm, carries out drying treatment after glazing;
(3) dried base substrate loading of kiln is fired, when firing, from room temperature to 120 minutes 500 DEG C of used times, 90 minutes used times from 500 DEG C to 950 DEG C, 20 minutes used times from 950 DEG C to 1100 DEG C, 15 minutes used times from 1100 DEG C to 1200 DEG C, 10 minutes used times from 1200 DEG C to 1265 DEG C, be incubated and be cooled to 1155 DEG C after 40 minutes, be down to 30 minutes 1155 DEG C of used times and be incubated 30 minutes at 1155 DEG C, last powered-down naturally cooling, whole firing time is 355 minutes.The brilliant flower diameter 0.2cm of gained erythema.
Embodiment 4
Glaze formula:
Albite 35 parts, 15 parts, quartz, burning 15 parts, talcum, 8 parts, calcite, 20 parts, bone ash, 8 parts, glass powder, barium carbonate 12 parts, ferric oxide 15 parts of, Gao Ling soil 1.5 parts, Fluorspar Powder 1.5 parts.
Preparation method:
(1) take each raw material by glaze formula, put into ball mill wet-milling, material during wet-milling: ball: the weight ratio of water is 1: 2: 0.8, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, and glaze slip water ratio is 45 ~ 48%, old rear for subsequent use;
(2) glazing on biscuit, glazing thickness is 1.1mm, carries out drying treatment after glazing;
(3) dried base substrate loading of kiln is fired, when firing, from room temperature to 200 minutes 500 DEG C of used times, 105 minutes used times from 500 DEG C to 950 DEG C, 30 minutes used times from 950 DEG C to 1100 DEG C, 20 minutes used times from 1100 DEG C to 1200 DEG C, 15 minutes used times from 1200 DEG C to 1270 DEG C, be incubated and be cooled to 1170 DEG C after 45 minutes, be down to 25 minutes 1170 DEG C of used times and be incubated 90 minutes at 1170 DEG C, last powered-down naturally cooling, whole firing time is 530 minutes.The brilliant flower diameter 1cm of gained erythema.
Embodiment 5
Glaze formula:
Albite 40 parts, 20 parts, quartz, burning 20 parts, talcum, 10 parts, calcite, 25 parts, bone ash, 10 parts, glass powder, barium carbonate 15 parts, ferric oxide 20 parts of, Gao Ling soil 2 parts, Fluorspar Powder 2 parts
Preparation method:
(1) take each raw material by glaze formula, put into ball mill wet-milling, material during wet-milling: ball: the weight ratio of water is 1: 2: 1, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, and glaze slip water ratio is 45 ~ 48%, old rear for subsequent use;
(2) glazing on biscuit, glazing thickness is 1.2mm, carries out drying treatment after glazing;
(3) dried base substrate loading of kiln is fired, when firing, from room temperature to 240 minutes 500 DEG C of used times, 120 minutes used times from 500 DEG C to 950 DEG C, 40 minutes used times from 950 DEG C to 1100 DEG C, 25 minutes used times from 1100 DEG C to 1200 DEG C, 20 minutes used times from 1200 DEG C to 1280 DEG C, be incubated and be cooled to 1180 DEG C after 50 minutes, be down to 20 minutes 1180 DEG C of used times and be incubated 120 minutes at 1180 DEG C, last powered-down naturally cooling, whole firing time is 655 minutes.The brilliant flower diameter 2cm of gained erythema.
Claims (9)
1. an erythema crystalline glaze, it is characterized in that, this glaze forms primarily of the raw material of following weight parts: albite 20 ~ 40 parts, 10 ~ 20 parts, quartz, burning 10 ~ 20 parts, talcum, 1 ~ 10 part, calcite, 10 ~ 25 parts, bone ash, 1 ~ 10 part, glass powder, barium carbonate 5 ~ 15 parts, ferric oxide 5 ~ 20 parts.
2. a kind of erythema crystalline glaze according to claim 1, it is characterized in that, this glaze forms primarily of the raw material of following weight parts: albite 25 ~ 35 parts, 10 ~ 15 parts, quartz, burning 10 ~ 15 parts, talcum, 2 ~ 8 parts, calcite, 10 ~ 20 parts, bone ash, 2 ~ 8 parts, glass powder, barium carbonate 5 ~ 10 parts, ferric oxide 10 ~ 15 parts.
3. a kind of erythema crystalline glaze according to claim 1 and 2, it is characterized in that, this glaze also comprises the raw material of following weight parts: kaolin 0.5 ~ 2 part, Fluorspar Powder 0.3 ~ 2 part.
4. a kind of erythema crystalline glaze according to claim 3, it is characterized in that, this glaze also comprises the raw material of following weight parts: kaolin 0.8 ~ 1.5 part, Fluorspar Powder 0.5 ~ 1 part.
5. adopt a ceramic preparation for erythema crystalline glaze described in above-mentioned arbitrary claim, it is characterized in that, comprise the steps: that (1) takes each raw material by glaze formula, put into ball mill wet-milling and obtain glaze slip, old rear for subsequent use; (2) glazing on biscuit, glazing thickness is 0.8 ~ 1.2mm, carries out drying treatment after glazing; (3) dried base substrate loading of kiln is fired, when firing, from room temperature to 90 ~ 240 minutes 500 DEG C of used times, 1250 DEG C ~ 1280 DEG C are risen to rapidly after 1200 DEG C, soak is after 10 ~ 50 minutes, slowly be down to 1150 DEG C ~ 1180 DEG C and be incubated 20 ~ 120 minutes, last powered-down naturally cooling, whole firing time is 230 ~ 655 minutes.
6. ceramic preparation according to claim 5, it is characterized in that, material during step (1) described wet-milling: ball: the weight ratio of water is 1: 2: 0.6 ~ 1, grinding gained glaze slip fineness is crossed 200 ~ 300 mesh sieves and is tailed over and be less than 1%, and glaze slip water ratio is 45 ~ 48%.
7. ceramic preparation according to claim 5, it is characterized in that, in step (3), the concrete technology fired is from room temperature to 90 ~ 240 minutes 500 DEG C of used times, 60 ~ 120 minutes used times from 500 DEG C to 950 DEG C, 10 ~ 40 minutes used times from 950 DEG C to 1100 DEG C, 10 ~ 25 minutes used times from 1100 DEG C to 1200 DEG C, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C of 10 ~ 20 minutes used times, be incubated and be cooled to 1150 DEG C ~ 1180 DEG C after 10 ~ 50 minutes, be down to 20 ~ 40 minutes preset temperature used times and be incubated 20 ~ 120 minutes at preset temperature, last powered-down naturally cooling, whole firing time is 230 ~ 655 minutes.
8. ceramic preparation according to claim 7, is characterized in that, when firing, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C, be incubated after 10-50 minute, be cooled to 1150 DEG C ~ 1160 DEG C and be incubated 20 ~ 60 minutes.
9. ceramic preparation according to claim 7, is characterized in that, when firing, from 1200 DEG C to 1250 DEG C ~ 1280 DEG C, be incubated after 10-50 minute, be cooled to 1160 DEG C ~ 1180 DEG C and be incubated 60 ~ 120 minutes.
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