CN104445371A - 一种用于光催化的氧化锌纳米片材料及制备方法 - Google Patents
一种用于光催化的氧化锌纳米片材料及制备方法 Download PDFInfo
- Publication number
- CN104445371A CN104445371A CN201410685786.5A CN201410685786A CN104445371A CN 104445371 A CN104445371 A CN 104445371A CN 201410685786 A CN201410685786 A CN 201410685786A CN 104445371 A CN104445371 A CN 104445371A
- Authority
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- China
- Prior art keywords
- zinc oxide
- zinc
- preparation
- oxide nano
- filter paper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 title claims abstract description 76
- 239000011787 zinc oxide Substances 0.000 title claims abstract description 38
- 239000002135 nanosheet Substances 0.000 title claims abstract description 25
- 239000000463 material Substances 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 238000007146 photocatalysis Methods 0.000 title abstract description 8
- 230000001699 photocatalysis Effects 0.000 title abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 5
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000004246 zinc acetate Substances 0.000 claims abstract description 5
- 229910052984 zinc sulfide Inorganic materials 0.000 claims abstract 2
- 229960001296 zinc oxide Drugs 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 13
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 230000007613 environmental effect Effects 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- KGWDUNBJIMUFAP-KVVVOXFISA-N Ethanolamine Oleate Chemical compound NCCO.CCCCCCCC\C=C/CCCCCCCC(O)=O KGWDUNBJIMUFAP-KVVVOXFISA-N 0.000 claims description 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 3
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- -1 polyoxyethylene Polymers 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 238000003786 synthesis reaction Methods 0.000 claims 1
- 238000006731 degradation reaction Methods 0.000 abstract description 9
- 230000015556 catabolic process Effects 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 5
- STZCRXQWRGQSJD-GEEYTBSJSA-M methyl orange Chemical compound [Na+].C1=CC(N(C)C)=CC=C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 STZCRXQWRGQSJD-GEEYTBSJSA-M 0.000 abstract description 5
- 229940012189 methyl orange Drugs 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 3
- 239000002086 nanomaterial Substances 0.000 abstract description 2
- 239000002202 Polyethylene glycol Substances 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 239000002738 chelating agent Substances 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 229920001223 polyethylene glycol Polymers 0.000 abstract 1
- 239000010865 sewage Substances 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 description 4
- 239000011941 photocatalyst Substances 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- 238000013019 agitation Methods 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 238000006555 catalytic reaction Methods 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 238000005286 illumination Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 239000000987 azo dye Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 238000000870 ultraviolet spectroscopy Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- RNWHGQJWIACOKP-UHFFFAOYSA-N zinc;oxygen(2-) Chemical compound [O-2].[Zn+2] RNWHGQJWIACOKP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G9/00—Compounds of zinc
- C01G9/02—Oxides; Hydroxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/06—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of zinc, cadmium or mercury
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
- B01J35/39—Photocatalytic properties
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/30—Treatment of water, waste water, or sewage by irradiation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/90—Other properties not specified above
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2305/00—Use of specific compounds during water treatment
- C02F2305/10—Photocatalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (5)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410685786.5A CN104445371B (zh) | 2014-11-25 | 2014-11-25 | 一种用于光催化的氧化锌纳米片材料及制备方法 |
CN201610467003.5A CN106115766B (zh) | 2014-11-25 | 2014-11-25 | 一种高效降解染料的纳米材料的制备方法 |
Applications Claiming Priority (1)
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CN201410685786.5A CN104445371B (zh) | 2014-11-25 | 2014-11-25 | 一种用于光催化的氧化锌纳米片材料及制备方法 |
Related Child Applications (1)
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CN201610467003.5A Division CN106115766B (zh) | 2014-11-25 | 2014-11-25 | 一种高效降解染料的纳米材料的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN104445371A true CN104445371A (zh) | 2015-03-25 |
CN104445371B CN104445371B (zh) | 2016-07-13 |
Family
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Family Applications (2)
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CN201410685786.5A Expired - Fee Related CN104445371B (zh) | 2014-11-25 | 2014-11-25 | 一种用于光催化的氧化锌纳米片材料及制备方法 |
CN201610467003.5A Expired - Fee Related CN106115766B (zh) | 2014-11-25 | 2014-11-25 | 一种高效降解染料的纳米材料的制备方法 |
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CN201610467003.5A Expired - Fee Related CN106115766B (zh) | 2014-11-25 | 2014-11-25 | 一种高效降解染料的纳米材料的制备方法 |
Country Status (1)
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CN (2) | CN104445371B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104941625A (zh) * | 2015-07-01 | 2015-09-30 | 盐城工学院 | 一种黑色氧化锌及其制备方法 |
CN105428644A (zh) * | 2016-01-02 | 2016-03-23 | 红河学院 | 一种具有薄片状微观形貌的镍锰酸锂正极材料的制备方法 |
CN114570405A (zh) * | 2022-03-17 | 2022-06-03 | 西安工程大学 | 二维介孔氮化钽光催化材料的制备方法及应用 |
CN115845863A (zh) * | 2023-01-09 | 2023-03-28 | 辽宁大学 | 一种铬掺杂四氧化三钴光催化剂及其制备方法与应用 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100550355B1 (ko) * | 2003-11-06 | 2006-02-08 | (주)디오 | 글리콜을 이용한 산화아연의 제조방법 |
CN1970683A (zh) * | 2005-11-26 | 2007-05-30 | 中国科学院合肥物质科学研究院 | 具有紫外发光性能的氧化锌纳米片薄膜材料及其制备方法 |
CN103303966A (zh) * | 2013-06-13 | 2013-09-18 | 浙江大学 | 一种纤锌矿结构的氧化锌纳米片的制备方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1533985A (zh) * | 2003-03-31 | 2004-10-06 | 上海大学 | 一种纳米级氧化锌粉体的制备方法 |
CN100493696C (zh) * | 2005-10-27 | 2009-06-03 | 南京大学 | 掺杂纳米氧化锌及其制备方法和光催化降解有机物和抗菌的应用 |
JP2008254990A (ja) * | 2007-04-09 | 2008-10-23 | Ishihara Sangyo Kaisha Ltd | 酸化亜鉛及びその製造方法並びにそれを用いた化粧料 |
CN102515246B (zh) * | 2011-12-02 | 2013-12-04 | 南京林业大学 | 一种多孔纳米ZnO的制备方法 |
-
2014
- 2014-11-25 CN CN201410685786.5A patent/CN104445371B/zh not_active Expired - Fee Related
- 2014-11-25 CN CN201610467003.5A patent/CN106115766B/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100550355B1 (ko) * | 2003-11-06 | 2006-02-08 | (주)디오 | 글리콜을 이용한 산화아연의 제조방법 |
CN1970683A (zh) * | 2005-11-26 | 2007-05-30 | 中国科学院合肥物质科学研究院 | 具有紫外发光性能的氧化锌纳米片薄膜材料及其制备方法 |
CN103303966A (zh) * | 2013-06-13 | 2013-09-18 | 浙江大学 | 一种纤锌矿结构的氧化锌纳米片的制备方法 |
Non-Patent Citations (4)
Title |
---|
BAO WANG ET AL.: ""Filter paper—templated preparation of ZnO thin films and examination of their gas—sensing properties"", 《PARTICUOLOGY》 * |
GUODONG WEI ET AL.: ""Synthesis of ZnO Nanosheets by Microwave Thermal Vapor Method"", 《JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY》 * |
李洪峰等: ""以棉花为模板制备生物形态ZnO"", 《材料导报》 * |
杨立荣等: ""PEG辅助的溶胶凝胶法制备多孔ZnO薄膜"", 《功能材料与器件学报》 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104941625A (zh) * | 2015-07-01 | 2015-09-30 | 盐城工学院 | 一种黑色氧化锌及其制备方法 |
CN104941625B (zh) * | 2015-07-01 | 2018-01-23 | 盐城工学院 | 一种黑色氧化锌及其制备方法 |
CN105428644A (zh) * | 2016-01-02 | 2016-03-23 | 红河学院 | 一种具有薄片状微观形貌的镍锰酸锂正极材料的制备方法 |
CN114570405A (zh) * | 2022-03-17 | 2022-06-03 | 西安工程大学 | 二维介孔氮化钽光催化材料的制备方法及应用 |
CN114570405B (zh) * | 2022-03-17 | 2024-01-09 | 西安工程大学 | 二维介孔氮化钽光催化材料的制备方法及应用 |
CN115845863A (zh) * | 2023-01-09 | 2023-03-28 | 辽宁大学 | 一种铬掺杂四氧化三钴光催化剂及其制备方法与应用 |
CN115845863B (zh) * | 2023-01-09 | 2024-03-22 | 辽宁大学 | 一种铬掺杂四氧化三钴光催化剂及其制备方法与应用 |
Also Published As
Publication number | Publication date |
---|---|
CN104445371B (zh) | 2016-07-13 |
CN106115766B (zh) | 2017-08-29 |
CN106115766A (zh) | 2016-11-16 |
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Inventor after: Zhang Yanhua Inventor after: Liu Huang Inventor after: Xiao Wei Inventor after: Deng Ying Inventor after: Yang Hongtao Inventor after: Yu Hong Inventor after: Sun Lanlan Inventor after: Huang Lei Inventor before: Zhang Yanhua Inventor before: Liu Huang Inventor before: Xiao Wei Inventor before: Deng Ying Inventor before: Yu Hong Inventor before: Zhang Tiejun Inventor before: Sun Lanlan Inventor before: Huang Lei |
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