CN104311213A - Total nutrient liquid fertilizer containing amino acids, and preparation method thereof - Google Patents
Total nutrient liquid fertilizer containing amino acids, and preparation method thereof Download PDFInfo
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- CN104311213A CN104311213A CN201410477074.4A CN201410477074A CN104311213A CN 104311213 A CN104311213 A CN 104311213A CN 201410477074 A CN201410477074 A CN 201410477074A CN 104311213 A CN104311213 A CN 104311213A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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Abstract
A total nutrient liquid fertilizer containing amino acids comprises, by weights, 6-12 parts of N, 1-6 parts of P, 3-10 parts of K, 1-3 parts of Ca, 1-3 parts of Mg, 9-13 parts of Zn, 2-10 parts of Mn, 1-2 parts of B, 0.5-2 parts of Cu, 0.2-0.5 parts of Mo, 3-10 parts of Fe, 10-15 parts of amino acids, 1-10 parts of a plant growth regulator, 2-5 parts of an organic chelating agent and 30-40 parts of water. The liquid fertilizer provides comprehensive nutrition for plants, enhances the freeze, drought, salt and disease resistance of the plants, enhances the synthesis and translocation of substances in the plants, promotes the formation of adenosine triphosphate (ATP), promotes the photosynthesis and protein synthesis, induces the formation of chlorophyll, promotes the cell protoplasm flow, improves the cell vitality and accelerates the growth of the plants.
Description
Technical field
The present invention relates to a kind of fertilizer, the one particularly simultaneously containing the necessary macroelement of plant-growth, moderate-element, trace element and plant-growth regulator is containing amino acid whose total nutrient liquid fertilizer.
Technical background
Growth and development of plants needs macroelement, moderate-element and trace element.These nutritive elements are except passing through except soil, air and water supply on a small quantity, and major part needs to carry out supply by fertilising.But because existing chemical fertilizer is solid chemical fertilizer mostly, excessive using causes soil compaction, acid base imbalance with blindly applying fertilizer for a long time, and plant absorption nutrient speed slows down, and disease and pest generally occurs; A large amount of N P and K runs off and also causes widespread pollution from the overuse of fertilizers and pesticides in rural area serious, some areas deterioration of the ecological environment, the Sustainable development of serious restriction agriculture production.
Current, international fertilizer consumption is to high density, fluidization future development.Liquid Fertilizer is a kind of typical high concentration fertilizer, and in the country that irrigation technique and automatization fertilising are popularized, Liquid Fertilizer is widely used.U.S.'s Liquid Fertilizer accounts for 38% of whole fertilizer, and Liquid Fertilizer is almost all used in the field of Israel, and Australia, France, Germany, Spain, Romania etc. are all the countries widely applying Liquid Fertilizer.
Liquid Fertilizer contains the various nutritive elements needed for plant-growth, as nitrogen, phosphorus, potassium, calcium, magnesium, sulphur and trace element etc., also can add water-soluble organic substance (as humic acid, amino acid, Lalgine, plant-growth regulator etc.).Liquid Fertilizer has the plurality of advantages such as production cost is low, production environment is clean, formula easily adjustment, easy exploiting multifunctional fertilizers, easily some deliquescent materials of interpolation (as yellow humic acid, amino acid, chelated microelements etc.), nutrient content is high, easy to use, nontoxic, harmless, pollution-free, absorption rate is fast.
Summary of the invention
The object of this invention is to provide and a kind ofly meet the fertile containing amino acid total nutrient liquid of China's ecological circulation Economic development and ecological, environmental protective consciousness, improve edatope, supplement plant desired nutritional.
Product of the present invention contains a large amount of, the middle amounts such as nitrogen, phosphorus, potassium, calcium, magnesium, sulphur, zinc, manganese, iron, boron and micro-and amino acid, plant-growth regulator etc., uses conveniently, improves utilization rate of fertilizer, reduce environmental pollution.
One of the present invention is made up of following component containing amino acid whose total nutrient liquid fertilizer, is weight part:
6 ~ 12 parts, nitrogen, 1 ~ 6 part, phosphorus, 3 ~ 10 parts, potassium, calcium 1 ~ 3 part, 1 ~ 3 part, magnesium, 9 ~ 13 parts, zinc, 2 ~ 10 parts, manganese, boron 1 ~ 2 part, copper 0.5 ~ 2 part, molybdenum 0.2 ~ 0.5 part, iron 3 ~ 10 parts, amino acid/11 0 ~ 15 part, plant-growth regulator 1 ~ 10 part, organic sequestering agent 2 ~ 5 parts, 30 ~ 40 parts, water.
Described a kind of PH containing amino acid whose total nutrient liquid fertilizer is 3 ~ 9.
Described nitrogen is one or more in urea, ammonium nitrate, ammonium chloride, saltpetre, primary ammonium phosphate; Phosphorus is one or more in potassium primary phosphate, primary ammonium phosphate, calcium phosphate; Potassium is one or more in potassium primary phosphate, saltpetre, Repone K.
Calcium is one or more in nitrocalcite, calcium phosphate, EDTA calcium.
Magnesium is that magnesium sulfate is or/and in magnesium chloride.
Described zinc is that zinc sulfate is or/and zinc chloride; Manganese is that manganous sulfate is or/and Manganous chloride tetrahydrate; Boron is that borax is or/and boric acid; Copper is that cupric sulfate pentahydrate is or/and dried cupric sulfate; Molybdenum is that ammonium molybdate is or/and Sodium orthomolybdate; Iron is one or more in ferrous sulfate, ferrous ammonium sulphate, NaFeEDTA.
Described plant-growth regulator is that brassinolide is or/and sodium nitrophenolate.
Described organic sequestering agent is selected from one or more in ethylenediamine tetraacetic acid (EDTA) (sodium), citric acid, glycine, L-glutamic acid, tartrate etc.
A kind of preparation method containing amino acid whose total nutrient liquid fertilizer of the present invention, concrete steps are as follows:
1) in massfraction, by the mixing of the water of the organic sequestering agent of 2 ~ 5 parts, the manganese of 2 ~ 10 parts, the zinc of 9 ~ 13 parts, the copper of 0.5 ~ 2 part, the aminoacids complex of 10 ~ 15 parts and 30 ~ 40 parts, stirring is carried out being obtained by reacting mixing solutions, makes manganese, zinc, copper be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium of the iron of 1 ~ 6 part, the boron of 1 ~ 2 part, the molybdenum of 0.2 ~ 0.5 part and 1 ~ 3 part in the mixing solutions obtained in step 1), be uniformly mixed and make solution;
3) in step 2) add the plant-growth regulator of the nitrogen of 6 ~ 12 parts, the phosphorus of 1 ~ 6 part, the potassium of 3 ~ 10 parts, the calcium of 1 ~ 3 part and 1 ~ 10 part in the solution that obtains, be uniformly mixed, filter, obtain a kind of fertile containing amino acid whose total nutrient liquid.
Temperature of reaction described in step 1) is 20 ~ 60 DEG C, and the described reaction times is 0.5 ~ 2.5 hour.
Total amount >=80 grams per liter of described a kind of nitrogen, phosphorus and potassium element containing containing in amino acid whose total nutrient liquid fertilizer; Total amount >=25 grams per liter of the calcium contained, magnesium and element sulphur; Total amount >=30 grams per liter of the zinc contained, manganese, boron, iron, copper and molybdenum element; Amino acid >=100 grams per liter contained; Plant-growth regulator >=10 grams per liter contained.
Usage quantity of the present invention uses according to the mode water distribution of weight ratio, is respectively: foliage-spray: dilution 800-1000 times, seedling stage, vegetative period, SPRING WHEAT BEFORE AND AFTER FLOWERING, and fruit development period all can spray, and every 7-15 days sprays 1 time, sprays 2-4 time altogether; Brushing trunk: dilution 100-200 doubly; Fill with root: dilution 2000-3000 doubly.
One of the present invention is the Liquid Fertilizer that one is rich in macroelement (nitrogen, phosphorus and potassium), moderate-element (calcium, magnesium and sulphur), trace element (zinc, manganese, boron, iron, copper and molybdenum), amino acid and plant-growth regulator containing amino acid whose total nutrient liquid fertilizer, and this Liquid Fertilizer provides the whole nutrition needed for plant.One of the present invention is a kind of nontoxic, harmless, free of contamination green and protecting environmental fertilizer containing amino acid whose total nutrient liquid fertilizer, and can be applicable to various plants, is a kind of broad spectrum type fertilizer.One of the present invention not only can provide comprehensive nutrition for plant containing amino acid whose total nutrient liquid fertilizer, strengthen freeze proof, the drought resisting of plant, anti-salt and diseases and insect pests resistance, synthesis and the running of plant substance in vivo can also be strengthened, promote the formation of adenosine triphyosphate ATP, promote photosynthesis and protein synthesis, induce chlorophyllous formation, promote cellular plasm flowing, improve cell viability, accelerate vine growth and development etc.Preparation method's technique of the present invention is simple, easy and simple to handle, and can effectively avoid reacting between each component in fertilizer and producing precipitation, can long-term storage, also can with other combined use of pesticides.
Embodiment
embodiment 1
1) by the mixing of the water of the ethylenediamine tetraacetic acid (EDTA) of 3 kilograms, the manganous sulfate of 4 kilograms, the zinc sulfate of 11 kilograms, the copper sulfate of 1 kilogram, the aminoacids complex of 12.5 kilograms and 38 kilograms, at temperature of reaction is 40 ~ 50 DEG C, is uniformly mixed 1.5 hours, makes manganous sulfate, zinc sulfate, copper sulfate be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium sulfate of the NaFeEDTA of raw material 3 kilograms, the boric acid of 1 kilogram, the ammonium molybdate of 0.3 kilogram and 2 kilograms in the mixing solutions obtained in step 1), be uniformly mixed reaction and make solution in 1 hour;
3) in step 2) add the urea of raw material 9 kilograms, 3 kilograms of potassium primary phosphates, 3 kilograms of saltpetre, the EDTA calcium of 2 kilograms and brassinolide of 7 kilograms in the solution that obtains, after being uniformly mixed, filter, obtain containing amino acid whose total nutrient liquid fertile.
embodiment 2
1) by the mixing of the water of the sodium ethylene diamine tetracetate of 3.5 kilograms, the manganous sulfate of 6 kilograms, the zinc sulfate of 10 kilograms, the copper sulfate of 1 kilogram, the aminoacids complex of 13 kilograms and 36 kilograms, at temperature of reaction is 40 ~ 50 DEG C, is uniformly mixed 1.5 hours, makes manganous sulfate, zinc sulfate, copper sulfate be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium sulfate of the ferrous sulfate of raw material 2 kilograms, the boric acid of 1 kilogram, the Sodium orthomolybdate of 0.2 kilogram and 2 kilograms in the mixing solutions obtained in step 1), be uniformly mixed reaction and make solution in 1 hour;
3) in step 2) add the ammonium nitrate of raw material 11 kilograms, 3 kilograms of potassium primary phosphates, 3 kilograms of saltpetre, the EDTA calcium of 2 kilograms and brassinolide of 6 kilograms in the solution that obtains, after being uniformly mixed, filter, obtain containing amino acid whose total nutrient liquid fertile.
embodiment 3
1) by the mixing of the water of the ethylenediamine tetraacetic acid (EDTA) of 3 kilograms, the Manganous chloride tetrahydrate of 3 kilograms, the zinc sulfate of 10 kilograms, the copper sulfate of 1 kilogram, the aminoacids complex of 12 kilograms and 38 kilograms, at temperature of reaction is 40 ~ 50 DEG C, is uniformly mixed 1.5 hours, makes manganous sulfate, zinc sulfate, copper sulfate be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium sulfate of the NaFeEDTA of raw material 3 kilograms, the borax of 1.5 kilograms, the ammonium molybdate of 0.2 kilogram and 2.5 kilograms in the mixing solutions obtained in step 1), be uniformly mixed reaction and make solution in 1 hour;
3) in step 2) add the urea of raw material 10 kilograms, 3 kilograms of potassium primary phosphates, 2.5 kilograms of saltpetre, the nitrocalcite of 2.5 kilograms and brassinolide of 8 kilograms in the solution that obtains, after being uniformly mixed, filter, obtain containing amino acid whose total nutrient liquid fertile.
embodiment 4
1) by the mixing of the water of the sodium ethylene diamine tetracetate of 3.5 kilograms, the manganous sulfate of 5 kilograms, the zinc sulfate of 10 kilograms, the copper sulfate of 1.5 kilograms, the aminoacids complex of 15 kilograms and 40 kilograms, at temperature of reaction is 50 ~ 55 DEG C, is uniformly mixed 1 hour, makes manganous sulfate, zinc sulfate, copper sulfate be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium chloride of the NaFeEDTA of raw material 2 kilograms, the borax of 1 kilogram, the ammonium molybdate of 0.2 kilogram and 2 kilograms in the mixing solutions obtained in step 1), be uniformly mixed reaction and make solution in 1 hour;
3) in step 2) add the ammonium nitrate of raw material 12 kilograms, 3 kilograms of potassium primary phosphates, 2.5 kilograms of saltpetre, the EDTA calcium of 1.5 kilograms and sodium nitrophenolates of 2 kilograms in the solution that obtains, after being uniformly mixed, filter, obtain containing amino acid whose total nutrient liquid fertile.
embodiment 5
1) by the mixing of the water of the ethylenediamine tetraacetic acid (EDTA) of 2.5 kilograms, the manganous sulfate of 6 kilograms, the zinc chloride of 9 kilograms, the copper sulfate of 1.5 kilograms, the aminoacids complex of 14 kilograms and 39 kilograms, at temperature of reaction is 50 ~ 55 DEG C, is uniformly mixed 1 hour, makes manganous sulfate, zinc sulfate, copper sulfate be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium sulfate of the NaFeEDTA of raw material 3 kilograms, the boric acid of 1 kilogram, the ammonium molybdate of 0.3 kilogram and 2.5 kilograms in the mixing solutions obtained in step 1), be uniformly mixed reaction and make solution in 1 hour;
3) in step 2) add the urea of raw material 9 kilograms, 3 kilograms of potassium primary phosphates, 3 kilograms of saltpetre, the nitrocalcite of 3 kilograms and sodium nitrophenolates of 3 kilograms in the solution that obtains, after being uniformly mixed, filter, obtain containing amino acid whose total nutrient liquid fertile.
embodiment 6
1) by the mixing of the water of the ethylenediamine tetraacetic acid (EDTA) of 3 kilograms, the manganous sulfate of 7 kilograms, the zinc sulfate of 9 kilograms, the copper sulfate of 1 kilogram, the aminoacids complex of 15 kilograms and 39 kilograms, at temperature of reaction is 50 ~ 55 DEG C, is uniformly mixed 1 hour, makes manganous sulfate, zinc sulfate, copper sulfate be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium chloride of the NaFeEDTA of raw material 5 kilograms, the borax of 1 kilogram, the Sodium orthomolybdate of 0.2 kilogram and 2 kilograms in the mixing solutions obtained in step 1), be uniformly mixed reaction and make solution in 1 hour;
3) in step 2) add the urea of raw material 9 kilograms, 3 kilograms of potassium primary phosphates, 3 kilograms of saltpetre, the EDTA calcium of 1 kilogram and sodium nitrophenolates of 2 kilograms in the solution that obtains, after being uniformly mixed, filter, obtain containing amino acid whose total nutrient liquid fertile.
The usage quantity of this product uses according to the mode water distribution of weight ratio, is respectively: foliage-spray: dilution 800-1000 times, seedling stage, vegetative period, SPRING WHEAT BEFORE AND AFTER FLOWERING, and fruit development period all can spray, and every 7-15 days sprays 1 time, sprays 2-4 time altogether; Brushing trunk: dilution 100-200 doubly; Fill with root: dilution 2000-3000 doubly.
Manure trial:
We choose using Chinese sorghum, paddy rice, citrus, corn containing amino acid whose total nutrient liquid fertilizer obtained by embodiment 1, meanwhile, we also adopt commercially available liquid fertilizer that Chinese sorghum, paddy rice, citrus, corn are carried out to the contrast of corresponding fertilizer efficiency and use (abbreviation control group).
Application process: foliage-spray: dilution 800-1000 times, seedling stage, vegetative period, SPRING WHEAT BEFORE AND AFTER FLOWERING, fruit development period all sprays, and every 7-15 days sprays 1 time, sprays 2-4 time altogether; Brushing trunk: dilution 100-200 doubly; Fill with root: dilution 2000-3000 doubly.
Pass through Experimental Comparison, spray obtained by embodiment 1 at Chinese sorghum seedling stage, jointing stage, full heading time and grouting parameter fertile containing amino acid whose total nutrient liquid, after using 20 days seedling stage, comparatively control group phase specific root length increases 3.19cm, plant height increases 3.60cm, root heavily increases 0.031g, and stem heavily increases 0.031g, and leaf heavily increases 0.058g.Mu increases fine strain of millet 55kg, stimulation ratio 10.9%, and disease and pest incidence is starkly lower than contrast.
Fertile containing amino acid whose total nutrient liquid what rice seedling phase, tillering phase, boot stage and heading stage use obtained by embodiment 1, compared with control group, paddy rice seedling-slowing stage shortens, effective tillering increases, the percentage of earbearing tiller improves, and thousand seed weight increases, and per mu yield increases 75kg, stimulation ratio 13.27%, disease and pest incidence is starkly lower than contrast.
Citrus trees sprays obtained by embodiment 1 containing after amino acid whose total nutrient liquid fertilizer, comparatively control group is compared, leaf look becomes dark green, tree vigo(u)r obviously strengthens, citrus physiological fruit drop obviously reduces, fruit-setting rate improves 1.5 ~ 4.1 percentage points, and output significantly increases, and fruit shape index, peel thickness have reduction trend.
Spray obtained by embodiment 1 at Maize at Seedling Stage and vegetative period fertile containing amino acid whose total nutrient liquid, compared with control group, bald sharp phenomenon is light, full seed, and grain number per spike increases by 10.8, and thousand seed weight increases 8.7g, and per mu yield increases 28.3kg, stimulation ratio 5.8%.
We have also been made identical manure trial to embodiment 2-6, and its test-results and embodiment 1 manure trial test-results there is no significant difference, therefore no longer do deposited stating to the manure trial of embodiment 2-6 at this.
Claims (9)
1. one kind contains amino acid whose total nutrient liquid fertilizer, it is characterized in that, counts by weight ratio, described Liquid Fertilizer is composed of the following components: 6 ~ 12 parts, nitrogen, 1 ~ 6 part, phosphorus, 3 ~ 10 parts, potassium, calcium 1 ~ 3 part, 1 ~ 3 part, magnesium, 9 ~ 13 parts, zinc, 2 ~ 10 parts, manganese, boron 1 ~ 2 part, copper 0.5 ~ 2 part, molybdenum 0.2 ~ 0.5 part, iron 3 ~ 10 parts, amino acid/11 0 ~ 15 part, plant-growth regulator 1 ~ 10 part, organic sequestering agent 2 ~ 5 parts, 30 ~ 40 parts, water.
2. one according to claim 1 is fertile containing amino acid whose total nutrient liquid, it is characterized in that, total amount >=80 grams per liter of described nitrogen, phosphorus and potassium element; Total amount >=25 grams per liter of calcium, magnesium and element sulphur; Total amount >=30 grams per liter of zinc, manganese, boron, iron, copper and molybdenum element; Amino acid >=100 grams per liter; Plant-growth regulator >=10 grams per liter.
3. one according to claim 1 is fertile containing amino acid whose total nutrient liquid, and it is characterized in that, described nitrogen is one or more in urea, ammonium nitrate, ammonium chloride, saltpetre, primary ammonium phosphate; Phosphorus is one or more in potassium primary phosphate, primary ammonium phosphate, calcium phosphate; Potassium is one or more in potassium primary phosphate, saltpetre, Repone K.
4. one according to claim 1 is fertile containing amino acid whose total nutrient liquid, and it is characterized in that, described calcium is one or more in nitrocalcite, calcium phosphate, EDTA calcium; Magnesium is that magnesium sulfate is or/and magnesium chloride.
5. one according to claim 1 is fertile containing amino acid whose total nutrient liquid, and it is characterized in that, described zinc is that zinc sulfate is or/and zinc chloride; Manganese is that manganous sulfate is or/and Manganous chloride tetrahydrate; Boron is that borax is or/and boric acid; Copper is that cupric sulfate pentahydrate is or/and dried cupric sulfate; Molybdenum is that ammonium molybdate is or/and Sodium orthomolybdate; Iron is one or more in ferrous sulfate, ferrous ammonium sulphate, NaFeEDTA.
6. one according to claim 1 and 2 is fertile containing amino acid whose total nutrient liquid, and it is characterized in that, described plant-growth regulator is that brassinolide is or/and sodium nitrophenolate.
7. one according to claim 1 is fertile containing amino acid whose total nutrient liquid, and it is characterized in that, described organic sequestering agent is selected from one or more in ethylenediamine tetraacetic acid (EDTA) (sodium), citric acid, glycine, L-glutamic acid, tartrate etc.
8., containing a preparation method for amino acid whose total nutrient liquid fertilizer, it is characterized in that, described preparation method comprises the following steps:
1) in massfraction, by the mixing of the water of the organic sequestering agent of 2 ~ 5 parts, the manganese of 2 ~ 10 parts, the zinc of 9 ~ 13 parts, the copper of 0.5 ~ 2 part, the amino acid of 10 ~ 15 parts and 30 ~ 40 parts, stirring is carried out being obtained by reacting mixing solutions, makes manganese, zinc, copper be dissolved into the mixing solutions of Chelating state manganese, zinc, copper completely;
2) add the magnesium of the iron of 1 ~ 6 part, the boron of 1 ~ 2 part, the molybdenum of 0.2 ~ 0.5 part and 1 ~ 3 part in the mixing solutions obtained in step 1), be uniformly mixed and make solution;
3) in step 2) add the plant-growth regulator of the nitrogen of 6 ~ 12 parts, the phosphorus of 1 ~ 6 part, the potassium of 3 ~ 10 parts, the calcium of 1 ~ 3 part and 1 ~ 10 part in the solution that obtains, be uniformly mixed, filter, obtain a kind of fertile containing amino acid whose total nutrient liquid.
9. one according to claim 8 is fertile containing amino acid whose total nutrient liquid, and it is characterized in that, the temperature of reaction described in step 1) is 20 ~ 60 DEG C, and the described reaction times is 0.5 ~ 2.5 hour.
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