CN102775251A - Water-soluble humic acid grape special fertilizer and production method thereof - Google Patents

Water-soluble humic acid grape special fertilizer and production method thereof Download PDF

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Publication number
CN102775251A
CN102775251A CN2012102909325A CN201210290932A CN102775251A CN 102775251 A CN102775251 A CN 102775251A CN 2012102909325 A CN2012102909325 A CN 2012102909325A CN 201210290932 A CN201210290932 A CN 201210290932A CN 102775251 A CN102775251 A CN 102775251A
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water
soluble
acid
special fertilizer
parts
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高进华
周丽
李元峰
解学仕
孙士俊
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STANLEY FERTILIZER STOCK CO Ltd
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STANLEY FERTILIZER STOCK CO Ltd
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Abstract

The invention discloses a water-soluble humic acid grape special fertilizer and relates to the technical field of water-soluble fertilizers. The special fertilizer comprises the following raw materials in parts by weight: 3-10 parts of water-soluble humic acid, 20-70 parts of urea, 25-60 parts of water-soluble monoammonium phosphate, 20-50 parts of water-soluble potassium sulfate and 0.5-1.5 parts of EDTA chelate trace element; and the spray granulation technology of a granulation tower is adopted for granulation to obtain the water-soluble humic acid grape special fertilizer. Compared with the prior art, the special fertilizer disclosed by the invention has the advantages of high nutrient content, comprehensive nutrition and high utilization rate of fertilizers, and can obviously improve the output and quality of grape.

Description

A kind of fulvo acid grape special fertilizer and working method thereof
Technical field
The present invention relates to the water soluble fertilizer technical field, particularly relate to a kind of water-soluble grape special fertilizer.
Background technology
Grape is the perennial vine crop of Vitaceae Vitis, and in global fruit was produced, it is the first that the output of grape and cultivated area occupy always.Grape is not only delicious good to eat, and nutritive value is very high, and sugar degree is main up to 10%-30% with glucose in the sophisticated berry, can directly be absorbed by human body, also contains mineral calcium, potassium, phosphorus, iron and multivitamin, and multiple essential amino acid.
Thank to researchs such as Jianchang and show that the Daze Mount vintage that is grown on the brunisolic soil is 18t/hm 2, per hectare nutrition absorption amount is nitrogen (N) 138kg, phosphorus (P 2O 5) 105 kg, potassium (K 2O) 225 kg, its assimilation ratio are 1:0.8:1.6.Grape has the trend above the potassium absorbed dose to the absorbed dose of calcium in the data of Fregoni (1984).Therefore, grape high-yield is calcium>potassium>nitrogen>phosphorus to the demand of nutrition.
Because grape variety is various, need fertile performance different, add that the requirement of yield per unit is different, grape science fertilizer practice requires reasonably to confirm dose, according to the victory researchs such as (2001) of horse, 1000 m 2The vineyard produces 1500 kg grapes, absorbed nitrogen (N) 8.84 ㎏, phosphorus (P 2O 5) 4.15 ㎏, potassium (K 2O) 10.23 ㎏, the ratio of absorbed nitrogen phosphorus potassium is 1:0.47:1.16.Yang Zhiyuan (2008) thinks; It is leading indicator with the growth potential that grape variety needs fertile characteristic; The prosperous kind of growing way is Shaoshi fertilizer suitably, and growing way kind on the weak side then can suitable many fertilises, and the applicating ratio of nitrogen phosphorus potassium is with 1:0.8 ~ 1:1 ~ 1.2 (the moderate-yield 1500kg/667 m that is advisable 2).
At present, mainly there are following three problems in common fertilizer concerning grape:
1, the common fertilizer life-time service can make soil become to harden, and the crumb structure of soil is destroyed serious, and the grape quality obviously descends, and the more important thing is the havoc ecotope.
2, the common fertilizer nutrient element releasing rule can't match with the grape law of nutritive absorption, and utilization rate of fertilizer is low.
3, orchard worker's fertilising is main with the experience fertilising often, and cost is higher, and causes Soil structure and environment to be damaged, and the crop anti-adversity ability descends.
Develop rapidly for adapting to current water-saving agriculture, exploitation meets nuisanceless production requirement, reach improve the soil, promote fertilizer efficiency, promote growth, degeneration-resistant and to improve the high level of water soluble fertilizer of crop yield and quality just necessary.The applicant combines the regulation of fertilizer requirement and the characteristics of grape simultaneously through surveying the soil prescription, has researched and developed a kind of fulvo acid grape special fertilizer, has proposed a new thinking for addressing the above problem.
Summary of the invention
To the deficiency of prior art, the object of the present invention is to provide a kind of good water solubility, green non-pollution, utilization rate of fertilizer high, improve the soil, culture fertility and can be applied to grape special fertilizer and working method thereof with the water fertilising.
A kind of fulvo acid grape special fertilizer of the present invention, the feed composition weight part is following:
Fulvo acid 3-10 part,
Urea 20-70 part,
Water-soluble phosphoric acid one ammonium 25-60 part,
Water-soluble vitriolate of tartar 20-50 part,
EDTA chelated microelement 0.5-1.5 part;
Above raw material is the commercially available prod, wherein:
Described fulvo acid is yellow humic acid sylvite, yellow humic acid ammonium salt or wherein a kind of, belongs to water-soluble macromolecular organic compound, specification of quality: water-soluble >=90%, humic acids content >=60%;
Said urea is small particle urea, and nitrogen content >=46.2%, particle diameter are 0.85mm-2.80mm;
Said water-soluble phosphoric acid one ammonium nitrogen content is 12%, and phosphorus pentoxide content is 61%;
Potassium oxide content is 52% in the said water-soluble vitriolate of tartar;
Said EDTA chelated microelement is the mixture more than two kinds in EDTA chelating calcium, EDTA chelated magnesium, the EDTA chelating zinc, is Powdered;
The content that relates in the above raw material is mass percent.
The preparation method of a kind of fulvo acid grape special fertilizer of the present invention:
In the fused solution of urea and monoammonium phosphate, allocate vitriolate of tartar into through heating; Add humic acids and trace element then; It is mixed with fused solution, under the temperature of fusion self and mechanical agitation, be combined into low temperature eutectic rapidly, adopt prilling tower sprinkling pelleting technology to carry out granulation then with certain flowing property; In the process that in prilling tower, falls of spray tear drop, carry out heat exchange and cool off rapidly and solidifies acquisition fulvo acid grape special fertilizer with the airflow that rises.
The technical indicator of fulvo acid grape special fertilizer product of the present invention: humic acids>=3.0%, N+P 2O 5+ K 2O>=45%, trace element>=0.5%, water-insoluble≤2%, moisture≤2%.
A kind of fulvo acid grape special fertilizer of the present invention, further preferred feed composition weight part is following:
Fulvo acid 3.5-8 part,
Urea 30-50 part,
Water-soluble phosphoric acid one ammonium 30-45 part,
Water-soluble vitriolate of tartar 25-35 part,
EDTA chelated microelement 0.5-1 part.
A kind of fulvo acid grape special fertilizer of the present invention, most preferred feed composition weight part is following:
3.5 parts of fulvo acids,
31 parts in urea,
30 parts of water-soluble phosphoric acid one ammoniums,
35 parts of water-soluble vitriolate of tartar,
0.5 part of EDTA chelated microelement.
Grape special fertilizer of the present invention has the following advantages:
1, grape special fertilizer nutrient content of the present invention is high, nutrition is complete; Contain organic matter, nitrogen, phosphorus, potassium and various trace elements, can make the balanced coordination of crop alimentary, can not only significantly improve crop yield and quality; And the quantity that can effectively increase soil microorganisms is with active; Be in the nutrient element of stationary state in the activating soil, improve the soil, culture fertility.
2, grape special fertilizer of the present invention can promote grape fruit ripe; Increase grape sugar degree and soluble solid content, reduce total acid content, obviously improve the taste of grape; Improve simultaneously that it is cold-resistant, the ability of drought resisting, high temperature resistant and disease-resistant worm, thereby improve vintage and quality.
3, product of the present invention product good water solubility of the present invention, solubility>=98%, impurity is few, water-insoluble≤2%, utilization rate of fertilizer is high, and the comparable conventional fertilizer application consumption of fertilizer amount reduces 10-20%, and saving of work and time is practiced thrift cost.
Embodiment
Below in conjunction with embodiment the present invention is elaborated, but protection scope of the present invention is not only for so.
Embodiment 1: preparation fulvo acid grape special fertilizer, nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide content are respectively 18%, 18%, 18%, are mass percent.
The feed composition weight part is following:
3.5 parts of fulvo acids,
31 parts in urea,
30 parts of water-soluble phosphoric acid one ammoniums,
35 parts of water-soluble vitriolate of tartar,
0.5 part of EDTA chelated microelement.
The preparation method:
Urea mix with monoammonium phosphate melt altogether after; Mix with vitriolate of tartar, humic acids and EDTA chelated microelement again; Formation has the low temperature eutectic of certain flowing property; Carry out the prilling tower sprinkling pelleting then, carry out heat exchange and rapid cooling curing with the airflow that rises in the process that the spray tear drop falls in prilling tower, just process the fulvo acid grape special fertilizer.
The fertilizing method of grape special fertilizer of the present invention:
(1) with dissolving in this fertilizer adding container of fertilizer;
(2) inject fertilizer solution in the middle period of drip irrigation perdurability, the earlier little back of Open valve is big, and IR is few as far as possible, keeps evenly;
(3) can suitably the fertile consumption of drip irrigation be adjusted according to the growing way of crop.
In addition,, confirm the fertilizer nutrient proportioning of each breeding time and use quantity, rich water to advance together according to soil supplying nutrient capability, crop regulation of fertilizer requirement and target output, on a small quantity repeatedly, to satisfy the growth needs of crop. 
Embodiment 2: preparation fulvo acid grape special fertilizer, nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide content are respectively 17%, 15%, 20%, are mass percent.
The feed composition weight part is following:
4 parts of fulvo acids,
30 parts in urea,
25 parts of water-soluble phosphoric acid one ammoniums,
40 parts of water-soluble vitriolate of tartar,
1 part of EDTA chelated microelement.
Preparation technology and fertilizing method are with embodiment 1.
Comparative Examples 1: common NPK, specification are 18-18-18, Stanley Fertilizer Co.,Ltd's production and sales.
Comparative Examples 2: common NPK, specification are 17-15-20, Stanley Fertilizer Co.,Ltd's production and sales.
The effect of above embodiment 1,2 and Comparative Examples is following:
Test period: in April, 2011 ~ October.
Test place: in the demonstration vineyard, base, the agrotechnical center of Turfan Prefecture.
Experimental cultivar: local main breed thompson seedless grape.
Supply examination soil: silty loam, pH value are 8.1, organic matter 1.2, full nitrogen 0.161%, alkali-hydrolyzable nitrogen 79.52mg/kg, full phosphorus 0.093%, rapid available phosphorus 15.4mg/kg, available potassium 128.96mg/kg, full potassium 0.273%.
TP: 4 processing, every processing repetition 3 times are established in test altogether.
1. Comparative Examples 1: common NPK (specification is 18-18-18);
2. Comparative Examples 2: common NPK (specification is 17-15-20);
3. embodiment 1: fulvo acid grape special fertilizer (specification is 18-18-18);
4. embodiment 2: fulvo acid grape special fertilizer (specification is 17-15-20);
Above-mentioned fertilizer is Stanley Fertilizer Co.,Ltd and produces.
Totally 6 sub-districts, each sub-district random alignment, the uniform grape of 24 pier growing ways is selected in each sub-district, establishes guard rows, oozes when preventing to water, leaks, sub-district area S=181.3m 2April 7 applied fertilizer to each processing according to TR.
Experimental field grape germinateed April 21, and May 25 bloomed, May 15, intertillage on July 20; April 7, June 2, June 28, July 31 water; April 30, May 20, July 26 prune 3 times, spray medicine control in June 27 grape leafhopper, results at the beginning of 10 months.
Each fruit ear of handling of clip and really grain at random; It is heavy heavy with fringe to measure grain with electronic balance, with the hand-held saccharous detector mensuration of WYT type soluble solid content, with Coomassie brilliant blue G250 method survey soluble protein content; Survey titratable acid content with acid, survey Vitamin C content with ultraviolet light absorption method.Utilize Excel, DPS software that experimental data is carried out significance of difference analysis.
Experimental result is seen table 1, table 2.
Table 1 different fertilizer is handled the influence to vintage
Handle Grain heavy (g) Fringe heavy (g) Output (kg/hm 2
Comparative Examples 1 12.34B 622.12C 29860C
Comparative Examples 2 12.29B 621.87C 29764C
Embodiment 1 15.45A 863.10A 39562A
Embodiment 2 13.89AB 748.68B 35892B
Annotate: different letter representations reach 1% level of signification in the table, down together.
Table 2 different fertilizer is handled the influence to grape quality
Figure 523785DEST_PATH_IMAGE002
Experiment shows, under the fertilizer level of equal nutrient (NPK content >=50%), uses fulvo acid grape special fertilizer of the present invention, and grape leave is abundant, dark green leaf color, well developed root system, and resistance against diseases is strong.Can find out by table 1; After the fulvo acid grape special fertilizer is handled; The grain of different treatment weighs and the fringe weight average is higher than Comparative Examples; The averageparticle that embodiment 1, embodiment 2 handle increases 3.11g, 1.6g than Comparative Examples 1, Comparative Examples 2 heavily respectively, and average fringe increases 240.98g, 126.81g heavily respectively, and mean yield increases by 9702 kg/hm respectively 2, 6128 kg/hm 2, through measuring and calculating, administration of water soluble humic acids grape special fertilizer can increase production 20.5%-32.4%.Wherein, the amplification that embodiment 1 (specification is 18-18-18) handles is maximum, reaches utmost point level of signification.
Can find out that by table 2 after the fulvo acid grape special fertilizer was handled, the soluble solid content of different treatment, soluble proteins, Vitamin C content all were higher than Comparative Examples; And the content of titratable acid all is lower than Comparative Examples; After administration of water soluble humic acids grape special fertilizer is described, can increase the sugar degree and the soluble solid content of grape, reduce total acid content; Can obviously improve the taste of grape, improve grape quality.
The processing of therefore, using fulvo acid grape special fertilizer of the present invention obviously improved grape quality, improved output.So grape special fertilizer of the present invention should vigorously promote the use.

Claims (4)

1. fulvo acid grape special fertilizer is characterized in that the feed composition weight part is following:
Fulvo acid 3-10 part,
Urea 20-70 part,
Water-soluble phosphoric acid one ammonium 25-60 part,
Water-soluble vitriolate of tartar 20-50 part,
EDTA chelated microelement 0.5-1.5 part;
Above raw material is the commercially available prod, wherein:
Described fulvo acid is yellow humic acid sylvite, yellow humic acid ammonium salt or wherein a kind of, belongs to water-soluble macromolecular organic compound, specification of quality: water-soluble >=90%, humic acids content >=60%;
Said urea is small particle urea, and nitrogen content >=46.2%, particle diameter are 0.85mm-2.80mm;
Said water-soluble phosphoric acid one ammonium nitrogen content is 12%, and phosphorus pentoxide content is 61%;
Potassium oxide content is 52% in the said water-soluble vitriolate of tartar;
Said EDTA chelated microelement is a two or more mixture in EDTA chelating calcium, EDTA chelated magnesium, the EDTA chelating zinc, is Powdered;
The content that relates in the above raw material is mass percent.
2. fulvo acid grape special fertilizer as claimed in claim 1 is characterized in that the feed composition weight part is following:
Fulvo acid 3.5-8 part,
Urea 30-50 part,
Water-soluble phosphoric acid one ammonium 30-45 part,
Water-soluble vitriolate of tartar 25-35 part,
EDTA chelated microelement 0.5-1 part.
3. fulvo acid grape special fertilizer as claimed in claim 2 is characterized in that the feed composition weight part is following:
3.5 parts of fulvo acids,
31 parts in urea,
30 parts of water-soluble phosphoric acid one ammoniums,
35 parts of water-soluble vitriolate of tartar,
0.5 part of EDTA chelated microelement.
4. like the preparation method of claim 1,2 or 3 described fulvo acid grape special fertilizers: in the fused solution of urea and monoammonium phosphate, allocate vitriolate of tartar into through heating; Add humic acids and trace element then; It is mixed with fused solution; Under the temperature of fused solution self and mechanical agitation, be combined into low temperature eutectic rapidly with certain flowing property; Adopt prilling tower sprinkling pelleting technology to carry out granulation at last, in the process that in prilling tower, falls of spray tear drop, carry out heat exchange and cool off rapidly and solidifies acquisition fulvo acid grape special fertilizer with the airflow that rises.
CN2012102909325A 2012-08-16 2012-08-16 Water-soluble humic acid grape special fertilizer and production method thereof Pending CN102775251A (en)

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104151079A (en) * 2014-08-25 2014-11-19 河北沃田生物肥业有限公司 Organic-inorganic microbiological water-soluble fertilizer specially used for grape and preparation method thereof
CN104591879A (en) * 2014-12-30 2015-05-06 成都新柯力化工科技有限公司 Special controlled-release water soluble fertilizer for grapes and preparation method thereof
CN104892323A (en) * 2015-06-26 2015-09-09 陕西博农农资有限公司 Humic acid water-soluble compound fertilizer and method for manufacturing same
CN104973993A (en) * 2015-06-30 2015-10-14 新疆锦华肥业有限公司 Plant water-saving, draught-resistant, and yield-increasing agent and preparation method thereof
CN105111016A (en) * 2015-08-23 2015-12-02 云南省农业科学院热带亚热带经济作物研究所 Water-soluble humic acid fertilizer and preparation method
CN105111017A (en) * 2015-08-23 2015-12-02 云南省农业科学院热带亚热带经济作物研究所 Humic acid fertilizer for correcting lemon yellowing and preparation method
CN106631517A (en) * 2017-01-17 2017-05-10 河北中仁化肥有限公司 Humic-acid-containing water-soluble fertilizer capable of increasing selenium content of grapes, and preparation method and application thereof
CN106699385A (en) * 2016-12-28 2017-05-24 郑州阿波罗肥业有限公司 Manntiol-Ca- and biochemical fulvic acid-containing special fertilizer for drought-resistant grape
CN107056530A (en) * 2017-03-10 2017-08-18 四川好时吉化工有限公司 A kind of humic acid fertilizer for grape
CN108503490A (en) * 2018-06-07 2018-09-07 广州护地肥料科技有限公司 One kind fertilizer containing humic acid water-soluble and preparation method thereof
CN109678587A (en) * 2019-03-01 2019-04-26 刘世洪 A kind of organic potassium sulfate of new type water-solubility and preparation method thereof
CN109734515A (en) * 2019-03-05 2019-05-10 河北春潮生物科技有限公司 Dedicated multi-element water soluble fertilizer of fruit tree and preparation method thereof
CN110483124A (en) * 2019-05-09 2019-11-22 新疆农业科学院土壤肥料与农业节水研究所(新疆维吾尔自治区新型肥料研究中心) A kind of thompson seedless grape compound fertilizer special
CN111217651A (en) * 2020-02-13 2020-06-02 浙江丰瑜生态科技股份有限公司 Humic acid-containing water-soluble fertilizer suitable for grapes and preparation method and use method thereof
CN113354471A (en) * 2021-06-24 2021-09-07 湖北宜施壮农业科技有限公司 Compound fertilizer for flying application and preparation method thereof
CN114213176A (en) * 2022-01-14 2022-03-22 晟丰(烟台)农业科技有限公司 Fertilizer for improving stress resistance and quality of crops and preparation method thereof

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CN101570456A (en) * 2008-10-22 2009-11-04 新疆农垦科学院农业新技术推广服务中心 Water soluble humic acid multi-element solid fertilizer and production method thereof
CN102503640A (en) * 2011-10-29 2012-06-20 史丹利化肥股份有限公司 Special functional melt granulated humic acid fertilizer and production method thereof
CN102503641A (en) * 2011-10-29 2012-06-20 史丹利化肥股份有限公司 Novel green efficient multifunctional humic acid special fertilizer for soybean and preparation method thereof

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CN101570456A (en) * 2008-10-22 2009-11-04 新疆农垦科学院农业新技术推广服务中心 Water soluble humic acid multi-element solid fertilizer and production method thereof
CN102503640A (en) * 2011-10-29 2012-06-20 史丹利化肥股份有限公司 Special functional melt granulated humic acid fertilizer and production method thereof
CN102503641A (en) * 2011-10-29 2012-06-20 史丹利化肥股份有限公司 Novel green efficient multifunctional humic acid special fertilizer for soybean and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN104151079A (en) * 2014-08-25 2014-11-19 河北沃田生物肥业有限公司 Organic-inorganic microbiological water-soluble fertilizer specially used for grape and preparation method thereof
CN104151079B (en) * 2014-08-25 2016-07-13 河北沃田生物肥业有限公司 The preparation method of Fructus Vitis viniferae special organic-inorganic microorganism water soluble fertilizer
CN104591879A (en) * 2014-12-30 2015-05-06 成都新柯力化工科技有限公司 Special controlled-release water soluble fertilizer for grapes and preparation method thereof
CN104892323A (en) * 2015-06-26 2015-09-09 陕西博农农资有限公司 Humic acid water-soluble compound fertilizer and method for manufacturing same
CN104973993A (en) * 2015-06-30 2015-10-14 新疆锦华肥业有限公司 Plant water-saving, draught-resistant, and yield-increasing agent and preparation method thereof
CN105111016A (en) * 2015-08-23 2015-12-02 云南省农业科学院热带亚热带经济作物研究所 Water-soluble humic acid fertilizer and preparation method
CN105111017A (en) * 2015-08-23 2015-12-02 云南省农业科学院热带亚热带经济作物研究所 Humic acid fertilizer for correcting lemon yellowing and preparation method
CN106699385A (en) * 2016-12-28 2017-05-24 郑州阿波罗肥业有限公司 Manntiol-Ca- and biochemical fulvic acid-containing special fertilizer for drought-resistant grape
CN106631517A (en) * 2017-01-17 2017-05-10 河北中仁化肥有限公司 Humic-acid-containing water-soluble fertilizer capable of increasing selenium content of grapes, and preparation method and application thereof
CN107056530A (en) * 2017-03-10 2017-08-18 四川好时吉化工有限公司 A kind of humic acid fertilizer for grape
CN108503490A (en) * 2018-06-07 2018-09-07 广州护地肥料科技有限公司 One kind fertilizer containing humic acid water-soluble and preparation method thereof
CN109678587A (en) * 2019-03-01 2019-04-26 刘世洪 A kind of organic potassium sulfate of new type water-solubility and preparation method thereof
CN109734515A (en) * 2019-03-05 2019-05-10 河北春潮生物科技有限公司 Dedicated multi-element water soluble fertilizer of fruit tree and preparation method thereof
CN110483124A (en) * 2019-05-09 2019-11-22 新疆农业科学院土壤肥料与农业节水研究所(新疆维吾尔自治区新型肥料研究中心) A kind of thompson seedless grape compound fertilizer special
CN111217651A (en) * 2020-02-13 2020-06-02 浙江丰瑜生态科技股份有限公司 Humic acid-containing water-soluble fertilizer suitable for grapes and preparation method and use method thereof
CN111217651B (en) * 2020-02-13 2021-11-30 浙江丰瑜生态科技股份有限公司 Humic acid-containing water-soluble fertilizer suitable for grapes and preparation method and use method thereof
CN113354471A (en) * 2021-06-24 2021-09-07 湖北宜施壮农业科技有限公司 Compound fertilizer for flying application and preparation method thereof
CN114213176A (en) * 2022-01-14 2022-03-22 晟丰(烟台)农业科技有限公司 Fertilizer for improving stress resistance and quality of crops and preparation method thereof

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Application publication date: 20121114