CN104233491B - 一种多孔纳米纤维的制备方法 - Google Patents
一种多孔纳米纤维的制备方法 Download PDFInfo
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- CN104233491B CN104233491B CN201410537559.8A CN201410537559A CN104233491B CN 104233491 B CN104233491 B CN 104233491B CN 201410537559 A CN201410537559 A CN 201410537559A CN 104233491 B CN104233491 B CN 104233491B
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- 239000002121 nanofiber Substances 0.000 title claims abstract description 62
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000002105 nanoparticle Substances 0.000 claims abstract description 26
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 25
- 238000009987 spinning Methods 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 23
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 21
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 21
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 21
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 21
- 229920000642 polymer Polymers 0.000 claims abstract description 18
- 239000004744 fabric Substances 0.000 claims abstract description 17
- 239000002904 solvent Substances 0.000 claims abstract description 16
- 230000005684 electric field Effects 0.000 claims abstract description 13
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims abstract description 11
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims abstract description 11
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims abstract description 11
- 239000007921 spray Substances 0.000 claims abstract description 10
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 8
- 230000000694 effects Effects 0.000 claims abstract description 8
- 238000002791 soaking Methods 0.000 claims abstract description 8
- 238000013019 agitation Methods 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 238000007654 immersion Methods 0.000 claims description 5
- 229920002239 polyacrylonitrile Polymers 0.000 claims description 5
- 229920005610 lignin Polymers 0.000 claims description 4
- 229920000728 polyester Polymers 0.000 claims description 2
- 239000002070 nanowire Substances 0.000 claims 1
- 239000008187 granular material Substances 0.000 abstract description 6
- 238000004140 cleaning Methods 0.000 abstract description 4
- 238000005553 drilling Methods 0.000 abstract description 4
- 239000004753 textile Substances 0.000 description 9
- 238000010041 electrostatic spinning Methods 0.000 description 7
- 239000000835 fiber Substances 0.000 description 5
- 239000002086 nanomaterial Substances 0.000 description 5
- 229920001577 copolymer Polymers 0.000 description 4
- 150000001470 diamides Chemical class 0.000 description 4
- 239000000975 dye Substances 0.000 description 4
- 238000004043 dyeing Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 230000003746 surface roughness Effects 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 238000007385 chemical modification Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- XLYOFNOQVPJJNP-ZSJDYOACSA-N heavy water Substances [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 description 1
- 238000003837 high-temperature calcination Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
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- Chemical Or Physical Treatment Of Fibers (AREA)
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CN201410537559.8A CN104233491B (zh) | 2014-10-13 | 2014-10-13 | 一种多孔纳米纤维的制备方法 |
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CN104233491A CN104233491A (zh) | 2014-12-24 |
CN104233491B true CN104233491B (zh) | 2016-10-26 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106884227A (zh) * | 2017-03-09 | 2017-06-23 | 嘉兴学院 | 一种木质素/增强剂复合纺丝液的配制方法 |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105040157B (zh) * | 2015-07-27 | 2017-08-08 | 北京林业大学 | 一种木质液化物静电纺丝液的制备及纺丝方法 |
CN105696114B (zh) * | 2016-03-07 | 2018-02-06 | 中国工程物理研究院化工材料研究所 | 可调控碳纤维材料孔径及孔隙率的制备方法及碳纤维材料 |
CN109680353B (zh) * | 2018-12-27 | 2020-07-03 | 江苏恒力化纤股份有限公司 | 一种阳离子可染聚酯纤维及其制备方法 |
CN112695443B (zh) * | 2020-12-04 | 2022-03-29 | 宁波三同编织有限公司 | 一种衬衫面料及其制备方法 |
CN113308756A (zh) * | 2021-07-01 | 2021-08-27 | 扬州锦辉化纤有限公司 | 超细多孔锦纶6纤维及制备方法 |
CN113755964B (zh) * | 2021-09-29 | 2023-07-21 | 西安理工大学 | 一种介孔纤维素纤维材料的制备方法 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
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KR101265093B1 (ko) * | 2008-12-26 | 2013-05-16 | 한국과학기술연구원 | 나노 분말, 나노 잉크 및 마이크로 로드와 그 제조 방법 |
CN102021676B (zh) * | 2010-11-11 | 2012-05-23 | 东华大学 | 二氧化钛/活性炭复合纳米纤维膜的制备方法 |
KR101249952B1 (ko) * | 2010-12-20 | 2013-04-03 | 대림대학교산학협력단 | 에르븀이 첨가된 이산화티타늄 나노섬유의 제조방법 |
CN102776603A (zh) * | 2012-07-10 | 2012-11-14 | 东华大学 | 一种通过静电纺制备多孔中空纳米氧化铝纤维的方法 |
CN103011778B (zh) * | 2012-12-14 | 2014-01-15 | 山东大学 | 一种多孔氧化铝纳米纤维及其制备方法 |
CN103305965B (zh) * | 2013-06-04 | 2016-08-10 | 清华大学深圳研究生院 | 具有纳米微孔隙的硅碳复合材料及其制备方法与用途 |
CN103591032B (zh) * | 2013-10-23 | 2016-12-07 | 江苏大学 | 一种叶片泵流动不稳定性程度的监测方法和装置 |
CN103590132B (zh) * | 2013-11-25 | 2016-03-02 | 扬州大学 | 一种多孔结构静电纺丝纳米纤维的制备方法 |
CN103741263B (zh) * | 2014-01-15 | 2016-04-20 | 辽宁石油化工大学 | 一种高比表面多孔TiO2纳米纤维的制备方法 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106884227A (zh) * | 2017-03-09 | 2017-06-23 | 嘉兴学院 | 一种木质素/增强剂复合纺丝液的配制方法 |
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