CN104193417A - Elder brother glaze and younger brother glaze combined celadon ware calcining process and glaze formulas - Google Patents
Elder brother glaze and younger brother glaze combined celadon ware calcining process and glaze formulas Download PDFInfo
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- CN104193417A CN104193417A CN201410444480.0A CN201410444480A CN104193417A CN 104193417 A CN104193417 A CN 104193417A CN 201410444480 A CN201410444480 A CN 201410444480A CN 104193417 A CN104193417 A CN 104193417A
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Abstract
The invention relates to the field of celadon ware arts and crafts and particularly discloses a traditional dragon spring elder brother glaze and younger brother glaze combined calcining process and glaze formulas. The expansion coefficient difference of an elder brother glaze and a younger brother glaze is relatively large, the cracking limiting temperature of the elder brother glaze is higher than the highest limiting temperature for calcining the younger brother glaze, and the flowability of the younger brother glaze becomes high when the elder brother glaze reaches the cracking limiting temperature, so that the traditional celadon artworks almost have no condition that the elder brother glaze and the younger brother glaze are combined to be calcined, and particularly, artworks with different glazes at the inside and outside, such as a vessel with the inside made of the elder brother glaze and the outside made of the younger brother glaze or a vessel with the inside made of the younger brother glaze and the outside made of the elder brother glaze, are not tried by an artist. Through changing the glaze formulas of the elder brother glaze and the younger brother glaze, the lowest limiting temperature for hacking the elder brother glaze is lowered, the highest limiting temperature for calcining the younger brother glaze is raised, an overlapping region exists between the temperature for calcining the elder brother glaze and the temperature for calcining the younger brother glaze, the hacking of the elder brother glaze is ensured, meanwhile, the flowability of the younger brother glaze is relatively stable, and the basis is laid for the combined calcining of the elder brother glaze and the younger brother glaze.
Description
Technical field
The present invention relates to celadon industrial art field, relate in particular to and a kind of traditional dragon's fountain brother glaze is combined to the processing method of firing with younger brother's glaze.
Background technology
Longquan celadon starts from Shanxi generation, during the Northern Song Dynasty, begins to take shape, and when Song Yuan, enters the period of great prosperity, porcelain making scale is unique, skill reaches the peak of perfection, and the plum green in Di kiln, lavender grey glaze have reached the tidemark of celadon glaze colours, and therefore dragon's fountain becomes national famous Ci Ye center.Longquan celadon product has two kinds: a kind of is white tire and cinnabar tire celadon, famous " Di kiln " or " Longqun Cave ", and another kind is the black tire celadon of crackle glaze, claims in " brother's kiln ".
Di kiln celadon glaze layer is plump, and glaze colours green grass or young crops is green, and gloss is soft, and sparkling and crystal-clear moistening, surpasses emerald.There are the different glaze colours such as plum green, pale blue, bluish white, yellowish pea green glaze, light orchid, sallow." brother's kiln " celadon be take, and magnificent, ancient line sheet of falling forward is decorative means, it is as broken in cracked ice pattern, crab claw line, ox hair line, flowing water line, roe line, meals blood line, hundred rubbish etc. that its glaze layer is full, shining and clean in addition, have the title of " purple mouthful iron foot ", set each other off with glaze line sheet, more aobvious ancient servant, elegance, treasure in profound title porcelain.
Geware glaze matter is purely dense, very not lustrous and transparent, in glaze, has bubble more, as dimly visible in pearl, therefore common name " poly-foam is collected together pearl ".In the precious light of glaze colours, accumulate, moist as crisp.Line sheet is varied, and the key character that is referred to as yellow eel line, black blue line, brother's vitreous enamel with track is crackle glaze, and this is a kind of natural cracking phenomenon occurring on glaze.Cracking is the defect during porcelain is fired originally, and people had grasped the rule of cracking afterwards, allows consciously its generation hack, thereby has produced a kind of aesthetic feeling of uniqueness.Song dynasty brother vitreous enamel enamel jade-like stone profit, entire body glaze is by the cutting that interweaves of thick dark or thin two kinds of shallow streaklines, and term is called " cracked ice pattern ", is commonly called as " spun gold iron wire ".Brother's kiln china clay weak pulse is purple, and matter is thin, has glaze grey, cream-coloured, three kinds of enamel coloured silks of pale blue look, the full crackle in surface.Because soil property iron-holder is higher, while burning embryo, reduce, porcelain embryo is purple black iron look, and the bottom that porcelain is not coated with glaze manifests the original iron look of porcelain embryo, be " iron foot ", and the thinner oral area of muffle painting is purple, is " purple mouthful ", is commonly called as " purple mouthful iron foot ".In general, it is rather precious that the large little person of hacking of device and little device do not hack greatly person.Because brother's vitreous enamel is careful, exquisite,, there is imitation in each generation to it later., also there is the climax of imitative brother's vitreous enamel in the Dao Liao Qing Dynasty particularly.In the Dao Liao Qing Dynasty later stage, brother's glaze is significantly not as clear early stage, and color is more and more darker, hacks more and more in small, broken bitsly, and rough uneven glaze even appears in glaze, and it is loose that tire matter also becomes.Pale yellow line, roe line; With line shape, be referred to as guiding principle shape line, plum blossom line, line in small, broken bits, big or small check, cracked ice pattern etc., always by name hundred extremely broken.
The difference of brother's kiln and Di kiln maximum is, brother's kiln is to hack porcelain, and there is the lines of picture slight crack on celadon surface, this line is because of the carcass coefficient of expansion, to be greater than the coefficient of expansion of glaze, when firing is cooling, occurring, is originally a kind of defect, but produces the special decorative effect of " spun gold iron wire ".Di kiln is not hack porcelain.
Because the coefficient of expansion difference of brother's glaze and younger brother's glaze is larger, brother's glaze cracking ultimate temperature is higher than the highest threshold temperature of firing younger brother's glaze, when brother's glaze reaches capacity Cracking Temperature, it is large that the mobility of younger brother's glaze becomes, cause, traditional celadon artwork seldom occurs that brother's glaze is combined situation about firing with younger brother's glaze, and especially the inner brother of employing of vessel glaze, the outside artwork of younger brother's glaze or the inner younger brother of employing of vessel glaze, this inside and outside different glaze of the outside brother of employing glaze that adopts also do not have technique great master to attempt.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of inner sintering technology method from outside different glaze of vessel of firing.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is as follows: a kind of celadon sintering technology method that brother's glaze combines with younger brother's glaze, comprises following processing step:
(1) base: the base substrate of making vessel according to demand;
(2) brushing stopper line: at dry vessel base substrate opening part brushing stopper line, the main component of its stopper line is Zijin soil;
(3) biscuiting: brushing stopper line dried base substrate are placed in to kiln biscuiting, and biscuiting temperature is 780～820 ℃, and the biscuiting time is 5～8h, naturally cools to room temperature after biscuiting completes;
(4) glazing: first, glazing operation is carried out in the inside of vessel base substrate, be dried after glazing completes; Secondly, glazing operation is carried out in the outside of vessel base substrate, after glazing completes, be dried, the glaze that the outside use of its base substrate is inner different from base substrate, when brother's glaze is used in base substrate inside, the outside use of base substrate younger brother glaze; When the inner use of base substrate younger brother glaze, the outside brother's glaze that uses of base substrate; Again, to carry out glaze spraying inside and outside whole glazing dry base substrate simultaneously, its glaze spraying pass is 2～3 times; Finally, glaze is picked in the blocked up place of base substrate glazing.
(5) glaze firing: the base substrate loading of kiln that glazing is completed, carry out glaze firing; That its glaze firing comprises is successively dry, oxidation, reduction, become porcelain, insulation double teacher, and at its drying stage, kiln temperature slowly rises, wicket offers the gap for moisture evaporation is overflowed in base substrate, through 2～3 hours, when reaching 300～400 ℃, temperature closes wicket, continue heat temperature raising;
At its oxidation stage, with 4～5 hours, kiln temperature is promoted to 950 ℃, make base substrate obtain being oxidized fully slowly, then use approximately 1 hours, make kiln temperature rise to 980 ℃ and carry out transition insulation;
At its reduction phase, since 980 ℃, carry out strong firing with reductive flame, heat-up rate is controlled at 1 ℃～1.5 ℃/min, and kiln temperature rises to 1250 ℃ from 980 ℃, and gaseous-pressure is enlarged to 0.02～0.05Mpa, carries out the strong reduction reaction of 3～4 hours;
At it, become the porcelain stage, turn gaseous-pressure to 0.005～0.02Mpa down, reduce reducing atmosphere, within 2 hours, cellar for storing things temperature is raised to 1280 ℃ from 1250 ℃;
At its holding stage, keep kiln temperature flame-out after between 1280 ℃～1290 ℃ 20～30 minutes;
(6) cooling: after glaze firing completes, after kiln temperature naturally cools to room temperature, to open kiln, take out finished product.
Further, in described step (4), adopt taxi driver brother's glaze, calculate by mass percentage, by following component and content, formed:
The younger brother's glaze adopting in described step (4) is lavender grey glaze or plum green, and described lavender grey glaze is calculated by mass percentage, following component and content, consists of:
Described plum green is calculated by mass percentage, following component and content, consists of:
Further, its vessel base substrate, before glazing, is first processed the dust of surfaces externally and internally by air pump and wet sponge.
Further, before the outside glazing of its vessel base substrate, its base substrate outside surface is carried out to even swabbing processing near the position of bottom.
Further, before the outside glazing of its vessel base substrate, its base substrate outside surface is carried out to even swabbing processing near the position of bottom.
The glaze formula of brother's glaze of the present invention and younger brother's glaze, it has reduced the lowest limit temperature that brother's glaze hacks, promoted the highest threshold temperature that younger brother's glaze is fired, make the firing temperature of brother's glaze and the firing temperature of younger brother's glaze have overlapping interval, when guaranteeing that brother's glaze hacks, the mobility of younger brother's glaze is relatively stable, is combined to fire to lay the foundation for brother's glaze with younger brother's glaze.Use brother's glaze of the present invention to be combined the celadon product of firing with younger brother's glaze, overturned the tradition that traditional celadon product is fired with same glaze, especially brother's glaze glaze different from this limit firing temperature of younger brother's glaze combines, in celadon field, start the beginning, there is great historic significance.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail.It should be noted that, each raw material in the glaze formula relating in the present invention, the place of production is Zhejiang Province's Longquan City, and its title and composition, for its those skilled in the relevant art, are all clear and definite.
In Jiangxi Science technology press publishes, the < < pottery 300 that Pan Zhaohong writes asks that > > has included the glaze formula of Zhejiang Province's Longquan City, its Geware glaze by mass percentage, comprises following component:
Its lavender grey glaze by mass percentage, comprises following component:
Its plum green by mass percentage, comprises following component:
Above-mentioned lavender grey glaze and plum green are traditional Di kiln glaze.In this book, collecting taxi driver brother's glaze and younger brother's glaze is traditional glaze formula, and its firing temperature is generally, brother's glaze: 1290 ℃～1320 ℃, and younger brother's glaze: 1270 ℃～1280 ℃.As mentioned above, the minimum temperature of hacking of its brother's glaze is higher than the highest threshold temperature of younger brother's glaze, when reach brother's glaze hack temperature time, the mobility of younger brother's glaze is excessive, therefore, traditional taxi driver brother's glaze and younger brother's glaze cannot be fired simultaneously.
The problem that cannot simultaneously fire in order to solve above-mentioned brother's glaze and younger brother's glaze, the present invention adjusts the formula of brother's glaze and younger brother's glaze.
Its brother's glaze, calculates by mass percentage, following component and content, consists of:
Above-mentioned brother's glaze formula asks that with < < pottery 300 > > includes taxi driver brother's glaze formula and compares, the content of Wingdale increases to some extent, and quartz and feldspar have been increased, for the technician in celadon field, Wingdale, feldspar and quartzy in glaze and blank batching, play the effect of solvent, the increase of its content, the effect playing is to have increased mobility, has reduced the ultimate temperature that brother's glaze hacks.Through the applicant, improveing taxi driver brother's glaze firing temperature is 1280 ℃～1310 ℃.
Its younger brother's glaze comprises lavender grey glaze and plum green, and its lavender grey glaze is calculated by mass percentage, following component and content, consists of:
Its plum green is calculated by mass percentage, following component and content, consists of:
The formula of above-mentioned younger brother's glaze and < < pottery 300 ask that younger brother's glaze formula that > > includes compares, it is mainly the limestone content having reduced as solvent, the stability of glaze is increased, mobility reduces, and corresponding firing temperature raises.Improved younger brother's glaze, its firing temperature is: 1280 ℃～1290 ℃.
Known through taxi driver brother's glaze and younger brother's glaze after improvement are fired to temperature analysis, it has an overlapping temperature range, and 1280 ℃～1290 ℃.Therefore,, as long as temperature controlled enough accurate, it improves rear taxi driver brother's glaze and younger brother's glaze has had and can, with the basis of klining system, also with regard to the different glaze of inside and outside use at same vessel, lay the foundation.
In the present embodiment, the celadon sintering technology method that its brother's glaze combines with younger brother's glaze, comprises following processing step:
(1) base: the base substrate of making vessel according to demand.
(2) brushing stopper line: at dry vessel base substrate opening part brushing stopper line, for brother's glaze and younger brother's glaze are separated, prevent from mixing, the main component of its stopper line is Zijin soil.
(3) biscuiting: brushing stopper line dried base substrate are placed in to kiln biscuiting, biscuiting temperature is 780～820 ℃, the biscuiting time is 5～8h, after biscuiting completes, naturally cools to room temperature, to the base substrate of its biscuiting, with air pump and wet sponge, the dust of surfaces externally and internally is processed clean.
(4) glazing: first, glazing operation is carried out in the inside of vessel base substrate, be dried after glazing completes; Secondly, glazing operation is carried out in the outside of vessel base substrate, after glazing completes, be dried, it should be noted that, before its outside glazing, its base substrate outside surface is carried out to even swabbing processing near the position of bottom, after preventing glaze, past current downflow in sintering procedure.
The glaze that the outside use of its base substrate is inner different from base substrate, when the inner use of base substrate brother glaze, the outside use of base substrate younger brother glaze; When the inner use of base substrate younger brother glaze, the outside brother's glaze that uses of base substrate; Again, to carry out glaze spraying inside and outside whole glazing dry base substrate simultaneously, its glaze spraying pass is 2～3 times; Finally, glaze is picked in the blocked up place of base substrate glazing.
In the present embodiment, its brother's glaze is calculated by mass percentage, following component and content, consists of:
When its younger brother's glaze is selected lavender grey glaze, calculate by mass percentage, by following component and content, formed:
When its younger brother's glaze is selected plum green, calculate by mass percentage, by following component and content, formed:
(5) glaze firing: the base substrate loading of kiln that glazing is completed, carry out glaze firing; That its glaze firing comprises is successively dry, oxidation, reduction, become porcelain, insulation double teacher, and at its drying stage, kiln temperature slowly rises, wicket offers the gap for moisture evaporation is overflowed in base substrate, through 2～3 hours, when reaching 300～400 ℃, temperature closes wicket, continue heat temperature raising;
At its oxidation stage, with 4～5 hours, kiln temperature is promoted to 950 ℃, make base substrate obtain being oxidized fully slowly, then use approximately 1 hours, make kiln temperature rise to 980 ℃ and carry out transition insulation;
At its reduction phase, since 980 ℃, carry out strong firing with reductive flame, heat-up rate is controlled at 1 ℃～1.5 ℃/min, and kiln temperature rises to 1250 ℃ from 980 ℃, and gaseous-pressure is enlarged to 0.02～0.05Mpa, carries out the strong reduction reaction of 3～4 hours;
At it, become the porcelain stage, turn gaseous-pressure to 0.005～0.02Mpa down, reduce reducing atmosphere, within 2 hours, cellar for storing things temperature is raised to 1280 ℃ from 1250 ℃;
At its holding stage, keep kiln temperature flame-out after between 1280 ℃～1290 ℃ 20～30 minutes.
(6) cooling: after glaze firing completes, after kiln temperature naturally cools to room temperature, to open kiln, take out finished product.
The glaze formula of brother's glaze of the present invention and younger brother's glaze, it has reduced the lowest limit temperature that brother's glaze hacks, promoted the highest threshold temperature that younger brother's glaze is fired, make the firing temperature of brother's glaze and the firing temperature of younger brother's glaze have overlapping interval, when guaranteeing that brother's glaze hacks, the mobility of younger brother's glaze is relatively stable, is combined to fire to lay the foundation for brother's glaze with younger brother's glaze.Use brother's glaze of the present invention to be combined the celadon product of firing with younger brother's glaze, overturned the tradition that traditional celadon product is fired with same glaze, especially brother's glaze glaze different from this limit firing temperature of younger brother's glaze combines, in celadon field, start the beginning, there is great historic significance.
Claims (8)
1. the celadon sintering technology method that brother's glaze combines with younger brother's glaze, is characterized in that, comprises following processing step:
(1) base: the base substrate of making vessel according to demand;
(2) brushing stopper line: at dry vessel base substrate opening part brushing stopper line, the main component of its stopper line is Zijin soil;
(3) biscuiting: brushing stopper line dried base substrate are placed in to kiln biscuiting, and biscuiting temperature is 780～820 ℃, and the biscuiting time is 5～8h, naturally cools to room temperature after biscuiting completes;
(4) glazing: first, glazing operation is carried out in the inside of vessel base substrate, be dried after glazing completes; Secondly, glazing operation is carried out in the outside of vessel base substrate, after glazing completes, be dried, the glaze that the outside use of its base substrate is inner different from base substrate, when brother's glaze is used in base substrate inside, the outside use of base substrate younger brother glaze; When the inner use of base substrate younger brother glaze, the outside brother's glaze that uses of base substrate; Again, to carry out glaze spraying inside and outside whole glazing dry base substrate simultaneously, its glaze spraying pass is 2～3 times; Finally, glaze is picked in the blocked up place of base substrate glazing.
(5) glaze firing: the base substrate loading of kiln that glazing is completed, carry out glaze firing; That its glaze firing comprises is successively dry, oxidation, reduction, become porcelain, insulation double teacher, and at its drying stage, kiln temperature slowly rises, wicket offers the gap for moisture evaporation is overflowed in base substrate, through 2～3 hours, when reaching 300～400 ℃, temperature closes wicket, continue heat temperature raising;
At its oxidation stage, with 4～5 hours, kiln temperature is promoted to 950 ℃, make base substrate obtain being oxidized fully slowly, then use approximately 1 hours, make kiln temperature rise to 980 ℃ and carry out transition insulation;
At its reduction phase, since 980 ℃, carry out strong firing with reductive flame, heat-up rate is controlled at 1 ℃～1.5 ℃/min, and kiln temperature rises to 1250 ℃ from 980 ℃, and gaseous-pressure is enlarged to 0.02～0.05Mpa, carries out the strong reduction reaction of 3～4 hours;
At it, become the porcelain stage, turn gaseous-pressure to 0.005～0.02Mpa down, reduce reducing atmosphere, within 2 hours, cellar for storing things temperature is raised to 1280 ℃ from 1250 ℃;
At its holding stage, keep kiln temperature flame-out after between 1280 ℃～1290 ℃ 20～30 minutes;
(6) cooling: after glaze firing completes, after kiln temperature naturally cools to room temperature, to open kiln, take out finished product.
2. according to processing method claimed in claim 1, it is characterized in that, in described step (4), adopt taxi driver brother's glaze, calculate by mass percentage, by following component and content, formed:
The younger brother's glaze adopting in described step (4) is lavender grey glaze or plum green, and described lavender grey glaze is calculated by mass percentage, following component and content, consists of:
Described plum green is calculated by mass percentage, following component and content, consists of:
3. according to the processing method described in claim 1 or 2, it is characterized in that, its vessel base substrate, before glazing, is first processed the dust of surfaces externally and internally by air pump and wet sponge.
4. according to the processing method described in claim 1 or 2, it is characterized in that, before the outside glazing of its vessel base substrate, its base substrate outside surface is carried out to even swabbing processing near the position of bottom.
5. according to processing method claimed in claim 3, it is characterized in that, before the outside glazing of its vessel base substrate, its base substrate outside surface is carried out to even swabbing processing near the position of bottom.
6. for a processing method taxi driver brother glaze described in claim 1-5 any one, calculate by mass percentage, by following component and content, formed:
7. the younger brother's glaze being combined with brother's glaze described in claim 6, described younger brother's glaze is lavender grey glaze, calculates by mass percentage, following component and content, consists of:
8. the younger brother's glaze being combined with brother's glaze described in claim 6, described younger brother's glaze is plum green, calculates by mass percentage, following component and content, consists of:
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104803662A (en) * | 2015-04-07 | 2015-07-29 | 陈均林 | Ge-Di kiln twistable glaze Yin-Yang fish ceramic product and manufacturing technology thereof |
| CN105272151A (en) * | 2015-10-13 | 2016-01-27 | 施振强 | Preparation method of modern Longquan Ge kiln porcelain |
| CN105503148A (en) * | 2015-12-31 | 2016-04-20 | 龙泉市金宏瓷业有限公司 | Preparation method of high-strength magnesium Longquan celadon billet, glaze and product |
| CN105777064A (en) * | 2016-03-17 | 2016-07-20 | 龙泉市建春青瓷厂 | Black-body celadon body material, black-body celadon ware and production method of black-body celadon ware |
| CN106083010A (en) * | 2016-06-22 | 2016-11-09 | 宜兴市金鱼陶瓷有限公司 | Celadon bright finish and the ceramic preparation of crack surface |
| CN108484103A (en) * | 2018-05-02 | 2018-09-04 | 遂昌县文昌青瓷厂 | A kind of double-colored mud Zijin soil celadon pot manufacture craft |
| CN110293618A (en) * | 2019-07-19 | 2019-10-01 | 龙泉玉德青瓷有限公司 | The processing method of the dragon's fountain ceramics of brother's kiln Di kiln combination |
| CN112028606A (en) * | 2020-09-08 | 2020-12-04 | 赵卫洪 | Longquan Ge kiln garbage broken glaze and firing process thereof |
| CN112174525A (en) * | 2020-09-19 | 2021-01-05 | 龙泉市卫洪青瓷工作室 | Preparation method of Longquan Ge kiln garbage broken porcelain and glaze |
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| CN104803662A (en) * | 2015-04-07 | 2015-07-29 | 陈均林 | Ge-Di kiln twistable glaze Yin-Yang fish ceramic product and manufacturing technology thereof |
| CN104803662B (en) * | 2015-04-07 | 2017-11-07 | 陈均林 | A kind of younger brother brother twists tire female and male fish and manufacture craft |
| CN105272151A (en) * | 2015-10-13 | 2016-01-27 | 施振强 | Preparation method of modern Longquan Ge kiln porcelain |
| CN105503148A (en) * | 2015-12-31 | 2016-04-20 | 龙泉市金宏瓷业有限公司 | Preparation method of high-strength magnesium Longquan celadon billet, glaze and product |
| CN105503148B (en) * | 2015-12-31 | 2017-11-14 | 龙泉市金宏瓷业有限公司 | A kind of preparation method of the base of high strength magnesium Longquan celadon, glaze and product |
| CN105777064A (en) * | 2016-03-17 | 2016-07-20 | 龙泉市建春青瓷厂 | Black-body celadon body material, black-body celadon ware and production method of black-body celadon ware |
| CN106083010A (en) * | 2016-06-22 | 2016-11-09 | 宜兴市金鱼陶瓷有限公司 | Celadon bright finish and the ceramic preparation of crack surface |
| CN106083010B (en) * | 2016-06-22 | 2018-12-18 | 宜兴市金鱼陶瓷有限公司 | The ceramic preparation of celadon smooth surface and crack surface |
| CN108484103A (en) * | 2018-05-02 | 2018-09-04 | 遂昌县文昌青瓷厂 | A kind of double-colored mud Zijin soil celadon pot manufacture craft |
| CN110293618A (en) * | 2019-07-19 | 2019-10-01 | 龙泉玉德青瓷有限公司 | The processing method of the dragon's fountain ceramics of brother's kiln Di kiln combination |
| CN112028606A (en) * | 2020-09-08 | 2020-12-04 | 赵卫洪 | Longquan Ge kiln garbage broken glaze and firing process thereof |
| CN112174525A (en) * | 2020-09-19 | 2021-01-05 | 龙泉市卫洪青瓷工作室 | Preparation method of Longquan Ge kiln garbage broken porcelain and glaze |
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| CN104193417B (en) | 2016-04-06 |
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