CN105272151A - Preparation method of modern Longquan Ge kiln porcelain - Google Patents
Preparation method of modern Longquan Ge kiln porcelain Download PDFInfo
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- CN105272151A CN105272151A CN201510668604.8A CN201510668604A CN105272151A CN 105272151 A CN105272151 A CN 105272151A CN 201510668604 A CN201510668604 A CN 201510668604A CN 105272151 A CN105272151 A CN 105272151A
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Abstract
The invention relates to a preparation method of modern Longquan Ge kiln porcelain, which adopts mineral raw materials and chemical raw materials and comprises the following steps: Step 1: adding a certain amount of alumina powder and balled iron paste pug into kaoline pug, and obtaining a green body by slurrying, forming and drying; Step 2: spraying balled iron paste slurry onto the internal and external surfaces of the dry green body prepared in the previous step, and obtaining a bisque body via drying and bisque firing; Step 3: applying a first layer of Ge kiln glaze on the internal and external surfaces of the bisque body prepared in the previous step in a rinsing manner, and applying a second layer of Ge kiln glaze on the surface of the first layer of Ge kiln glaze in a glaze spraying manner after the glaze is aired till the water content is less than 30%; and Step 4: after drying the bisque body, putting into a kiln for high-temperature firing by a reduction flame to form a modern Longquan Ge kiln porcelain product. The product has rich colors, clear crack grain, a strong stereoscopic contrast feeling, an excellent artistic effect and wide application prospects.
Description
Technical field
The invention belongs to ceramic (pottery) field, be specifically related to a kind of preparation method of modern dragon's fountain brother kiln porcelain.
Background technology
The iron tire purple mouth iron foot government porcelain kiln goods of dragon's fountain brother kiln, be found in the Southern Song Dynasty apart from modern about 1000, condense the porcelain making elite place of dragon's fountain artisan, but owing to there are following technological difficulties in its preparation process, first: be fired into power low, due in the iron tire foot purple mouth goods china clay used that tradition fires brother's kiln containing higher ferro element, the desired firing temperature of Longqun Cave pyrogene porcelain is not reached when firing, easily cause base substrate to subside, deformation rate is large, the problem of easily hardening cracking; Second: the problem of base glaze coefficient of expansion coupling, base substrate and mineral glaze is caused to be difficult to combine with it because the shrinking percentage of the purple mouth goods of conventional iron tire foot is excessive with instability, in the process of kiln cooling, the shrinkage rates of base substrate is greater than the shrinkage rates of glaze paint, and the crackle that glaze paint will be caused to occur that opening is larger can hurt user instead of the distinctive little open-delta winding of dragon's fountain; 3rd: the problem of color development instability, the conventional iron tire purple mouth goods of foot because its raw material adopts is the distinctive natural high Fe contained china clay in dragon's fountain native country because iron-holder main in china clay is unstable, so the instability of its color development can be caused; 4th: goods hold yielding problem, because the iron-holder of the purple mouth goods of conventional iron tire foot is higher, cause base substrate fusing point to reduce, during high-temperature firing, the shrinking percentage of china clay is comparatively large, can cause subsiding of carcass after cooling.Due to above technological difficulties, cause the making handicraft of the purple mouth goods of iron tire foot in the succession process in later stage because the difficulty of difficult forming complex process handicraft succession greatly, causes the handicraft of the purple mouth iron foot of iron tire to run off in a large number.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of bottleneck breaking through the purple mouth product producing process of traditional dragon's fountain brother kiln iron tire foot, utilizes natural mineral and industrial chemicals to prepare the preparation method of modern dragon's fountain brother kiln porcelain.
For solving above technical problem, technical scheme of the present invention is: a kind of preparation method of modern dragon's fountain brother kiln porcelain, adopts raw mineral materials and industrial chemicals, comprises the following steps:
Step one: add a certain amount of alumina powder and baslled iron mud pug in kaolin pug, obtains base substrate after changing slurry, shaping, drying;
Step 2: spray baslled iron material-mud on the dry base substrate surfaces externally and internally that upper step is obtained, then carries out drying, biscuiting obtains plain tire;
Step 3: the surfaces externally and internally obtaining plain tire in upper step adopt swing glaze mode on the first layer Geware glaze, wait dry to glaze water ratio lower than 30% after, then adopt the mode of glaze spraying second layer Geware glaze on the surface of the first layer Geware glaze;
Step 4: previous step glaze tire enters kiln through reducing flame high-temperature firing, obtains modern dragon's fountain brother kiln porcelain products after drying.
The material composition of described baslled iron mud pug is by weight percentage: Zijin soil 65%, fireclay 16%, kaolin 19%.
The preparation technology of described baslled iron material-mud is: in baslled iron mud pug, add its weight percent content is after the kaolin pug of 0 ~ 50%, through changing slurry, sieving and obtaining the baslled iron material-mud that water ratio is 25 ~ 50%.
After described baslled iron material-mud sieves, fineness is be less than 1% more than 10000-hole sieve.
The material composition of described Geware glaze is by weight percentage: kaolin 66.25%, plant ash 26.25%, Wingdale 3.75%, fluorite 2.5%, feldspar 1.25%.
In described step one, the add-on of alumina powder is 0.75 ~ 1.75% of kaolin pug quality, and the add-on of baslled iron mud pug is for kaolin pug quality 0 ~ 80%, and drying temperature is 100 DEG C.
In described step 2, baslled iron material-mud is sprayed on the thickness of base substrate surfaces externally and internally is 1 ~ 2mm.
In described step 2, bake out temperature is 100 DEG C, and biscuiting temperature is 800 ~ 860 DEG C.
In described step 3, the thickness of the first layer Geware glaze is 1 ~ 2mm, and the thickness of second layer Geware glaze is 1 ~ 2mm.
In described step 4, bake out temperature is 100 DEG C, and the temperature of high-temperature firing is 1240 ~ 1320 DEG C.
The preparation method of modern dragon's fountain brother kiln porcelain involved in the present invention, the natural mineral raw all adopting dragon's fountain locality to produce and industrial waste, the adaptation of product is wide, has objectively reproduced the unique products feature of dragon's fountain brother kiln in ancient times.Simultaneously, the present invention is by changing the add-on of aluminum oxide and baslled iron mud in blank, reach the object of adjustment base glaze matched expansion coefficient, the cracking degree of glaze paint can be controlled arbitrarily according to customer need, simultaneously by changing kaolinic add-on in baslled iron material-mud, reach the object controlling base substrate color, the product quality fired reaches the level of the purple mouth goods of traditional dragon's fountain brother kiln iron tire foot, method therefor of the present invention is scientific and reasonable, easy to implement, easy and simple to handle, good stability, conforming product rate are high, therefore has fabulous economy and social value.
Embodiment
Embodiment 1
Step one: add 1g alumina powder and 30g baslled iron mud pug in 100g kaolin pug, obtains base substrate after changing slurry, shaping, the 100 DEG C of dryings of throwing;
Step 2: spray the baslled iron material-mud that the thick water ratio of 1mm is 30% on the dry base substrate surfaces externally and internally that upper step obtains, then carries out 100 DEG C of oven dry, 810 DEG C of biscuitings obtains plain tire;
Step 3: the surfaces externally and internally obtaining plain tire in upper step adopt swing glaze mode on the thick the first layer Geware glaze of 1mm, wait dry to glaze water ratio lower than 30% after, then adopt the second layer Geware glaze of the mode of glaze spraying 2mm on the surface of the first layer Geware glaze;
Step 4: after 100 DEG C, previous step glaze tire is dried, enters kiln through reducing flame in 1260 DEG C of high-temperature firings, obtains modern dragon's fountain brother kiln porcelain products.
The material composition of described baslled iron mud pug is by weight percentage: Zijin soil 65%, fireclay 16%, kaolin 19%.
The material composition of described Geware glaze is by weight percentage: kaolin 66.25%, plant ash 26.25%, Wingdale 3.75%, fluorite 2.5%, feldspar 1.25%.
The preparation technology of described baslled iron material-mud is: in baslled iron mud pug, add its weight percent content is after the kaolin pug of 10%, through changing slurry, crossing ten thousand mesh sieves, tailing over and be less than 1%, obtains the baslled iron material-mud that water ratio is 30%.
The present embodiment resulting product is iron tire vola, purple tire mouth, and carcass becomes light green, and glaze paint is fine cracks lines, three-dimensional contrast feels strong, and artistic effect is splendid.
Embodiment 2
Step one: add 1.5g alumina powder and 70g baslled iron mud pug in 100g kaolin pug, obtains base substrate after changing slurry, shaping, the 100 DEG C of dryings of throwing;
Step 2: spray the baslled iron material-mud that the thick water ratio of 2mm is 40% on the dry base substrate surfaces externally and internally that upper step obtains, then carries out 100 DEG C of oven dry, 830 DEG C of biscuitings obtains plain tire;
Step 3: the surfaces externally and internally obtaining plain tire in upper step adopt swing glaze mode on the thick the first layer Geware glaze of 2mm, wait dry to glaze water ratio lower than 30% after, then adopt the second layer Geware glaze of the mode of glaze spraying 2mm on the surface of the first layer Geware glaze;
Step 4: after 100 DEG C, previous step glaze tire is dried, enters kiln through reducing flame in 1300 DEG C of high-temperature firings, obtains modern dragon's fountain brother kiln porcelain products.
The material composition of described baslled iron mud pug is by weight percentage: Zijin soil 65%, fireclay 16%, kaolin 19%.
The material composition of described Geware glaze is by weight percentage: kaolin 66.25%, plant ash 26.25%, Wingdale 3.75%, fluorite 2.5%, feldspar 1.25%.
The preparation technology of described baslled iron material-mud is: in baslled iron mud pug, add its weight percent content is after the kaolin pug of 25%, through changing slurry, crossing ten thousand mesh sieves, tailing over and be less than 1%, obtains the baslled iron material-mud that water ratio is 40%.
The present embodiment resulting product is iron tire vola, purple tire mouth, and carcass becomes blackish green, and glaze paint is thick crackle lines, three-dimensional contrast feels strong, and artistic effect is splendid.
Embodiment 3
Step one: add 1.7g alumina powder in 100g kaolin pug, obtains base substrate after changing slurry, shaping, the 100 DEG C of dryings of throwing;
Step 2: spray the baslled iron material-mud that the thick water ratio of 2mm is 50% on the dry base substrate surfaces externally and internally that upper step obtains, then carries out 100 DEG C of oven dry, 850 DEG C of biscuitings obtains plain tire;
Step 3: the surfaces externally and internally obtaining plain tire in upper step adopt swing glaze mode on the thick the first layer Geware glaze of 2mm, wait dry to glaze water ratio lower than 30% after, then adopt the second layer Geware glaze of the mode of glaze spraying 2mm on the surface of the first layer Geware glaze;
Step 4: after 100 DEG C, previous step glaze tire is dried, enters kiln through reducing flame in 1320 DEG C of high-temperature firings, obtains modern dragon's fountain brother kiln porcelain products.
The material composition of described baslled iron mud pug is by weight percentage: Zijin soil 65%, fireclay 16%, kaolin 19%.
The material composition of described Geware glaze is by weight percentage: kaolin 66.25%, plant ash 26.25%, Wingdale 3.75%, fluorite 2.5%, feldspar 1.25%.
The preparation technology of described baslled iron material-mud is: in baslled iron mud pug, add its weight percent content is after the kaolin pug of 45%, through changing slurry, crossing ten thousand mesh sieves, tailing over and be less than 1%, obtains the baslled iron material-mud that water ratio is 50%.
The present embodiment resulting product is iron tire vola, purple tire mouth, and carcass becomes deep green, and strongly, artistic effect is splendid for glaze paint flawless lines, three-dimensional contrast sense.
Claims (10)
1. a preparation method for modern dragon's fountain brother kiln porcelain, adopts raw mineral materials and industrial chemicals, comprises the following steps:
Step one: add a certain amount of alumina powder and baslled iron mud pug in kaolin pug, obtains base substrate after changing slurry, shaping, drying;
Step 2: spray baslled iron material-mud on the dry base substrate surfaces externally and internally that upper step is obtained, then carries out drying, biscuiting obtains plain tire;
Step 3: the surfaces externally and internally obtaining plain tire in upper step adopt swing glaze mode on the first layer Geware glaze, wait dry to glaze water ratio lower than 30% after, then adopt the mode of glaze spraying second layer Geware glaze on the surface of the first layer Geware glaze;
Step 4: previous step glaze tire enters kiln through reducing flame high-temperature firing, obtains modern dragon's fountain brother kiln porcelain products after drying.
2. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, is characterized in that: the material composition of described baslled iron mud pug is by weight percentage: Zijin soil 65%, fireclay 16%, kaolin 19%.
3. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, it is characterized in that: the preparation technology of described baslled iron material-mud is: in baslled iron mud pug, add its weight percent content is after the kaolin pug of 0 ~ 50%, through changing slurry, sieving and obtaining the baslled iron material-mud that water ratio is 25 ~ 50%.
4. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 3, is characterized in that: after described baslled iron material-mud sieves, fineness is be less than 1% more than 10000-hole sieve.
5. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, is characterized in that: the material composition of described Geware glaze is by weight percentage: kaolin 66.25%, plant ash 26.25%, Wingdale 3.75%, fluorite 2.5%, feldspar 1.25%.
6. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, it is characterized in that: in described step one, the add-on of alumina powder is 0.75 ~ 1.75% of kaolin pug quality, the add-on of baslled iron mud pug is for kaolin pug quality 0 ~ 80%, and drying temperature is 100 DEG C.
7. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, is characterized in that: in described step 2, baslled iron material-mud is sprayed on the thickness of base substrate surfaces externally and internally is 1 ~ 2mm.
8. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, it is characterized in that: in described step 2, bake out temperature is 100 DEG C, biscuiting temperature is 800 ~ 860 DEG C.
9. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, it is characterized in that: in described step 3, the thickness of the first layer Geware glaze is 1 ~ 2mm, the thickness of second layer Geware glaze is 1 ~ 2mm.
10. the preparation method of modern dragon's fountain brother kiln porcelain according to claim 1, it is characterized in that: in described step 4, bake out temperature is 100 DEG C, the temperature of high-temperature firing is 1240 ~ 1320 DEG C.
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Cited By (4)
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CN107602083A (en) * | 2017-09-27 | 2018-01-19 | 禹州市正玉钧窑有限公司 | A kind of pottery preparation technology with aging crack |
CN108484103A (en) * | 2018-05-02 | 2018-09-04 | 遂昌县文昌青瓷厂 | A kind of double-colored mud Zijin soil celadon pot manufacture craft |
CN111204980A (en) * | 2020-03-04 | 2020-05-29 | 景德镇陶瓷大学 | Glaze for forming purple glaze, glaze and preparation method of purple glaze |
CN112723856A (en) * | 2020-12-25 | 2021-04-30 | 唐山北方瓷都陶瓷集团卫生陶瓷有限责任公司 | Low-deformation ceramic biscuit and preparation process thereof |
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CN107602083A (en) * | 2017-09-27 | 2018-01-19 | 禹州市正玉钧窑有限公司 | A kind of pottery preparation technology with aging crack |
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CN111204980A (en) * | 2020-03-04 | 2020-05-29 | 景德镇陶瓷大学 | Glaze for forming purple glaze, glaze and preparation method of purple glaze |
CN111204980B (en) * | 2020-03-04 | 2021-07-23 | 景德镇陶瓷大学 | Glaze for forming purple glaze, glaze and preparation method of purple glaze |
CN112723856A (en) * | 2020-12-25 | 2021-04-30 | 唐山北方瓷都陶瓷集团卫生陶瓷有限责任公司 | Low-deformation ceramic biscuit and preparation process thereof |
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