CN101768017A - Lavender grey glaze and manufacture method of products thereof - Google Patents
Lavender grey glaze and manufacture method of products thereof Download PDFInfo
- Publication number
- CN101768017A CN101768017A CN201010101768A CN201010101768A CN101768017A CN 101768017 A CN101768017 A CN 101768017A CN 201010101768 A CN201010101768 A CN 201010101768A CN 201010101768 A CN201010101768 A CN 201010101768A CN 101768017 A CN101768017 A CN 101768017A
- Authority
- CN
- China
- Prior art keywords
- glaze
- kiln
- biscuit
- kiln temperature
- hour
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention relates to a lavender grey glaze. After raw materials of the lavender grey glaze are proportioned according to the prescription, the ball milling, sieving and de-ironing procedures are carried out to obtain slurry. The raw material comprises dehydrated and dried powder. By introducing talc, chromic oxide and the like into the raw materials, the invention solves the problems of easy burnt blistering and smoke absorption in the high-temperature roasting process of the traditional lavender grey glaze ceramic. The glaze surface is green, smooth, fine and beautiful, the color is pure, and the ceramic is clean and similar to jade. The invention also discloses a method for manufacturing the ceramic products by using lavender grey glaze, and the lavender grey glaze ceramic finished product manufactured by the method has the advantages of high yield rate, good density and strong acid and alkaline corrosion resistance property.
Description
Technical field
The invention belongs to the domestic ceramics technical field, be specifically related to the making method of a kind of pale blue glaze and products thereof in the high temperature coloured glaze.
Background technology
The Handicraft decorative of " winning victory with glaze " is in vogue always, by burning till back external appearance characteristic classification: crackle glaze, fancy glaze, one-glaze ware or the like.One-glaze ware is simple and unsophisticated, plain with it, always doted on by the men of literature and writing.And wherein lavender grey glaze is is more viewed and admired lying hidden and undeveloped not to the utmost as ice like beautiful, dark green smooth, fine and smooth magnificent giving with it.Modern any glaze water is traced to its source, and all is the lime glaze of early stage lavender grey glaze, through lime alkali glaze, deduces and goes out.Tradition pale blue glaze exists the too harsh problem of processing requirement in being applied to the ceramic product manufacturing processed, easily produces " foamings " phenomenon as burning, and atmosphere control out of true just easily produces " smoking " phenomenon, causes that the ceramic product qualification rate is low, difficulty goes out smart mouth.
Summary of the invention
The object of the present invention is to provide a kind of pale blue glaze, this glaze wide adaptability easily burns and produces viridescent, smoothness, exquisiteness, magnificent, the glaze effect that colour purity matter is clean as beautiful; The present invention also provides the method with the blue or green ceramic product of this kind lavender grey glaze powder process, and this method is easy to implement, and with the ceramic pale blue product that this method is made, ratio defective product height, product good compactness, Heat stability is good, antiacid caustic corrosion is strong, and beautiful appearance is generous.
Pale blue glaze of the present invention, be with raw material by formulation ratio after, through ball milling, sieve, slurry that iron removal step makes, comprise the powder after dehydrating, it is characterized in that the lavender grey glaze material formula is formed and be by weight:
Glaze fruit 62～76%, feldspar 10～16%, quartz 6～10%, talcum 4～6%,
Two ashes 4～6%, chromic oxide 0.04～0.05%.
Above-mentioned ball milling operation is with selected good raw material, by behind the top formulation ratio, mixes, and the ball milling altar of packing into, press ball milling: material: water=1.5: 1: 0.8, grind to form glaze slip, be good with about 30 hours.The oversize glaze that contracts easily of time, the time, too short glaze glossiness was not good enough.
After ball milling is good, during following ball milling altar, sieve, deironing measures concentration with proportion.Operating process will strictly observe industrial hygiene, in order to avoid sneak into impurity, makes the glaze color development impure.
The glaze fruit: be a kind of porcelain stone, mineral composition andesine class mineral content is higher, and maturing temperature is lower, at 1280～1320 ℃.
Feldspar: have the ability of fusion quartz and clay, reduce the firing temperature of goods, promote into growing of porcelain reaction and mullite crystal, promote the compact structure of goods, improve the physical strength and the glaze smooth finish of goods.
Quartzy: as to be vitreous generation body in glaze, to give high wear resistance of glaze and hardness, good chemerosiveness resistent, and the coefficient of expansion of reduction glaze.
Talcum: the effect of the thermal expansion coefficient of glass of reduction is arranged, can promote the generation in middle layer, weaken glaze and split tendency.
Two ashes: contain small amounts iron, manganese oxide, phosphoric acid, play and flux when melting effect, the interaction of trace element and give gentle and refined sense.
Chromic oxide: an amount of chromic oxide best results, send out slightly serpentinous cyanic colours very little, if excess, green thickens, but tone is not just.
The making method of pale blue ceramic product of the present invention, comprise technical process such as the preparation of base glaze, moulding, refine, drying, biscuiting, glazing, loading of kiln, glaze firing, its technology point is: to the control of time, temperature and the glazing process of the biscuiting of porcelain base, glaze firing, number of times, thickness.Be specially:
After moulding porcelain base drying, go into the biscuiting of kiln through 6～7 hour time, slowly stop after burning 840～880 ℃ of temperature with warm fire, naturally cooling is the biscuit kiln discharge after 15～20 hours, two processes of inside and outside glaze divide are gone up in brush dust glazing again, biscuit glazing, earlier pale blue glaze slip furnishing water content 38～45%, with swinging on the glaze method glaze in the secondary biscuit, the gauge control of glaze layer is at 2～2.3 millimeters; After the interior glaze of biscuit is first-class, drain the moisture content of biscuit, with dipping in the outer glaze of secondary biscuit on the glaze method, the gauge control of glaze layer is at 2～2.3 millimeters again.The work in-process that inside and outside glaze is all first-class, the plane pin can be gone into kiln and be carried out glaze firing.Glaze firing will be through evaporation, reduction, become porcelain, insulation four-stage, at evaporation stage: first hour be the kiln temperature from the kiln igniting, only be warming up to 500～550 ℃.Work in-process water evaporates in the kiln is done; Second hour be that the kiln temperature is warming up to 820～870 ℃ from 500～550 ℃ and ends, be incubated 12～20 minutes; Use 50～70 minutes again, the kiln temperature is warming up to 980～1010 ℃ from 820～870 ℃, and insulation was at 1～1.20 hour.At reduction phase: the kiln temperature is warming up to 1160～1180 ℃ from 980～1010 ℃ in first hour, and kiln temperature reduction in second hour heats up and slows down a little, rises to 1220～1260 ℃ from 1160～1180 ℃.Generate the porcelain stage: in this stage kiln temperature rise temperature, per minute will be controlled 2～1.5 ℃ of intensification degree, and the time was controlled at 30～35 minutes, and the kiln temperature is risen to till 1280～1310 ℃ from 1220～1260 ℃.At holding stage: when the kiln temperature reaches 1280～1310 ℃, stop to heat up, after from then on beginning to be incubated 5～10 minutes, stop burning things which may cause a fire disaster.Allow kiln temperature naturally cooling 15～20 hours, the finished product kiln discharge.
Characteristics of the present invention are: by introducing an amount of talcum, solved traditional lavender grey glaze pottery in the high-temperature melting process easily burning bubble and the problem of " smoking ", and lavender grey glaze light transmission of the present invention is strong, good springiness has firm sense, and is bright and clean soft, not dazzling, prescription is reasonable, and firing temperature is wide, easy handling.
Lavender grey glaze product of the present invention burns till and adopts shuttle kiln to burn till, and burning till fuel is heavy oil, liquefied petroleum gas (LPG), water-gas.
Situation about not introducing in detail among the present invention is identical with conventional ceramic product, no longer narration.
Embodiment
Below in conjunction with example the invention will be further described implementation result of the present invention.
Embodiment one
The glaze formula weight percent is formed: glaze fruit 65, feldspar 16, quartz 8, talcum 6, two ashes 5.Add chromic oxide 0.04%.
In making processes:
To various glaze slurries by the meticulous selection of prescription requirement after, mix, again with ballstone: glaze, water ratio are: 1.5: 1: 0.8, the grinding plant of packing into ground to form glaze slip.
After a beautiful kettle spring of china clay moulding drying, go into kiln through 6 hours biscuiting, burn temperature slowly with warm fire and stop for 840 ℃, naturally cooling is the biscuit kiln discharge after 15 hours, the brush dust glazing again of this biscuit.Glazing divides two processes of inside and outside glaze that go up, and elder generation 38%, goes up glaze in this biscuit of secondary to glaze slip furnishing water content earlier with swinging the glaze method, and the gauge control of glaze is at 2 millimeters; Will the moisture content in the biscuit be drained after the interior glaze of this biscuit is first-class, with dipping in the outer glaze of this biscuit of secondary on the glaze method, the gauge control of glaze layer is at 2 millimeters again.The work in-process of first-class inside and outside glaze dig pin and can go into kiln and carry out glaze firing, and glaze firing will be through evaporation, reduction, become porcelain, insulation four-stage, and at evaporation stage: first hour is that the kiln temperature begins to be warming up to 500 ℃ from the kiln igniting, and the work in-process water evaporates in the kiln is done; The second hour be that the kiln temperature is warming up to 820 ℃ from 500 ℃ and ends, be incubated 12 minutes, use 50 minutes again, the kiln temperature rises to 980 ℃ from 820 ℃, is incubated 1 hour.
At reduction phase: the kiln temperature is warming up to 1160 ℃ from 980 ℃ in first hour; Kiln temperature reduction in the second hour heats up and slows down a little, is warming up to 1220 ℃ from 1160 ℃.Becoming the porcelain stage: in this stage kiln temperature rise temperature, will control 2 ℃ in the minute, the time was controlled in 30 minutes, make the kiln temperature when 1220 ℃ are warming up to 1280 ℃ till.At holding stage: when the kiln temperature reaches 1280 ℃, stop to heat up, from then on begin to be incubated 5 minutes, stop burning things which may cause a fire disaster, allow kiln temperature naturally cooling 15 hours, the finished product kiln discharge.
Originally burn till in shuttle kiln and carry out, burning till fuel is oil liquefied gas.
Embodiment two
Embodiment glaze ingredients by weight percentage composition: glaze fruit 73, feldspar 11, quartz 6, talcum 5, two ashes 5.Add chromic oxide 0.05%.
In making processes:
After the meticulous selection of various glaze, even by the prescription batch mixes, again with ballstone: glaze: the water ratio is: 1.5: 1: 0.8, the grinding plant of packing into ground to form glaze slip.
Behind garlic bottle of china clay moulding, go into the biscuiting of kiln between 7 hours, slowly burning temperature with warm fire stops for 880 ℃, naturally cooling is the biscuit kiln discharge after 20 hours, two processes of inside and outside glaze divide are gone up in brush dust glazing again, biscuit glazing, earlier glaze slip furnishing water content 45%, adopt then and swing the upward interior glaze of this biscuit of secondary of glaze method elder generation, the gauge control of glaze layer is at 2.3 millimeters; Will drain the moisture content of biscuit after the interior glaze of biscuit is first-class, employing is dipped in the glaze method and is gone up the outer glaze of secondary biscuit again, and the gauge control of glaze layer is at 2.3 millimeters.The work in-process of first-class inside and outside glaze, the plane pin can be gone into kiln and be carried out glaze firing, and glaze firing will be through evaporation, reduction, one-tenth porcelain, insulation four-stage.At evaporation stage: first hour is that the kiln temperature rises to 550 ℃ from igniting, makes the work in-process water evaporates in the kiln dried; The second hour be that the kiln temperature is raised to 870 ℃ from 550 ℃ and ends, be incubated 20 minutes, use 70 minutes again, the kiln temperature rises to 1010 ℃ from 870 ℃, is incubated 1020 hours.At reduction phase: the kiln temperature is warming up to 1180 ℃ from 1010 ℃ in first hour; Kiln temperature reduction in second hour slows down a little, rises to 1260 ℃ from 1180 ℃.Becoming the porcelain stage: in this stage kiln temperature rise temperature, per minute will be controlled at 1.5 ℃, and the time was controlled in 35 minutes, and the kiln temperature is risen to till 1310 ℃ from 1260 ℃.At holding stage: when the kiln temperature reaches 1310 ℃, stop to heat up, after from then on beginning to be incubated 10 minutes, stop burning things which may cause a fire disaster, allow kiln temperature naturally cooling 20 hours, the finished product kiln discharge.
Originally burn till in shuttle kiln and carry out, burning till fuel is oil liquefied gas.
Claims (3)
1. pale blue glaze, be with raw material by formulation ratio after, through ball milling, sieve, slurry that iron removal step makes, comprise the powder after dehydrating, it is characterized in that the lavender grey glaze material formula is formed and be by weight:
Glaze fruit 62～76%, feldspar 10～16%, quartz 6～10%, talcum 4～6%, two ashes 4～6%, chromic oxide 0.04～0.05%.
2. according to the described pale blue glaze of claim 1, it is characterized in that described ball milling, is that batch mixes is even, and the ball milling altar of packing into is pressed ball milling: material: water=1.5: 1: 0.8, grind and made slurry in 28～32 hours.
3. use the production method of pale blue glaze according to claim 1 for one kind, comprise blank preparation, moulding, biscuiting, glazing, glaze firing technical process, it is characterized in that:
After the porcelain base drying of moulding, go into kiln through 6～7 hours biscuiting, stop after burning 840～880 ℃ of temperature slowly with warm fire, naturally cooling is after 15～20 hours, the biscuit kiln discharge;
The biscuit glazing divides two processes of inside and outside glaze that go up, and 38～45%, with swinging the interior glaze of secondary biscuit on the glaze method, the gauge control of glaze layer is at 2～2.3 millimeters the glaze slip furnishing water ratio of celadon in elder generation; After the interior glaze of biscuit is first-class, drain the moisture content of biscuit, with dipping in the outer glaze of secondary base on the glaze method, the gauge control of glaze layer is at 2～2.3 millimeters again;
The work in-process of first-class glaze are gone into kiln and are burnt till and will reduce, become porcelain, insulation four-stage through evaporation:
At evaporation stage, first hour is to begin to heat up from the kiln igniting, kiln temperature rise to 500～550 ℃, work in-process water evaporates in the kiln is done, the second hour be that the kiln temperature rises to 820～870 ℃ from 500～550 ℃ and ends, be incubated 12～20 minutes, use 50～70 minutes again, make the kiln temperature rise to 980～1010 ℃ from 820～870 ℃, be incubated 1～1.20 hour;
At reduction phase, the kiln temperature rises to 1160～1180 ℃ from 980～1010 ℃ in first hour, and kiln temperature reduction in second hour heats up and slows down a little, rises to 1220～1260 ℃ from 1160～1180 ℃;
Becoming the porcelain stage, this stage: kiln temperature rise temperature, per minute will be controlled at 2～1.5 ℃, and the time was controlled in 30～35 minutes, and the kiln temperature is risen to till 1280～1310 ℃ from 1220～1260 ℃;
At holding stage, when the kiln temperature reaches 1280～1310 ℃, stop to heat up, after from then on beginning to be incubated 5～10 minutes, stop burning things which may cause a fire disaster, allow kiln temperature naturally cooling 15～20 hours, the finished product kiln discharge.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010101768XA CN101768017B (en) | 2010-01-27 | 2010-01-27 | Lavender grey glaze and manufacture method of products thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010101768XA CN101768017B (en) | 2010-01-27 | 2010-01-27 | Lavender grey glaze and manufacture method of products thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101768017A true CN101768017A (en) | 2010-07-07 |
| CN101768017B CN101768017B (en) | 2011-12-21 |
Family
ID=42501143
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201010101768XA Expired - Fee Related CN101768017B (en) | 2010-01-27 | 2010-01-27 | Lavender grey glaze and manufacture method of products thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101768017B (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102060571A (en) * | 2010-10-29 | 2011-05-18 | 南京工业大学 | Green glaze for daily porcelain |
| CN102923954A (en) * | 2011-08-11 | 2013-02-13 | 湖南泰鑫瓷业有限公司 | Iron-manganese series offwhite metal luster glaze and its making method |
| CN103449844A (en) * | 2013-08-27 | 2013-12-18 | 湖南泰鑫瓷业有限公司 | Method for spraying iron crystallization glaze after transfer printing on fambe glaze surface |
| CN104193417A (en) * | 2014-09-03 | 2014-12-10 | 许继武 | Elder brother glaze and younger brother glaze combined celadon ware calcining process and glaze formulas |
| CN104529538A (en) * | 2014-11-28 | 2015-04-22 | 黄怀韩 | Celeste blue glaze and preparation method thereof |
| CN105110640A (en) * | 2015-07-22 | 2015-12-02 | 龙泉仿宋哥窑青瓷研究所 | Moonlight white glaze and firing method thereof |
| CN107793026A (en) * | 2017-11-30 | 2018-03-13 | 南宁市生润科技有限公司 | A kind of careless cyan sanitary ceramics glaze |
| CN108793753A (en) * | 2018-07-02 | 2018-11-13 | 福建省德化祥裕陶瓷文化有限责任公司 | A kind of antibacterial glaze water and preparation method thereof |
| CN110156330A (en) * | 2019-06-10 | 2019-08-23 | 潮州市长城世家瓷业有限公司 | A kind of non-leakage cyanic colours crack glaze porcelain utensil and its manufacture craft |
| CN113121200A (en) * | 2021-03-22 | 2021-07-16 | 李玉桃 | Preparation process of over-glaze color powder celadon |
-
2010
- 2010-01-27 CN CN201010101768XA patent/CN101768017B/en not_active Expired - Fee Related
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102060571A (en) * | 2010-10-29 | 2011-05-18 | 南京工业大学 | Green glaze for daily porcelain |
| CN102923954A (en) * | 2011-08-11 | 2013-02-13 | 湖南泰鑫瓷业有限公司 | Iron-manganese series offwhite metal luster glaze and its making method |
| CN102923954B (en) * | 2011-08-11 | 2016-08-03 | 湖南泰鑫瓷业有限公司 | A kind of ferrum-manganese systems canescence metal-lustrous glaze and preparation method thereof |
| CN103449844A (en) * | 2013-08-27 | 2013-12-18 | 湖南泰鑫瓷业有限公司 | Method for spraying iron crystallization glaze after transfer printing on fambe glaze surface |
| CN104193417A (en) * | 2014-09-03 | 2014-12-10 | 许继武 | Elder brother glaze and younger brother glaze combined celadon ware calcining process and glaze formulas |
| CN104529538A (en) * | 2014-11-28 | 2015-04-22 | 黄怀韩 | Celeste blue glaze and preparation method thereof |
| CN104529538B (en) * | 2014-11-28 | 2016-05-18 | 福建省德化县腾艺陶瓷有限公司 | A kind of celeste glaze and preparation method thereof |
| CN105110640A (en) * | 2015-07-22 | 2015-12-02 | 龙泉仿宋哥窑青瓷研究所 | Moonlight white glaze and firing method thereof |
| CN107793026A (en) * | 2017-11-30 | 2018-03-13 | 南宁市生润科技有限公司 | A kind of careless cyan sanitary ceramics glaze |
| CN108793753A (en) * | 2018-07-02 | 2018-11-13 | 福建省德化祥裕陶瓷文化有限责任公司 | A kind of antibacterial glaze water and preparation method thereof |
| CN110156330A (en) * | 2019-06-10 | 2019-08-23 | 潮州市长城世家瓷业有限公司 | A kind of non-leakage cyanic colours crack glaze porcelain utensil and its manufacture craft |
| CN113121200A (en) * | 2021-03-22 | 2021-07-16 | 李玉桃 | Preparation process of over-glaze color powder celadon |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101768017B (en) | 2011-12-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101768017B (en) | Lavender grey glaze and manufacture method of products thereof | |
| CN101734948B (en) | Longquan official ware celadon glaze of the Ming Dynasty and method for manufacturing Longquan official ware celadon product of the Ming Dynasty by using glaze | |
| CN106587911B (en) | Firing method of Jianshui purple pottery firewood firing pug product | |
| CN101885601B (en) | Method for manufacturing medium-temperature Longquan powder celadon | |
| CN104961443A (en) | High-strength deformation-resistant engineering ceramic product and preparation method thereof | |
| CN102731168B (en) | Preparation method of white body ice crackle vitreous enamel and products produced from white body ice crackle vitreous enamel | |
| CN105645925A (en) | Manufacturing method of ceramic cooker with high thermal shock resistance | |
| CN107216127A (en) | Dehua pearl white porcelain and its preparation technology | |
| CN101993238A (en) | Silver jade ceramics and preparation method thereof | |
| CN100443438C (en) | Highly heatproof and shockproof ceramic and its production method | |
| CN102408223B (en) | Technology for fabricating big vessel shaped Ru porcelain bottle | |
| CN103601534A (en) | High-whiteness under-glaze colorful low-temperature ceramic and preparation method thereof | |
| CN105731799A (en) | Copper red reduction transmutation glaze, copper red reduction transmutation glaze ceramic product and preparation method thereof | |
| CN106495742A (en) | Anti- wax stone bonding glaze, anti-wax stone bonding pottery and its preparation technology | |
| CN102173875A (en) | Preparation method of B2O3-TiO2 series fambe ceramic crystalline glaze | |
| CN111574189A (en) | Manufacturing process of iron oxide red kiln transformation glazed porcelain | |
| CN110228993A (en) | A kind of crackle celadon bottle for cosmetics processing technology with the non-crack glaze of inner face | |
| CN105399329A (en) | Preparation method and glaze material of celadon secret color glaze | |
| CN111204978A (en) | Ceramic glaze with non-cracking glaze surface and glazing method thereof | |
| CN107010922A (en) | The preparation method of furnace transmutation glaze boccaro fine earthenware | |
| CN110540363A (en) | Ge kiln secret color porcelain glaze and firing method thereof | |
| CN112408791B (en) | Firing method for high-temperature firing of bone china for daily use | |
| CN106396618A (en) | Method used for firing high temperature matte brownish red glazed porcelain in reducing atmosphere | |
| CN103086697B (en) | High-calcium ceramic and preparation process thereof | |
| CN106242504A (en) | A kind of strengthening sclerotin household china and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20111221 Termination date: 20130127 |