CN104173206A - Sunscreen transparent lipstick and preparation method thereof - Google Patents
Sunscreen transparent lipstick and preparation method thereof Download PDFInfo
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- CN104173206A CN104173206A CN201410443334.6A CN201410443334A CN104173206A CN 104173206 A CN104173206 A CN 104173206A CN 201410443334 A CN201410443334 A CN 201410443334A CN 104173206 A CN104173206 A CN 104173206A
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Abstract
The invention provides a sunscreen transparent lipstick which is prepared from the following components in percentage by weight: 90.1wt% of first component and 0.9wt% of second component, wherein the first component is a mixture of the following components: a mixture of dibutyl lauroyl glutamine, polyamide-3 and a bis-stearyl ethidene diamine/neopentyl glycol/stearyl alcohol hydrodimerized linoleate copolymer, C12-15 cholesteryl benzoate, heptyl undecylenate, benzophenone-3, ethylhexyl salicylate, homosalate, C10-30 acid cholesterol/lanosterol mixed ester, hydrogenated C6-20 polyolefin and dextrin isostearate; the second component is an auxiliary additive. The lipstick provided by the invention can pass through a three-month stability test, and is clear and transparent in appearance, good in sunscreen effect, high in melting point, good in moistening degree and difficult to break off.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of lip pomade, and the preparation method of this lip pomade.
Background technology
Lip pomade is the conventional lip care products of people, and production technology is very ripe.Along with the continuous progress of science and technology, lip pomade raw material is constantly brought forth new ideas, and the outward appearance of lip pomade and function are also in diversified development.Transparent lipstick can bring pure pure and fresh impression to consumer, and the person that is well suited for current consumption thirsts for breaking away from the psychological need of environmental pollution, and market prospect is wide.Sun-proof Transparent lipstick can rise to a new level by people's lip nursing idea.But at present in China, sun-proof Transparent lipstick does not also have real flow into the market places, its reason is that formula is unstable, properties of product are poor, raw material sources channel is limited.
Summary of the invention
An object of the present invention is the technical problem that will solve for above, provide that a kind of sun-proof result is good, transparency good, moisten spend, the Transparent lipstick of frangibility not.
Another object of the present invention is to provide the preparation method of this sun-proof Transparent lipstick.
For reaching above object, the invention provides a kind of sun-proof Transparent lipstick, this lip pomade is made up of the first component of 90.1wt% and 0.9% second component, wherein, the mixing that described the first component is following component:
Dibutyl lauroyl glutamine 3.73～4.40wt%,
Mixture 16.42～the 19.40wt% of Polyamide-3 and two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer,
C12-15 alcohol benzoate 16.10～20.00wt%,
Undecylenic acid heptyl ester 13.80～27.10wt%,
BP-3 8.47～10wt%,
Ethylhexyl salicylate 4.23～5.00wt%,
Homosalate 8.47～10.00wt%,
C10-30 acid cholesterol/lanosterol mixed ester 4.85～5.00wt%,
Hydrogenation C6-20 polyolefin 8.21～9.70wt%,
Dextrin isostearate 1.52～1.80wt%,
Described second component is complementary additive,
The percentage by weight sum of each component is 100% above.
Above percentage by weight all refers to that component accounts for the percentage ratio of lip pomade gross weight.
" complementary additive " of the present invention comprises and allows other conventional compositions used for cosmetic such as the oil-soluble dyes, activating agent, antioxidant, antiseptic, pigment, aromatic that use at lip according to regulation.
Preferably, in the mixture of described Polyamide-3 and two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer, both ratios are 1:7.
The present invention also provides the preparation method of described sun-proof Transparent lipstick, and its step is as follows:
(1) by the first component, be that dibutyl lauroyl glutamine, Polyamide-3 are mixed homogeneously with mixture, C12-15 alcohol benzoate, undecylenic acid heptyl ester, BP-3, ethylhexyl salicylate, homosalate, C10-30 acid cholesterol/lanosterol mixed ester, dextrin isostearate and the hydrogenation C6-20 polyolefin of two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer, stirring is warming up to 130～140 DEG C, melts transparent completely;
(2) add second component, maintain the temperature at 100 DEG C, stir to dissolving completely;
(3) be cooled to 95～100 DEG C, mixture is injected in mould, be cooled to 4～12 DEG C of demouldings.
The present invention creatively uses dibutyl lauroyl glutamine and Polyamide-3, two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer (another title is polyamide-8) collocation, in conjunction with various ingredients, and reasonable design the weight proportion of each component, overcome defect and the deficiency of existing Transparent lipstick.After tested, lip pomade of the present invention can pass through 3 months stability tests, and outward appearance is as clear as crystal, and sun-proof result is good, and fusing point is high, moist degree well, not frangibility.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme of the present invention is described in further detail, but protection scope of the present invention is not limited in following examples.The related raw material components of various embodiments of the present invention is prior art, can buy by commercial channel.Shown according to the form below, weigh each component of embodiment 1～3:
According to following steps, the component of embodiment 1～3 is prepared into sun-proof Transparent lipstick of the present invention:
(1) A phase component mixture, C12-15 alcohol benzoate, undecylenic acid heptyl ester, BP-3, ethylhexyl salicylate, homosalate, C10-30 acid cholesterol/lanosterol mixed ester, dextrin isostearate and the hydrogenation C6-20 polyolefin of (dibutyl lauroyl glutamine, Polyamide-3 with two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer) is mixed homogeneously, stirring is warming up to 130～140 DEG C, melts transparent completely;
(2) B phase component (tocopherol acetas, bisabolol, propyl hydroxybenzoate, pigment, essence) is added in the mixture of step (1), maintain the temperature at 100 DEG C, stir to dissolving completely;
(3) be cooled to 95～100 DEG C, mixture is injected in mould, be cooled to 4～12 DEG C of demouldings.
Prepared by embodiment 1～3 to the sun-proof Transparent lipstick of gained and test, detect its fusing point, breaking force, moisten degree, transparency, stability and theoretical sun-proof value
Test result is as shown in the table.
1, fusing point, adopts 2010 editions annex VIC melting point determinations of Chinese Pharmacopoeia;
2, breaking force, adopts the test of lipstick fracture instrument.Under normal circumstances, the lip pomade of 12.7mm diameter, breaking force is in 400-800g scope, in use frangibility not of guarantee.
3, moisten degree, adopt reality to use sensory evaluation, 5 submeters are expressed friendship, and 4 points represent better, and 3 points represent that generally 2 points of expressions are poor, 1 submeter differential; 20 people evaluate rear record data, average;
4, transparency, adopts range estimation evaluation.
5, stability test, refers to test 3 months under four kinds of conditions with 48 DEG C of circulations at 25 DEG C, subzero 18 DEG C, 48 DEG C, subzero 18 DEG C, recovers unchanged after room temperature, can normally use, using this as evaluation criteria.
6, theoretical sun-proof value is to calculate according to the consumption of sunscreen.Under normal circumstances, in the environment of oil-based solvent, the OXYBENZONE of 1% consumption can provide the spf value of 1.5 points, and 1% homosalate can provide the spf value of 1 point, and 1% ethylhexyl salicylate can provide the spf value of 1 point.
According to the test result shown in upper table, can find out, the lip pomade of the embodiment of the present invention 1～3 not only transparency is good, and moistens and spend, and has suitable hardness and reliable melting range, has sun-proof function, and can pass through 3 months stability tests.
Claims (4)
1. a sun-proof Transparent lipstick, is characterized in that this lip pomade is made up of the first component of 90.1wt% and 0.9% second component, wherein, and the mixing that described the first component is following component:
Dibutyl lauroyl glutamine 3.73～4.40wt%,
Mixture 16.42～the 19.40wt% of Polyamide-3 and two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer,
C12-15 alcohol benzoate 16.10～20.00wt%,
Undecylenic acid heptyl ester 13.80～27.10wt%,
BP-3 8.47～10wt%,
Ethylhexyl salicylate 4.23～5.00wt%,
Homosalate 8.47～10.00wt%,
C10-30 acid cholesterol/lanosterol mixed ester 4.85～5.00wt%,
Hydrogenation C6-20 polyolefin 8.21～9.70wt%,
Dextrin isostearate 1.52～1.80wt%,
Described second component is complementary additive,
The percentage by weight sum of each component is 100% above.
2. sun-proof Transparent lipstick according to claim 1, is characterized in that: described complementary additive comprises one or more the mixing in the oil-soluble dyes, activating agent, antioxidant, antiseptic, pigment, aromatic that allow to use at lip according to regulation.
3. sun-proof Transparent lipstick according to claim 1, is characterized in that: in the mixture of described Polyamide-3 and two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer, both ratios are 1:7.
4. the preparation method of sun-proof Transparent lipstick described in claims 1 to 3 any one, its step is as follows:
(1) by the first component, be that dibutyl lauroyl glutamine, Polyamide-3 are mixed homogeneously with mixture, C12-15 alcohol benzoate, undecylenic acid heptyl ester, BP-3, ethylhexyl salicylate, homosalate, C10-30 acid cholesterol/lanosterol mixed ester, dextrin isostearate and the hydrogenation C6-20 polyolefin of two-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer, stirring is warming up to 130～140 DEG C, melts transparent completely;
(2) add second component, maintain the temperature at 100 DEG C, stir to dissolving completely;
(3) be cooled to 95～100 DEG C, mixture is injected in mould, be cooled to 4～12 DEG C of demouldings.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410443334.6A CN104173206B (en) | 2014-09-02 | 2014-09-02 | Sun-proof Transparent lipstick and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410443334.6A CN104173206B (en) | 2014-09-02 | 2014-09-02 | Sun-proof Transparent lipstick and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104173206A true CN104173206A (en) | 2014-12-03 |
| CN104173206B CN104173206B (en) | 2016-09-14 |
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| CN201410443334.6A Expired - Fee Related CN104173206B (en) | 2014-09-02 | 2014-09-02 | Sun-proof Transparent lipstick and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108135828A (en) * | 2015-09-30 | 2018-06-08 | 爱茉莉太平洋股份有限公司 | The eye color make-up constituent of transparent unthickened fuel discrete dosage forms |
| CN109620744A (en) * | 2019-01-03 | 2019-04-16 | 山东珂诺恩生物科技有限公司 | A kind of natural lipstick and preparation method thereof |
| CN111601580A (en) * | 2017-12-26 | 2020-08-28 | 莱雅公司 | Solid anhydrous composition for removing color cosmetics on skin comprising hydrophobic polymers |
| CN111888276A (en) * | 2019-05-06 | 2020-11-06 | 太和康美(北京)中医研究院有限公司 | Lip care compositions containing novel phytosterol additives and methods of making same |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1950060A (en) * | 2004-07-15 | 2007-04-18 | 雅芳产品公司 | Transparent topical cosmetic gel having colored fibers and method of using |
| CN102573766A (en) * | 2009-10-12 | 2012-07-11 | 惠氏有限责任公司 | Sunscreen compositions |
| CN102811697A (en) * | 2011-04-05 | 2012-12-05 | 雅芳产品公司 | Clear or Translucent Composition |
| CN102885699A (en) * | 2012-09-28 | 2013-01-23 | 珀莱雅化妆品股份有限公司 | Transparent lipstick |
-
2014
- 2014-09-02 CN CN201410443334.6A patent/CN104173206B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1950060A (en) * | 2004-07-15 | 2007-04-18 | 雅芳产品公司 | Transparent topical cosmetic gel having colored fibers and method of using |
| CN102573766A (en) * | 2009-10-12 | 2012-07-11 | 惠氏有限责任公司 | Sunscreen compositions |
| CN102811697A (en) * | 2011-04-05 | 2012-12-05 | 雅芳产品公司 | Clear or Translucent Composition |
| CN102885699A (en) * | 2012-09-28 | 2013-01-23 | 珀莱雅化妆品股份有限公司 | Transparent lipstick |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108135828A (en) * | 2015-09-30 | 2018-06-08 | 爱茉莉太平洋股份有限公司 | The eye color make-up constituent of transparent unthickened fuel discrete dosage forms |
| CN111601580A (en) * | 2017-12-26 | 2020-08-28 | 莱雅公司 | Solid anhydrous composition for removing color cosmetics on skin comprising hydrophobic polymers |
| CN111601580B (en) * | 2017-12-26 | 2023-09-05 | 莱雅公司 | Solid anhydrous composition comprising a hydrophobic polymer for removing make-up from the skin |
| CN109620744A (en) * | 2019-01-03 | 2019-04-16 | 山东珂诺恩生物科技有限公司 | A kind of natural lipstick and preparation method thereof |
| CN111888276A (en) * | 2019-05-06 | 2020-11-06 | 太和康美(北京)中医研究院有限公司 | Lip care compositions containing novel phytosterol additives and methods of making same |
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| Publication number | Publication date |
|---|---|
| CN104173206B (en) | 2016-09-14 |
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