CN104173206B - Sun-proof Transparent lipstick and preparation method thereof - Google Patents
Sun-proof Transparent lipstick and preparation method thereof Download PDFInfo
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- CN104173206B CN104173206B CN201410443334.6A CN201410443334A CN104173206B CN 104173206 B CN104173206 B CN 104173206B CN 201410443334 A CN201410443334 A CN 201410443334A CN 104173206 B CN104173206 B CN 104173206B
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Abstract
The invention provides a kind of sun-proof Transparent lipstick, this lip pomade is made up of first component of 90.1wt% and the second component of 0.9%, wherein, described first component is the mixing of following component: dibutyl lauroyl glutamine, kymene hydrogenates the mixture of dimerized linoleic acid ester copolymer with double stearyl ethylenediamine/neopentyl glycols/stearyl alcohols, C12 15 alcohol benzoate, undecylenic acid heptyl ester, benzophenone 3, ethylhexyl salicylate, homosalate, C10 30 acid cholesterol/lanosterol mixed ester, hydrogenation C6 20 polyolefin, dextrin isostearate, described second component is complementary additive.The lip pomade of the present invention can pass through 3 months stability tests, and clear appearance is transparent, and sun-proof result is good, and fusing point is high, and moist degree well, is not easily broken.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of lip pomade, and the preparation method of this lip pomade.
Background technology
Lip pomade is the lip treatment products that people commonly use, and production technology is the most ripe.Along with the continuous progress of science and technology, lip
Cream raw material is constantly brought forth new ideas, and the outward appearance of lip pomade and function are also in diversified development.Transparent lipstick can to consumer bring pure clearly
New impression, is well suited for current consumer and thirsts for breaking away from the psychological need of environmental pollution, wide market.Sun-proof Transparent lipstick
The lip treatment idea of people can be risen to a new level.But at present in China, sun-proof Transparent lipstick is also the trueest
Positive flow into the market places, its reason is that formula is unstable, properties of product are poor, raw material sources channel is limited.
Summary of the invention
It is an object of the invention to for solve the technical problem that above, it is provided that a kind of sun-proof result is good, transparency good,
Moist degree well, the Transparent lipstick that is not easily broken.
It is a further object to provide the preparation method of this sun-proof Transparent lipstick.
For reaching object above, the invention provides a kind of sun-proof Transparent lipstick, this lip pomade is by first component and 0.9% of 90.1wt%
Second component composition, wherein, described first component is the mixing of following component:
Dibutyl lauroyl glutamine 3.73～4.40wt%,
Polyamide-3 hydrogenates the mixture of dimerized linoleic acid ester copolymer with double-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol
16.42～19.40wt%,
C12-15 alcohol benzoate 16.10～20.00wt%,
Undecylenic acid heptyl ester 13.80～27.10wt%,
BP-3 8.47～10wt%,
Ethylhexyl salicylate 4.23～5.00wt%,
Homosalate 8.47～10.00wt%,
C10-30 acid cholesterol/lanosterol mixed ester 4.85～5.00wt%,
Hydrogenation C6-20 polyolefin 8.21～9.70wt%,
Dextrin isostearate 1.52～1.80wt%,
Described second component is complementary additive,
The percentage by weight sum of the most each component is 100%.
Above percentage by weight refers both to component and accounts for the percentage ratio of lip pomade gross weight.
Oil-soluble dyes that " complementary additive " of the present invention includes allowing to use at lip according to regulation, activating agent, anti-
Other conventional compositions used for cosmetic such as oxygen agent, preservative, pigment, aromatic.
Preferably, described Polyamide-3 and double-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer
Mixture in, both ratios are 1:7.
Present invention also offers the preparation method of described sun-proof Transparent lipstick, its step is as follows:
(1) by the first component, i.e. dibutyl lauroyl glutamine, Polyamide-3 and double-stearyl ethylenediamine/neopentyl glycol/
Stearyl alcohol the hydrogenation mixture of dimerized linoleic acid ester copolymer, C12-15 alcohol benzoate, undecylenic acid heptyl ester, benzophenone
-3, ethylhexyl salicylate, homosalate, C10-30 acid cholesterol/lanosterol mixed ester, dextrin isostearate and hydrogen
Changing C6-20 polyolefin mix homogeneously, stirring is warming up to 130～140 DEG C, is completely melt transparent；
(2) add second component, maintain the temperature at 100 DEG C, be evenly stirred until and be completely dissolved；
(3) it is cooled to 95～100 DEG C, injects the mixture in mould, be cooled to 4～12 DEG C of demouldings.
The present invention is creatively by dibutyl lauroyl glutamine and Polyamide-3, double-stearyl ethylenediamine/neopentyl glycol/tristearin
Alcohol hydrogenation dimerized linoleic acid ester copolymer (another title is polyamide-8) collocation uses, in conjunction with various ingredients, and reasonable design
The weight proportion of each component, overcomes defect and the deficiency of existing Transparent lipstick.After tested, the lip pomade of the present invention can be by 3
Month stability test, clear appearance is transparent, and sun-proof result is good, and fusing point is high, and moist degree well, is not easily broken.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is described in further detail, but protection scope of the present invention not only
It is limited to following example.Raw material components involved by various embodiments of the present invention is prior art, can be buied by commercial channel.
Shown according to the form below, each component of weighing embodiment 1～3:
According to following steps, by the sun-proof Transparent lipstick of the component preparation cost invention of embodiment 1～3:
(1) by A phase component (dibutyl lauroyl glutamine, Polyamide-3 and double-stearyl ethylenediamine/neopentyl glycol/hard
Lipidol hydrogenation the mixture of dimerized linoleic acid ester copolymer, C12-15 alcohol benzoate, undecylenic acid heptyl ester, BP-3,
Ethylhexyl salicylate, homosalate, C10-30 acid cholesterol/lanosterol mixed ester, dextrin isostearate and hydrogenation
C6-20 polyolefin) mix homogeneously, stirring is warming up to 130～140 DEG C, is completely melt transparent；
(2) B phase component (tocopherol acetas, bisabolol, propyl hydroxybenzoate, pigment, essence) is added step (1)
Mixture in, maintain the temperature at 100 DEG C, be evenly stirred until and be completely dissolved；
(3) it is cooled to 95～100 DEG C, injects the mixture in mould, be cooled to 4～12 DEG C of demouldings.
The sun-proof Transparent lipstick that embodiment 1～3 prepares gained is tested, detect its fusing point, breaking force, moisten degree, transparent
Degree, stability and theoretical sun-proof value
Test result is as shown in the table.
1, fusing point, uses 2010 editions annex VIC melting point determinations of Chinese Pharmacopoeia；
2, breaking force, uses lipstick fracture instrument test.Under normal circumstances, the lip pomade of 12.7mm diameter, breaking force is in 400-800g scope, ability
Ensure in use to be not easily broken.
3, moistening degree, use actually used sensory evaluation, 5 points represent, 4 points represent preferably, and 3 points represent general, 2 points
Representing poor, 1 point of expression is poor；20 people record data after evaluating, and average；
4, transparency, uses visual evaluation.
5, stability test, refers to test 3 months under the conditions of 48 DEG C of circulations four kinds at 25 DEG C, subzero 18 DEG C, 48 DEG C, subzero 18 DEG C, recovers
After room temperature unchanged, can normally use, in this, as evaluation criteria.
6, theoretical sun-proof value is that the consumption according to sunscreen calculates.Under normal circumstances, in the environment of oil-based solvent, the hexichol of 1% consumption
Ketone-3 can provide the spf value of 1.5 points, the homosalate of 1% that the spf value of 1 point, the ethylhexyl salicylate of 1% can be provided can to provide 1 point
Spf value.
According to the test result shown in upper table, it can be seen that the lip pomade not only transparency of the embodiment of the present invention 1～3 is good, Er Qiezi
Humidity is good, has suitable hardness and reliable melting range, has sun-proof function, and can pass through 3 months stability tests.
Claims (3)
1. a sun-proof Transparent lipstick, it is characterised in that this lip pomade is made up of first component of 90.1wt% and the second component of 0.9wt%, wherein, described first component is the mixing of following component:
Dibutyl lauroyl glutamine 3.73 ~ 4.40wt%,
Polyamide-3 hydrogenates the mixture 16.42 ~ 19.40wt% of dimerized linoleic acid ester copolymer with double-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol,
C12-15 alcohol benzoate 16.10 ~ 20.00wt%,
Undecylenic acid heptyl ester 13.80 ~ 27.10wt%,
BP-3 8.47 ~ 10wt%,
Ethylhexyl salicylate 4.23 ~ 5.00wt%,
Homosalate 8.47 ~ 10.00wt%,
C10-30 acid cholesterol/lanosterol mixed ester 4.85 ~ 5.00wt%,
Hydrogenation C6-20 polyolefin 8.21 ~ 9.70wt%,
Dextrin isostearate 1.52 ~ 1.80wt%,
Described second component is complementary additive,
The percentage by weight sum of the most each component is 100%；
Wherein, described Polyamide-3 is with the mixture of double-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation dimerized linoleic acid ester copolymer, and both ratios are 1:7.
Sun-proof Transparent lipstick the most according to claim 1, it is characterised in that: described complementary additive includes allowing the oil-soluble dyes used at lip, activating agent, antioxidant, preservative, pigment, one or more mixing in aromatic according to regulation.
3. the preparation method of sun-proof Transparent lipstick described in claim 1 or 2, its step is as follows:
(1) by the first component, i.e. dibutyl lauroyl glutamine, Polyamide-3 is mixed homogeneously with double-stearyl ethylenediamine/neopentyl glycol/stearyl alcohol hydrogenation mixture of dimerized linoleic acid ester copolymer, C12-15 alcohol benzoate, undecylenic acid heptyl ester, BP-3, ethylhexyl salicylate, homosalate, C10-30 acid cholesterol/lanosterol mixed ester, dextrin isostearate and hydrogenation C6-20 polyolefin, stirring is warming up to 130 ~ 140 DEG C, is completely melt transparent；
(2) add second component, maintain the temperature at 100 DEG C, be evenly stirred until and be completely dissolved；
(3) it is cooled to 95 ~ 100 DEG C, injects the mixture in mould, be cooled to 4 ~ 12 DEG C of demouldings.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410443334.6A CN104173206B (en) | 2014-09-02 | 2014-09-02 | Sun-proof Transparent lipstick and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410443334.6A CN104173206B (en) | 2014-09-02 | 2014-09-02 | Sun-proof Transparent lipstick and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104173206A CN104173206A (en) | 2014-12-03 |
| CN104173206B true CN104173206B (en) | 2016-09-14 |
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| CN201410443334.6A Expired - Fee Related CN104173206B (en) | 2014-09-02 | 2014-09-02 | Sun-proof Transparent lipstick and preparation method thereof |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102463230B1 (en) * | 2015-09-30 | 2022-11-04 | (주)아모레퍼시픽 | Transparent oil-dispersed fluid type cosmetic composition for eye make-up |
| WO2019126999A1 (en) * | 2017-12-26 | 2019-07-04 | L'oreal | Solid anhydrous composition comprising a hydrophobic polymer for removing makeup on the skin |
| CN109620744B (en) * | 2019-01-03 | 2021-12-07 | 山东珂诺恩生物科技有限公司 | Natural lipstick and preparation method thereof |
| CN111888276B (en) * | 2019-05-06 | 2021-05-04 | 太和康美(北京)中医研究院有限公司 | Lip care composition containing phytosterol additive and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1950060A (en) * | 2004-07-15 | 2007-04-18 | 雅芳产品公司 | Transparent topical cosmetic gel having colored fibers and method of using |
| CN102573766A (en) * | 2009-10-12 | 2012-07-11 | 惠氏有限责任公司 | Sunscreen compositions |
| CN102811697A (en) * | 2011-04-05 | 2012-12-05 | 雅芳产品公司 | Clear or Translucent Composition |
| CN102885699A (en) * | 2012-09-28 | 2013-01-23 | 珀莱雅化妆品股份有限公司 | Transparent lipstick |
-
2014
- 2014-09-02 CN CN201410443334.6A patent/CN104173206B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1950060A (en) * | 2004-07-15 | 2007-04-18 | 雅芳产品公司 | Transparent topical cosmetic gel having colored fibers and method of using |
| CN102573766A (en) * | 2009-10-12 | 2012-07-11 | 惠氏有限责任公司 | Sunscreen compositions |
| CN102811697A (en) * | 2011-04-05 | 2012-12-05 | 雅芳产品公司 | Clear or Translucent Composition |
| CN102885699A (en) * | 2012-09-28 | 2013-01-23 | 珀莱雅化妆品股份有限公司 | Transparent lipstick |
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| CN104173206A (en) | 2014-12-03 |
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