CN105534745B - A kind of emulsification composition and its in the application for preparing grease and dissolving each other in the natural rosemary antioxidant of type - Google Patents
A kind of emulsification composition and its in the application for preparing grease and dissolving each other in the natural rosemary antioxidant of type Download PDFInfo
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- CN105534745B CN105534745B CN201510991135.3A CN201510991135A CN105534745B CN 105534745 B CN105534745 B CN 105534745B CN 201510991135 A CN201510991135 A CN 201510991135A CN 105534745 B CN105534745 B CN 105534745B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention provides a kind of emulsification composition, including raw material composition by mass percentage as follows：Dispersant 5 ~ 20%；Emulsifying agent 15 ~ 45%；Crodaret 20 ~ 35%；Propane diols 20 ~ 45%；The dispersant is trimerization glycerol monosterate or six polyglycerol monooleates；The emulsifying agent is polysorbas20 or this Pan 80.Emulsification composition provided by the invention is after applied to processing rosemary antioxidant processing, the rosemary antioxidant arbitrarily to dissolve each other in oil phase and water phase is obtained, and occur without layering and precipitation, it also retains the antioxygenic property of former antioxidant, beneficial to packaging and transport, application of the rosemary antioxidant in cosmetics is further expanded.
Description
Technical field
The invention belongs to rosemary antioxidant embedding techniques field, more particularly, to a kind of emulsification composition and its
In the application for preparing grease and dissolving each other in the natural rosemary antioxidant of type.
Background technology
Rosemary is a kind of spice berry with a long history, it includes the phenols of a variety of tool antioxidations.Wherein
High-efficiency antioxidant material be bisphenols diterpene, scientific appraisal shows carnosic acid and carnosol is main active ingredient,
Other also have rosmanol etc..
With everybody attention to health, more and more insalubrious chemical compositions are progressively natural in cosmetics
Active ingredient substituted.
Rosemary is widely used in food, health care as a kind of natural, safe and efficient antibacterial, antioxidant by people
The fields such as product, cosmetics, in rosemary main antibacterial, antioxidant content be carnosic acid, ursolic acid, Rosmarinic acid, and this
In three kinds of materials antioxidant effect it is optimal for carnosic acid, but carnosic acid is due to being liposoluble constituent, no matter in emulsion also
Be in aqua all be difficult dispersing and dissolving, so limiting its products application scope in cosmetics significantly.
It there are no at present and handle oil formulation rosemary antioxidant to obtain product and the method that grease dissolves each other.
The content of the invention
A kind of deficiency of the invention according to current oil formulation rosemary antioxidant application range, there is provided emulsifying combination
Thing.
Resist it is another object of the present invention to provide above-mentioned emulsification composition preparing the grease natural rosemary of type that dissolves each other
Application in oxidant.
The technical purpose of the present invention is achieved through the following technical solutions：
The present invention provides a kind of emulsification composition, including raw material composition by mass percentage as follows：
The dispersant is trimerization glycerol monosterate or six polyglycerol monooleates；The emulsifying agent for polysorbas20 or
This Pan 80.
Since rosemary antioxidant sheet is as fat-soluble product, if emulsification is insufficient, unstable, the product can be made to exist
Because oil-in-water is not thorough, scattered uneven in application process, the appearance of product, application effect and basic anti-oxidant are ultimately resulted in
Effect etc. is reduced even without effect, because carnosic acid oil formulation to be carried out to the emulsification of complete stability, is actually sought to it
Uniformly embedded and disperseed in end product, its anti-oxidant effect will not be caused because of the influence of water even in aqueous
Fruit declines, and stable embedding and dispersiveness can ensure excellent and balanced antioxidant effect.
Therefore, emulsification needs the composite factors such as stability, dispersiveness, solubilising, defoaming to play a role jointly, could realize
Optimal emulsifying effectiveness.
Preferably, the emulsification composition is made of raw material as follows by mass percentage：
It is highly preferred that the emulsification composition is made of raw material as follows by mass percentage：
It is highly preferred that the emulsification composition is made of raw material as follows by mass percentage：
The present invention also provides a kind of molten type rosemary antioxidant of grease two, including the raw material of following component to be made：
Emulsification composition 65%~70%
Carnosic acid oil formulation 30~35%；
The raw material that the emulsification composition includes following component forms：
The dispersant is trimerization glycerol monosterate or six polyglycerol monooleates；The emulsifying agent for polysorbas20 or
This Pan 80.
Wherein, carnosic acid content is 10~30% in carnosic acid oil formulation.
Preferably, the emulsification composition is made of the raw material of following components：
The molten type rosemary antioxidant preparation process of grease two of the present invention is：Respectively by carnosic acid oil formulation and emulsification group
Compound dissolves in advance, above-mentioned both material mixing, homogeneous that then will have been dissolved, up to the molten type rosemary antioxygen of the grease two
Agent.
Specific aim of the present invention screens excellent safely and effectively emulgate ingredient, and by emulsifying technology, fat-soluble fan is changed
Fragrant extract carnosic acid oil formulation is combined with food-grade emulgate ingredient compounding, and being finally prepared into can be in aqua, finish, emulsion
In any miscible natural product.
Compared with prior art, the invention has the advantages that：
Emulsification composition provided by the invention is applied in fat-soluble rosemary antioxidant product, and being prepared can
With the system arbitrarily dissolved each other in oil phase and water phase, and the system occurs without layering and precipitation, also retains former antioxidant
Antioxygenic property, beneficial to packaging and transport, further expands application of the rosemary antioxidant in cosmetics.
Embodiment
The present invention is specifically described below by embodiment, it is necessary to which indicated herein is that the present embodiment is served only for pair
The present invention is further described, but it is not intended that limiting the scope of the invention, the person skilled in the art in the field
Some nonessential modifications and adaptations can be made according to the content of the invention described above.
Unless stated otherwise, the reagent of the invention used, method and apparatus for the art conventional reagent, method and are set
It is standby.
Embodiment 1：It is natural based on carnosic acid oil formulation to be prepared into the two molten type of grease that is widely used in cosmetic product
The proportioning component of antioxidant is following (by percentage to the quality)：
Auxiliary material：70%, carnosic acid oil formulation (10~30% content) 30%.
Wherein, adjunct ingredient is as follows：Trimerization glycerol monosterate 5%, RH40 Crodarets 15%, spits
Warm 20 (20%), propane diols 30%.
Preparation method is as follows：By carnosic acid content be 10% -30% carnosic acid oil formulation in 75~80 DEG C of water-baths
In fully dissolve.Then by the above-mentioned auxiliary material component compounded in 45~50 DEG C of water-baths it is slightly hot miscible.Finally, by above-mentioned two
Person carries out whirlpool mixing, homogeneous into transparent mixed solution.
Embodiment 2：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material 65%, carnosic acid oil formulation：30%
Wherein, trimerization glycerol monosterate 10%, RH40 Crodarets：20%, polysorbas20 (10%),
Propane diols 25%,
Embodiment 3：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：65%, carnosic acid oil formulation：35%
Wherein, six polyglycerol monostearate：10%, this Pan 80：25%, RH40 Crodaret：15%,
Propane diols：15%
Embodiment 4：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：70%, carnosic acid oil formulation：30%
Wherein, six polyglycerol monostearate：5%, this Pan 80：30%, RH40 Crodaret：20%,
Propane diols：15%.
Comparative example 1：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：65%, carnosic acid oil formulation：35%
Wherein, six polyglycerol monostearate：20%, this Pan 80：35%, RH40 Crodaret：5%,
Propane diols：5%.
Comparative example 2：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：70%, carnosic acid oil formulation：30%
Wherein, six polyglycerol monostearate：25%, this Pan 80：5%, RH40 Crodaret：10%,
Propane diols：30%.
Comparative example 3：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material 65%, carnosic acid oil formulation：35%
Wherein, trimerization glycerol monosterate 15%, RH40 Crodarets：40%, polysorbas20 (5%),
Propane diols 5%.
Comparative example 4：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material 70%, carnosic acid oil formulation：30%
Wherein, trimerization glycerol monosterate 5%, RH40 Crodarets：5%, polysorbas20 (5%), third
Glycol 55%.
Comparative example 5：
Formulation ratio and preparation method are with embodiment 1, the difference is that substituting polysorbas20 using Tween 80.
Comparative example 6
Formulation ratio and preparation method are with embodiment 2, the difference is that substituting the polyethylene glycol hydrogenated castors of RH40 using polysorbate60
Sesame oil.
Comparative example 7
Formulation ratio and preparation method are with embodiment 3, the difference is that substituting six polyglycereol monostearates using poloxamer
Ester.
Comparative example 8
Formulation ratio and preparation method are with embodiment 4, the difference is that substituting this using diacetyl tartarate list double glyceride
Pan 80.
Comparative example 9：
Formulation ratio and preparation method are with embodiment 4, the difference is that substituting propane diols using polyethylene glycol 400.
Comparative example 10：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：70%, carnosic acid oil formulation：30%
Wherein, six polyglycerol monostearate：0%, this Pan 80：30%, RH40 Crodaret：20%,
Propane diols：20%.
Comparative example 11：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：70%, carnosic acid oil formulation：30%
Wherein, six polyglycerol monostearate：20%, this Pan 80：0%, RH40 Crodaret：30%,
Propane diols：20%.
Comparative example 12：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：70%, carnosic acid oil formulation：30%
Wherein, six polyglycerol monostearate：20%, this Pan 80：30%, RH40 Crodaret：0%,
Propane diols：20%.
Comparative example 13：Preparation method is widely used in cosmetics production with embodiment 1 based on carnosic acid oil formulation is prepared into
The proportioning component of the molten type natural of grease two of product is as follows：
Auxiliary material：70%, carnosic acid oil formulation：30%
Wherein, six polyglycerol monostearate：20%, this Pan 80：30%, RH40 Crodaret：20%,
Propane diols：0%.
Blank example：
Without emulsification, the carnosic acid oil formulation for being original 3% -10%.
1st, dissolubility, dispersivity test：
The sample that above-described embodiment and comparative example are formulated respectively is taken into isodose, be added drop-wise to respectively in moisture retention water carry out it is molten
Xie Xing, dispersivity test, by observing its stability in aqueous after mixing, standing more than 12h.
2nd, Oxidation Resistance Test：The Oxidation Resistance Test of grease is done using olive oil in cosmetics register, is used videotape to record by cosmetics name
Limitation addition to be closed, under the conditions of 45 DEG C, does strenuous test, experimental period is two weeks, the peroxide value change of detection in every 3 days,
Appreciation gist is used as using the numerical value of last time.
The impact of performance of rosemary antioxidant in 1 embodiment 1~4 of table
The impact of performance of rosemary antioxidant in 2 comparative example 1~9 of table
Analysis of conclusion：
As can be seen from the above table, the basic recipe of comparative example 1~4 is consistent with embodiment, but due to the percentage of each component
There is bigger difference, its final in water dispersiveness and solubility to dispersion is all poor in grease, and oxidation resistance dies down.And
The formulation ratio and preparation method of comparative example 5~9 are respectively with embodiment 1~4, but due to substituted for different emulsifying agent, scattered
Agent, its final in water dispersiveness and grease dispersiveness is also very poor, and oxidation resistance dies down.Blank example sheet is made as oil
Agent, so bad dispersibility in water, the dissolubility good dispersion in grease, and the antioxidant effect in vegetable fat are also very
It is good.
In addition, comparative example 10~13 is due to lacking one kind in instant component, the emulsifiability that it is showed is not yet
It is good.
For example, comparative example 1 is the increase of six polyglycerol monostearate contents, the increase of this material is to emulsification composition
Emulsification and dispersion effect influence less, but it is relatively poor in cold water stability, while the reduction of RH40 and propane diols ratio
Corresponding solubilising and hydrophily effect is set to reduce and ultimately result in its emulsion stability variation.
Comparative example 2 reduces for the proportion of this Pan 80, due to the content reduction mainly as emulsifier component, although not influencing
Its dispersiveness, but stability is bad, and also there is aggregation in levels, its emulsification is not abundant.
Comparative example 5 substitutes polysorbas20 for Tween 80, although Tween 80 emulsibility and solubilising are all much like with polysorbas20,
Through the finish of Tween 80 emulsification, its hydrophily can not show a candle to polysorbas20, so the carnosic acid oil formulation after being emulsified with Tween 80 is in water
It is middle because hydrophily is poor and is not easy to disperse.
From the point of view of the interpretation of result of upper table, it is anti-oxidant to prepare a kind of two molten type of grease for being widely used in cosmetic product
Agent, the type selecting collocation of emulgate ingredient and ratio all serve very crucial.
The molten type antioxidant of the grease two for being widely used in cosmetics of the embodiment of the present invention 1~4 contain antibacterial anti-inflammatory into
Point, without adding chemical antimicrobial antiphlogistic component, and pass through human skin patch test, it is safe and efficient.Test method and result
It is as follows：
Tested material：It with the addition of the hydrosol of the molten type antioxidant of grease two of embodiment 1~4.
Negative control：Blank control.
Subject：Totally 30 people, male 15 people, 15 people of female, at 18-35 years old ages, meet subject and volunteer inclusion criteria.
Spot method for testing：Select qualified spot examination device, in closed patch test method, by tested material about 0.02ml~
0.025ml is applied in spot examination device, and external application special adhesive tape is pasted on subject's forearm song side, 24 it is small when after remove tested material, in going
Except 30min after tested material spot examination device, dermoreaction is observed after impression disappearance, is pressed《Cosmetics health specification》In (version in 2007)
Dermoreaction grade scale records its result.
Evaluation of result：Reaction result is recorded by table 3 (skin adverse reaction grade scale).
3 skin adverse reaction grade scale of table
Result of the test (see the table below 4)
Table 4
Analysis of conclusion：
The above results show that：In embodiment 1,2,3,4,30 all negative (grading systems of subjects skin：0
Level).Foundation《Cosmetics health specification》(version in 2007) human skin class patch experiment criterion, sample to human body without skin not
Good reaction.
Claims (4)
- A kind of 1. two natural rosemary antioxidant of molten type of grease, it is characterised in that the molten type Rosemary antioxidant of grease two Agent includes the raw material of following component：Emulsification composition 65% ~ 70%；Carnosic acid oil formulation 30 ~ 35%；Wherein, carnosic acid content is 10 ~ 30% in carnosic acid oil formulation；The emulsification composition is made of the raw material of following components：Trimerization glycerol monosterate 7 ~ 16%；Polysorbas20 15 ~ 30%；Crodaret 20 ~ 32%；Propane diols 20 ~ 43%.
- A kind of 2. two natural rosemary antioxidant of molten type of grease, it is characterised in that the molten type Rosemary antioxidant of grease two Agent includes the raw material of following component：Emulsification composition 65% ~ 70%；Carnosic acid oil formulation 30 ~ 35%；Wherein, carnosic acid content is 10 ~ 30% in carnosic acid oil formulation；The emulsification composition is made of the raw material of following components：Six polyglycereol monostearates 5 ~ 10%；This Pan 80 15 ~ 43%；Crodaret 20 ~ 32%；Propane diols 20 ~ 43%.
- 3. the preparation method of any two natural rosemary antioxidant of molten type of grease of claim 1~2, it is characterised in that Carnosic acid oil formulation and emulsification composition are dissolved in advance respectively, above-mentioned both material mixing, the homogeneous that then will have been dissolved, Up to the molten type rosemary antioxidant of the grease two.
- 4. application of any molten type rosemary antioxidant of grease two of claim 1~2 in cosmetic product.
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| CN106036355A (en) * | 2016-08-20 | 2016-10-26 | 陈爱梅 | Preparation method of antioxidant |
| CN108635259B (en) * | 2018-05-16 | 2020-12-01 | 河南中大恒源生物科技股份有限公司 | Oil-water soluble rosemary extract and preparation method and application thereof |
| CN110507611A (en) * | 2019-08-23 | 2019-11-29 | 中国医科大学 | A kind of carnosic acid nanometer emulsion oral liquid and preparation method thereof |
| CN115043724B (en) * | 2022-07-21 | 2024-09-17 | 海南舒普生物科技有限公司 | Carnosic acid oil preparation and preparation method thereof |
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|---|---|---|---|---|
| JPH1129432A (en) * | 1997-07-04 | 1999-02-02 | Shiseido Co Ltd | Water-in-oil type emulsion composition |
| CN101028461A (en) * | 2007-03-30 | 2007-09-05 | 吴敏 | Job's tears nut oil self-emusifying preparation and its making method |
| CN101971984A (en) * | 2010-09-06 | 2011-02-16 | 南昌大学 | Preparation method of DHA microemulsion |
| CN101982109A (en) * | 2010-09-06 | 2011-03-02 | 南昌大学 | Method for preparing cinnamon oil microemulsion |
-
2015
- 2015-12-24 CN CN201510991135.3A patent/CN105534745B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1129432A (en) * | 1997-07-04 | 1999-02-02 | Shiseido Co Ltd | Water-in-oil type emulsion composition |
| CN101028461A (en) * | 2007-03-30 | 2007-09-05 | 吴敏 | Job's tears nut oil self-emusifying preparation and its making method |
| CN101971984A (en) * | 2010-09-06 | 2011-02-16 | 南昌大学 | Preparation method of DHA microemulsion |
| CN101982109A (en) * | 2010-09-06 | 2011-03-02 | 南昌大学 | Method for preparing cinnamon oil microemulsion |
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