CN104163525B - 一种溴化制备溴氨酸钠盐的生产废水的处理方法 - Google Patents
一种溴化制备溴氨酸钠盐的生产废水的处理方法 Download PDFInfo
- Publication number
- CN104163525B CN104163525B CN201410433141.2A CN201410433141A CN104163525B CN 104163525 B CN104163525 B CN 104163525B CN 201410433141 A CN201410433141 A CN 201410433141A CN 104163525 B CN104163525 B CN 104163525B
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- Prior art keywords
- waste water
- processing method
- sodium salt
- acid sodium
- adsorbent
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- 239000002351 wastewater Substances 0.000 title claims abstract description 39
- TXMRAEGWZZVGIH-UHFFFAOYSA-M sodium;1-amino-4-bromo-9,10-dioxoanthracene-2-sulfonate Chemical compound [Na+].O=C1C2=CC=CC=C2C(=O)C2=C1C(Br)=CC(S([O-])(=O)=O)=C2N TXMRAEGWZZVGIH-UHFFFAOYSA-M 0.000 title claims abstract description 22
- 238000003672 processing method Methods 0.000 title claims abstract description 19
- 238000005893 bromination reaction Methods 0.000 title claims abstract description 17
- 230000031709 bromination Effects 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 claims abstract description 22
- 239000003463 adsorbent Substances 0.000 claims abstract description 13
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims description 12
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical group O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 235000006408 oxalic acid Nutrition 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 235000010265 sodium sulphite Nutrition 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 150000002500 ions Chemical class 0.000 claims description 2
- 238000004065 wastewater treatment Methods 0.000 abstract description 5
- 238000002360 preparation method Methods 0.000 abstract description 2
- 238000004064 recycling Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 239000000706 filtrate Substances 0.000 description 9
- 239000012528 membrane Substances 0.000 description 9
- 239000005416 organic matter Substances 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000009835 boiling Methods 0.000 description 4
- 239000012141 concentrate Substances 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 3
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
- 229910052794 bromium Inorganic materials 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 238000003828 vacuum filtration Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- QZZSAWGVHXXMID-UHFFFAOYSA-N 1-amino-4-bromo-9,10-dioxoanthracene-2-sulfonic acid Chemical compound C1=CC=C2C(=O)C3=C(Br)C=C(S(O)(=O)=O)C(N)=C3C(=O)C2=C1 QZZSAWGVHXXMID-UHFFFAOYSA-N 0.000 description 1
- PZSHANOBYYVNEX-UHFFFAOYSA-N 1-amino-9,10-dioxoanthracene-2-sulfonic acid Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC(S(O)(=O)=O)=C2N PZSHANOBYYVNEX-UHFFFAOYSA-N 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- -1 bromamine acid sodium salts Chemical class 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003014 ion exchange membrane Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005374 membrane filtration Methods 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
Landscapes
- Water Treatment By Sorption (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
Claims (6)
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CN201410433141.2A CN104163525B (zh) | 2014-08-28 | 2014-08-28 | 一种溴化制备溴氨酸钠盐的生产废水的处理方法 |
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CN201410433141.2A CN104163525B (zh) | 2014-08-28 | 2014-08-28 | 一种溴化制备溴氨酸钠盐的生产废水的处理方法 |
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CN104163525A CN104163525A (zh) | 2014-11-26 |
CN104163525B true CN104163525B (zh) | 2016-09-07 |
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CN201410433141.2A Active CN104163525B (zh) | 2014-08-28 | 2014-08-28 | 一种溴化制备溴氨酸钠盐的生产废水的处理方法 |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107400071A (zh) * | 2017-05-25 | 2017-11-28 | 盐城市瓯华化学工业有限公司 | 一种溴氨酸生产方法 |
CN109439013B (zh) * | 2018-12-12 | 2020-05-01 | 浙江闰土研究院有限公司 | 一种除溴氨酸类酸性染料中的铜和杂质的方法 |
CN114105832A (zh) * | 2021-12-02 | 2022-03-01 | 江苏亚邦染料股份有限公司 | 一种溴氨酸钠盐的环保生产工艺 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101041476A (zh) * | 2007-02-28 | 2007-09-26 | 南京师范大学 | 氨基c酸酸性废水的回收处理方法 |
CN101104533A (zh) * | 2007-06-05 | 2008-01-16 | 南开大学 | 一种h-酸生产废水的处理方法 |
CN101177310A (zh) * | 2007-11-02 | 2008-05-14 | 西南石油大学 | 一种含有机染料废水处理剂的制备方法 |
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2014
- 2014-08-28 CN CN201410433141.2A patent/CN104163525B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101041476A (zh) * | 2007-02-28 | 2007-09-26 | 南京师范大学 | 氨基c酸酸性废水的回收处理方法 |
CN101104533A (zh) * | 2007-06-05 | 2008-01-16 | 南开大学 | 一种h-酸生产废水的处理方法 |
CN101177310A (zh) * | 2007-11-02 | 2008-05-14 | 西南石油大学 | 一种含有机染料废水处理剂的制备方法 |
Non-Patent Citations (1)
Title |
---|
聚合吸附-离子交换法用于染色废水的脱色;卓宜安;《丝绸》;19781231(第04期);46-48 * |
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Effective date of registration: 20230703 Address after: 222000 duigougang Town, Guannan County, Lianyungang City, Jiangsu Province (Chemical Industrial Park) Patentee after: JIANGSU HUAER CHEMICAL Co.,Ltd. Address before: No. 105, Renmin West Road, Niutang Town, Wujin District, Changzhou City, Jiangsu Province, 213168 Patentee before: Jiangsu Yabang Dye Co.,Ltd. |
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Address after: 222000 duigougang Town, Guannan County, Lianyungang City, Jiangsu Province (Chemical Industrial Park) Patentee after: Jiangsu Yabang Wall Dyestuff Co.,Ltd. Country or region after: China Address before: 222000 duigougang Town, Guannan County, Lianyungang City, Jiangsu Province (Chemical Industrial Park) Patentee before: JIANGSU HUAER CHEMICAL Co.,Ltd. Country or region before: China |