CN104146157B - A kind of narrow leaved tea tree sets oily feed addictive preparation method - Google Patents
A kind of narrow leaved tea tree sets oily feed addictive preparation method Download PDFInfo
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- CN104146157B CN104146157B CN201410442511.9A CN201410442511A CN104146157B CN 104146157 B CN104146157 B CN 104146157B CN 201410442511 A CN201410442511 A CN 201410442511A CN 104146157 B CN104146157 B CN 104146157B
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Abstract
The invention discloses a kind of Australia tea tree oil (narrow leaved tea tree tree oil) feed addictive preparation method and the using method giving part livestock edible.Its step includes: the essential oil by terpineol-4 content being 30-40%, after three intensifications, insulation, makes essential oil be cooled to normal temperature; Add running water and vitamin E mixing, after adding thermal agitation, load container, after stirring with high-speed shearing machine, be filled into bottle and make additive.Additive is made dilution: dilute by the different proportion of additive and water, as the drinking water going out shell chicken, or as going out the drinking water of shell chicken after 7 days, or as the drinking water of small weaning pig, or as the drinking water of wean piggy after 10 days.Use the present invention as feed addictive or feedstuff additive feeding animals, the immunity of animal can be improved, can birds flu-preventing, prevention animal flu and other diseases.
Description
Technical field
The present invention relates to a kind of feed addictive preparation method, particularly relate to a kind of Australia tea tree oil (narrow leaved tea tree tree oil) feed addictive preparation method and preparing product using method.
Background technology
Australia tea tree oil is a kind of trade name, and its formal name used at school is narrow leaved tea tree tree oil.Narrow leaved tea tree tree is that primary growth is in a kind of bushes of Australian southeastern coast.Australia tea tree oil is used for wound disinfection by aborigines and has history in several thousand.Australia's tea oil successfully listed European Pharmacopoeia in 2000, had obtained the approval of the approval of Chinese Bureau of Drugs Supervision and U.S. FDA as food flavor additive.
Find that Australia tea tree oil can effectively suppress a lot of Causative virus through recent studies, have very large effect for treatment numerous disease and wound.As bone is ached, burn, flu etc.Due to the excellent specific property of Australia tea tree, introduce a fine variety in a lot of country, also have plantation in areas such as the Guangdong of China, Yunnan.
Along with the reach of science, free radical is considered to cause mankind aging, diseases induced, DNA mutation and cause the arch-criminal of tumour.The antioxidant of some scavenging free radicals is in succession found and has been applied in our daily life, as deep sea fish oil, lycopene, shrimp Celadon element, white profound extra large krill wet goods.Study in various applicable natural scientist, find that the terpineol-4 (terpinol-4) in the tea oil of Australia has extremely strong oxidation resistance, through the effort of recent two decades, Australia scientist is successful at first gathers and processes edible terpineol-4 essential oil from Australia tea tree.Detect through U.S. BROWNSWICKLAB, the ability of Australian tea tree ethereal oil scavenging free radicals is 4 times of white profound extra large krill oil, 30 times of Shi Xia Celadon element, 25 times of lycopene, 200 times of deep sea fish oil.Australia's tea tree ethereal oil not only has extremely strong antioxidation, have the function killing obstinate virus concurrently simultaneously, live body chicken embryo through Zhejiang Center For Disease Control and Prevention is tested, and has proved all avian influenza virus of H1N1, H5N1, H3N2, H7H9 can killed in chicken embryo.And similar experiment is in the world, and many places are all underway.
In sum, Australian tea oil (narrow leaved tea tree tree oil) being refined through giving secondary on essential oil basis, changing the molecular structure of original essential oil, making it some indexs and changed.With terpineol-4, this is an important indicator of antioxidant, and index is higher, and oxidation resistance is stronger, improves immunity ability stronger.From Australian tea oil (the narrow leaved tea tree tree oil) essential oil that factory produces for the first time, terpineol-4 numerical value content of manufactured goods is only 30-40%, and containing certain toxicity, only be used in cosmetics, skin care item, a small amount of flavoring essence additive etc., can not directly eat.
The chicken of current China, pig etc. bird, meat, needs within growth period that regular to give antibiotic etc. medicine disease-resistant, and this brings health hazard fundamentally to the edible of people.People utilize natural food as feed addictive in searching always, join in animal feed, improve the immunity of animal thus, birds flu-preventing, animal flu and other diseases.
Summary of the invention
Technical problem: the invention reside in and overcome the deficiencies in the prior art, provides a kind of narrow leaved tea tree to set oily feed addictive preparation method and application.
Technical scheme:
With regard to existing Australian tea oil (narrow leaved tea tree tree oil) essential oil, terpineol-4 numerical value content of its manufactured goods is 30-40%, secondary refines on this basis, under the prerequisite of not adding any chemical assistant, reduce toxic component, terpineol-4 numerical value content of manufactured goods is 60-66%.Essential oil after secondary refines is as animal feed additive and feedstuff additive, and to the immunity that can improve animal after feeding animal, birds flu-preventing, prevention animal catches a cold and other diseases.This numeral (not using any chemical assistant, content 60-66%) of newly making of terpineol-4, determines the oxidation resistance of this novel tea oil greatly higher than health products on market, such as astaxanthin, Co-Q10 etc.Demonstrate the general level of the health substantially increasing animal simultaneously.
Concrete scheme is as follows:
A kind of narrow leaved tea tree sets oily feed addictive preparation method, comprises the following steps:
Step 1: be that the essential oil that 30-40% extracts for the first time loads reactor as raw material using terpineol-4 content, is filled with nitrogen, keeps 0.2kg/CM in reactor
2-1kg/CM
2pressure, through three intensifications, insulation, is specially:
1) 30-45 DEG C is warming up to, insulation 50-60 minute;
2) be warming up to 45-70 DEG C, be incubated 60 minutes;
3) heat to 70-85 DEG C, be incubated 60 minutes;
After three times the process of heating terminates, essential oil is made to be cooled to normal temperature;
Step 2: take out the essential oil processed, adds water and vitamin E mixing; Essential oil: water: the ratio of vitamin E is 20:1000:5, first water and vitamin E are heated 90 DEG C stir after, add essential oil, with high-speed shearing machine stir after, be filled into bottle.
Described water can be pure water, distilled water or running water.
The additive of described step 2 gained is made dilution:
By additive: water is 1:1000 dilution, as the drinking water going out shell chicken;
By additive: water is 2:1000 dilution, as the drinking water going out shell chicken after 7 days.
The additive of described step 2 gained is made dilution:
By additive: water is 1:250 dilution, as the drinking water of small weaning pig;
By additive: water is 1:125 dilution, and the drinking water as wean piggy after 10 days is extremely sold.
Beneficial effect:
From plant produced Australian tea oil out (narrow leaved tea tree tree oil) essential oil, terpineol-4 numerical value content of manufactured goods is 30-40%.Present invention process secondary on special equipment refines, under the prerequisite of not adding any chemical assistant, terpineol-4 numerical value content of manufactured goods is 60-66%, and this numeral, determines the oxidation resistance of this novel tea oil greatly higher than astaxanthin etc. health products.
Australian tea oil (the narrow leaved tea tree tree oil) feed addictive that the present invention makes, is natural gathering and processing, acts on animal bodies, can make it to improve immunity, and not containing any toxic and side effect.Thus be specifically used in chicken, pig etc. meat, bird feeds, with it not containing hormone, not containing antibiotic, rely on the extremely strong oxidation resistance of self, greatly improve the immunity of animal, thus can birds flu-preventing, prevention animal flu and other diseases.Improve the general level of the health of animal greatly.
The present invention gives animal as feed addictive or feedstuff additive feeding, solves Australian tea oil (narrow leaved tea tree tree oil) essential oil never in the problem that animal directly eats.
Accompanying drawing explanation
Fig. 1 is that narrow leaved tea tree sets oily main component, the test data contrast tables such as raw material essential oil, essential oil of the present invention, Australia standard, New Zealand Standard.
Fig. 2 is the comparison diagram that free radical ability driven away by essential oil of the present invention and various antioxidant.
Detailed description of the invention
The invention will be further described for binding tests data.
1. a narrow leaved tea tree is set in oily feed addictive preparation method step 1 and is: the essential oil loading reactor by terpineol-4 content being 30-40%, open nitrogen cylinder, this nitrogen role be to the narrow leaved tea tree tree essential oil in reactor when chemical reaction, play stabilization.Then pressurize, 0.2kg/CM in reactor
2-1kg/CM
2during pressure, be warming up to 30-45 DEG C, insulation 50-60 minute; Allow pressure and temperature act on narrow leaved tea tree tree essential oil, make it chemical reaction occurs.Open oil circulating pump simultaneously, allow essential oil constantly circulate in reactor, realize the abundant reaction of essential oil.Be warming up to 45-70 DEG C of insulation 60 minutes again; Pressure keeps 0.2kg/CM
2-1kg/CM
2pressure, then heats to 70-85 DEG C, is incubated 60 minutes; Still 0.2kg/CM is kept
2-1kg/CM
2pressure, is finally cooled to normal temperature with cooling water in pancake coil.Turn off air compressor machine, turn off nitrogen, stop the circulation of essential oil.Very strong volatile feature is had in this process according to narrow leaved tea tree tree oil, the impurity in narrow leaved tea tree tree essential oil and unwanted composition are driven away, retain and improve need composition, just can output we need contain high anti-oxidation ability, the product oil of immunity can be improved.Terpineol-4 numerical value content of the essential oil manufactured goods after being refined by the secondary of above-mentioned steps gained is 60-66%.
This test data can detect with 9790 type gas chromatographs.
See Fig. 1, can find out that from the table of comparisons in the product that the present invention produces, terpineol-4 content is much better than the raw material essential oil content of tea oil factory, be much better than Australia, Zelanian national standard, this index improves the most important index of immunity, is the most important thing.
Concrete implementation example:
1, be that the essential oil of 30-40% loads reactor by terpineol-4 content, be filled with nitrogen, keep 0.2kg/CM in reactor
2pressure, through three intensifications, insulation, is specially:
1) be warming up to 30 DEG C, be incubated 50 minutes;
2) be warming up to 45 DEG C, be incubated 60 minutes;
3) heat to 70 DEG C, be incubated 60 minutes;
After three times the process of heating terminates, essential oil is made to be cooled to normal temperature.
2, be that the essential oil of 30-40% loads reactor by terpineol-4 content, be filled with nitrogen, keep 1kg/CM in reactor
2pressure, through three intensifications, insulation, is specially:
1) be warming up to 45 DEG C, be incubated 60 minutes;
2) be warming up to 70 DEG C, be incubated 60 minutes;
3) heat to 85 DEG C, be incubated 60 minutes;
After three times the process of heating terminates, essential oil is made to be cooled to normal temperature.
3, be that the essential oil of 30-40% loads reactor by terpineol-4 content, be filled with nitrogen, keep 0.5kg/CM in reactor
2pressure, through three intensifications, insulation, is specially:
1) be warming up to 40 DEG C, be incubated 55 minutes;
2) be warming up to 60 DEG C, be incubated 60 minutes;
3) heat to 80 DEG C, be incubated 60 minutes;
After three times the process of heating terminates, essential oil is made to be cooled to normal temperature.
To the essential oil that above-mentioned 1-3 specific embodiment refines, add running water and vitamin E mixing; Essential oil: running water: the ratio of vitamin E is 20:1000:5, glass beaker is put into running water and vitamin E, thermal agitation is added with heating mixer, after being warming up to 90 DEG C, add essential oil, after stirring with high-speed shearing machine, allow essential oil: running water: vitamin E fully mixes, then be filled into bottle.
Be illustrated specifically to raise test case below:
1, for the chicken in bird
1) take out shell 3 days little white feather chickens 27 chickens, weigh and weigh altogether 1209.6 grams (average 44.8 grams).With additive, vitamin E, the mixed finished product dilution of water of gained of the present invention; By the dilution of dilution 1:1000 water, put into tank or water fountain, abdicate shell chicken diet voluntarily; Within 7 days, press the dilution of dilution 2:1000 water afterwards, put into tank or water fountain, allow chicken diet voluntarily; Within 28th day, be weighed as average 13365 grams (average 495 grams).Within 40th day, to weigh average 32400 (average 1200 grams).Without dead.
2) without additive situation: take out shell 3 days little white feather chickens 27 chickens, weigh and weigh altogether 1236.6 grams (average 45.8 grams).Diet antibiotic and Cold proof medicine, be weighed as 9698 grams (average 421 grams) on the 28th day by 7 days dead 4.Within 40th day, to weigh 23460 (average 1020 grams).Dead 4.
By above-mentioned contrast, can find out that the chicken of the additive taking gained of the present invention is owing to improve immunity, healthy, body weight is compared and is able to normal increase.The death rate is lower.
2, for the pig in domestic animals
1) small weaning pig 5 is got, 71500 grams (average 14300 grams) additive, vitamin E, mixed finished product dilution of water with gained of the present invention of weighing; By the dilution of dilution 1:250 water, put into tank or water fountain, allow small weaning pig diet voluntarily; Within 10 days, press the dilution of dilution 1:125 water afterwards, put into tank or water fountain by pig diet voluntarily; Within 60 days, weigh 125500 grams (average 25100 grams), within 105 days, weigh 267500 grams (average 53500 grams), within 125 days, weigh 344000 grams (average 68800 grams).Without dead.
2) without additive situation: get small weaning pig 5 weigh 75500 grams (average 15100 grams) normally give antibiotic and Cold proof medicine.Within 60 days, weigh 93000 grams (average 23250 grams), within 105 days, weigh 191500 grams (average 47875 grams), within 125 days, weigh 191500 grams (average 63833 grams), dead 1.
By above-mentioned contrast, can find out that the piggy of the additive taking gained of the present invention is owing to improve immunity, healthy, body weight is compared and is able to normal increase.The death rate is lower.
Because narrow leaved tea tree tree oil has the characteristic improving immunity widely, by that analogy, according to animal food habit and feeding method, the additive of this invention gained, according to body weight, the feature of food-intake, after the adjustment of certain ratio, ox can be given, sheep, duck, goose, pigeon, rabbit etc. feeding animal, equally can obtain good health effect.
Meanwhile, this invention not only can use the form of aqua, can also with the form of capsule to animal edible.
Can also mix with feed, give feeding animal with the form of feed.
The applicable animal range of this invention is extensive, and using method is also varied.
Be illustrated with bird flu test below:
Get Strain (A type H4N4, H7N9, H3N2, H5N4), chicken embryo, GPRBC, MEM maintenance medium, dilution.Material medicine is done with the additive of gained of the present invention.
Experiment is established: positive control: with Tamiflu medicine and Experimental agents parallel laboratory test.
Viral dose contrast (100EID50): 100,10,1,0.1EID50: negative control.
By H1N1, the additive inoculation egg embryo of H7N9, H3N2, H5N4 dilution and this present invention gained, find that the additive of this present invention gained is to type A avian influenza H1N1 according to different proportionings, H7N9, H3N2, H5N4 have inhibitory action:
(1) concentration of A type H3N2 influenza virus can be suppressed completely to be 1:5,1:10;
(2) concentration of A type H5N4 influenza virus can be suppressed completely to be 1:5;
(3) concentration of A type H4N4 influenza virus can be suppressed completely to be 1:5,1:10;
(4) concentration of A type H7N9 influenza virus can be suppressed completely to be 1:5,1:10.
Fig. 2 is the comparison diagram that free radical ability driven away by additive of the present invention and various antioxidant.Narrow leaved tea tree tree is oily after refining through secondary, with the contrast of the various active ingredient Scavenging ability in nutrient and healthcare products.This shows, additive of the present invention is due to its distinctive Strong oxdiative ability, so its some health products compared on the market has the ability of stronger scavenging free radicals.
Claims (1)
1. narrow leaved tea tree sets an oily feed addictive preparation method, it is characterized in that comprising the following steps:
Step 1: be that the essential oil that 30-40% extracts for the first time loads reactor as raw material using terpineol-4 content from narrow leaved tea tree, is filled with nitrogen, keeps 0.2kg/CM in reactor
2-1kg/CM
2pressure, through three intensifications, insulation, is specially:
1) 30-45 DEG C is warming up to, insulation 50-60 minute;
2) be warming up to 45-70 DEG C, be incubated 60 minutes;
3) heat to 70-85 DEG C, be incubated 60 minutes;
After three times the process of heating terminates, essential oil is made to be cooled to normal temperature;
Step 2: take out the essential oil processed, adds water and vitamin E mixing; Essential oil: water: the ratio of vitamin E is 20:1000:5, first water and vitamin E is heated to 90 DEG C, after stirring, adds essential oil, after stirring, is filled into bottle with high-speed shearing machine.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105053532A (en) * | 2015-07-31 | 2015-11-18 | 王�琦 | Natural tea tree oil additive for substituting forage antibiotic, and production technology thereof |
| CN105079118A (en) * | 2015-07-31 | 2015-11-25 | 王�琦 | Natural tea tree oil agent used for improving human immunity and production process thereof |
| CN105795134A (en) * | 2016-03-16 | 2016-07-27 | 王璞 | Preparation and use methods of pure natural animal feed additive based on tea tree oil |
| CN106666103A (en) * | 2017-01-11 | 2017-05-17 | 厦门百度科技开发股份有限公司 | Composite feed additive and feed containing additive |
| CN107981048A (en) * | 2017-12-01 | 2018-05-04 | 王璞 | The method of preparation and use of feed addictive based on tea oil |
| CN110679739A (en) * | 2019-07-26 | 2020-01-14 | 河源澳美农业科技有限公司 | Melaleuca alternifolia (Australia tea tree) tree residue powder biological feed |
| CN110771736A (en) * | 2019-11-01 | 2020-02-11 | 广西壮族自治区林业科学研究院 | Biological feed containing baeckea frutescens residue and cajeput residue and preparation method thereof |
| CN110771733A (en) * | 2019-11-01 | 2020-02-11 | 广西壮族自治区林业科学研究院 | Melaleuca leucadendra residue biological feed and preparation method thereof |
| CN110771732A (en) * | 2019-11-01 | 2020-02-11 | 广西壮族自治区林业科学研究院 | Melaleuca leucadendra residue biological feed additive and preparation method thereof |
| CN114668147A (en) * | 2022-03-25 | 2022-06-28 | 华南农业大学 | Melaleuca alternifolia compound essential oil microemulsion and preparation method thereof |
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| WO2013044294A1 (en) * | 2011-09-29 | 2013-04-04 | P.Guinane Pty Ltd | Animal feed composition |
| CN103340928B (en) * | 2013-06-06 | 2015-08-26 | 广西壮族自治区中医药研究院 | A kind of essential oil composition for antibacterial desinsection and preparation method thereof |
| CN103734550B (en) * | 2014-01-29 | 2015-09-16 | 北京劲能生物科技股份公司 | A kind of nursery pig concentrated feed |
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