CN105795134A - Preparation and use methods of pure natural animal feed additive based on tea tree oil - Google Patents
Preparation and use methods of pure natural animal feed additive based on tea tree oil Download PDFInfo
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- CN105795134A CN105795134A CN201610151731.5A CN201610151731A CN105795134A CN 105795134 A CN105795134 A CN 105795134A CN 201610151731 A CN201610151731 A CN 201610151731A CN 105795134 A CN105795134 A CN 105795134A
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Abstract
The present invention discloses a preparation method of a pure natural animal feed additive based on tea tree oil. The feed additive is prepared by the following steps: essential oil containing 30-40% of terpineol-4 is subjected to three times of heating and heat preservation and then the heat preserved essential oil is lowered to a room temperature; attapulgite powder or zeolite powder is added into the essential oil to be mixed and the mixture is stirred to prepare a solid feed additive; and water is added and the mixture is stirred to prepare a drinking water additive. The additive is used as the solid feed additive in different proportions for pigs or chickens, cattle, sheep, ducks, geese, or fish and shrimps, etc., or added into an animal drinking water. By using the feed additives to feed animals, the feed additives can improve the immune system and the growth rate of animals.
Description
Technical field
The present invention relates to pure natural animal feed based on tea tree oil and drinking water additive preparation method, belong to animal feed and prepare skill
Art field.
Background technology
Australia tea tree oil is a kind of trade name, and its formal name used at school is Melaleuca Alternifolia tree oil.Melaleuca Alternifolia tree is to be grown on the big profit of Australia
A kind of bushes of sub-southeastern coast.Australia tea tree oil is had thousand of years history by aborigines for wound disinfection.Australia's tea
Tree oil successfully listed European Pharmacopoeia in 2000, as food flavor additive obtained China Bureau of Drugs Supervision approval and U.S. FDA batch
Accurate.
Find that Australia tea tree oil can effectively suppress much generally to deposit Causative virus through recent studies, for treatment numerous disease and wound
There is very large effect.As bone is ached, burn, flu, bird flu etc..Due to the excellent specific property of Australia tea tree, in a lot of countries
Introduce a fine variety, also have plantation in areas such as the Guangdong of China, Yunnan.
Along with the reach of science, free radical is considered as to cause mankind aging, diseases induced, DNA mutation to cause the unit of tumor
Fierce.Some antioxidants removing free radicals are in succession found and have been applied in our daily life, such as bathypelagic fish oil, Fructus Lycopersici esculenti
Red pigment, shrimp profound sea plain, white krill oil etc..In scientist studies the various applicable Natural antioxidant, find the big profit of Australia
The sub-terpinol-4 (terpineol-4) in tea tree oil has extremely strong antioxidant, through the effort of recent two decades, Australia scientist
Successfully from Australia tea tree, gather and process edible terpinol-4 quintessence oil at first.Detect through U.S. BROWNSWICKLAB, Australia
It is 4 times of white profound sea krill oil that tea tree ethereal oil removes the ability of free radical, is 30 times of shrimp element, 25 times of lycopene,
200 times of bathypelagic fish oil.Australia's tea tree ethereal oil not only has extremely strong antioxidation, has concurrently simultaneously and kills obstinate virus
Function, through Zhejiang Center For Disease Control and Prevention live body Embryo Gallus domesticus test, it has therefore proved that can kill the H1N1 in Embryo Gallus domesticus, H5N1,
The all bird flu viruss of H3N2, H7H9.And similar experiment is the most underway in many places, the world.
In sum, Australia's tea tree oil (Melaleuca Alternifolia tree oil) is refined through giving secondary on the basis of quintessence oil, changes
The molecular structure of original quintessence oil, is allowed to some indexs and is changed.For terpinol-4, this is an important finger of oxidant
Mark, index is the highest, and oxidation resistance is the strongest, improves immunity ability the strongest.From plant produced Australian tea tree oil out
(Melaleuca Alternifolia tree oil) quintessence oil, terpinol-4 numerical value content of manufactured goods is only 30-40%.
The chicken of current China, pig etc. birds, meat, in trophophase, need regularly to give antibiotic etc. medicine disease-resistant, this
Bring health hazard fundamentally to the edible of people.People always search for utilizing natural food as feed additive, join
In animal feed, thus improve the immunity of animal, pre-avian influenza-prevention, animal flu and other diseases.
A kind of method only having animal drinking water additive utilizing Melaleuca Alternifolia tree oil to make at present, Patent No.
" 2014104425119 ", the patent of invention of entitled " a kind of Melaleuca Alternifolia tree oil feed addictive preparation method ", this patent
Terpinol-4 content is that the quintessence oil that 30-40% extracts for the first time loads reactor as raw material by method, is filled with nitrogen, through heating up, protecting
Temperature, then in quintessence oil, addition water and vitamin E are mixed with and obtain, and join in the drinking-water of animal.The method is raw because adding dimension
Element E, is also not reaching to the animal food feed additive of pure natural referred to as completely, and is unfavorable for reducing production cost.
Summary of the invention
For reducing the production cost of feed additive, animal food feed additive and the drinking-water feedstuff of preparing complete pure natural add
Agent, the invention provides two kinds based on Australia tea tree oil (Melaleuca Alternifolia tree oil) as feedstuff and the preparation side of drinking water additive
Method, technical scheme is as follows:
With regard to existing Australia tea tree oil (Melaleuca Alternifolia tree oil) quintessence oil, terpinol-4 numerical value content of its manufactured goods is 30-
40%, secondary refines on this basis, and on the premise of without any chemical assistant, terpinol-4 numerical value content of manufactured goods is
40-60%.Quintessence oil after secondary refinement is as the finished product quintessence oil of animal feed additive or feedstuff additive, and concrete scheme is such as
Under:
Step 1: the quintessence oil that terpinol-4 content is 30-40% is loaded reactor, is filled with nitrogen, in keeping reactor
0.2kg/CM3 1kg/CM3 pressure, through three intensifications, insulation, particularly as follows:
1) it is warming up to 30-45 DEG C, is incubated 50-60 minute；
2) it is warming up to 45-70 DEG C and is incubated 60 minutes；
3) it is heated up to 70-75 DEG C, is incubated 60 minutes；
After three times the process of heating terminates, make quintessence oil be cooled to room temperature, i.e. obtain finished product quintessence oil；
Step 2: take out the finished product quintessence oil processed, adds attapulgite or zeolite powder mixing；Finished product quintessence oil: attapulgite or boiling
The ratio of stone powder is that 1:100～1000, attapulgite or zeolite powder needed 80 mesh or more than 80 mesh sieves, after stirring, obtains
Solid feed additive, loads container, seals less than 35 degree Celsius and preserves.This solid feed additive as piglet, growing and fattening pigs or
The additive of other animals, can be used for adding to the feedstuff including other poultrys, fowl and aquatic products, by solid feed additive with
Feedstuff mixes, and stirs, and solid feed additive with feedstuff ratio is: 1.5:1000.
Step 3: directly mixed with water and emulsifying agent by finished product quintessence oil, ratio is: finished product quintessence oil and water=5:1000, emulsifying agent is 3
Gram.Obtain liquid feed additive after stirring, load container and seal preservation.Liquid feed additive is added animal drinking water
In, ratio is liquid feed additive: water=1:250～1000.
Beneficial effect
From plant produced Australian tea tree oil (Melaleuca Alternifolia tree oil) quintessence oil out, terpinol-4 numerical value content of manufactured goods
It is 30-40%.Present invention secondary on this basis refines, on the premise of without any chemical assistant, and the terpinol-4 of manufactured goods
Numerical value content is 40-60%, it is determined that the oxidation resistance of this novel tea tree oil is greatly higher than astaxanthin etc. health product.This
The feed additive that invention is made, makes an addition in animal feed, can be allowed to improve immunity.The present invention is prepared feed additive
Join in chicken, pig, geese and ducks, cattle, sheep etc. meat, birds, Aquatic product category feed for nursing, owing to this product is without swashing
Element, relies on the extremely strong oxidation resistance of self, can not only improve immunity, and the speed of growth is accelerated after animal edible, body weight
Increase.The present invention adds with the quintessence oil of pure natural and attapulgite or zeolite powder, the animal food feedstuff having reached complete pure natural, nothing
Toxic and side effects, and be beneficial to reduce production cost.
Accompanying drawing explanation
Fig. 1 is daily ingestion amount and the body weight comparison diagram of the additive feeding live pig experiment utilizing this method to prepare.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described, and accompanying drawings is to using this additive feedstuff at feeding
Effect after animal and the Contrast on effect not using this additive feedstuff.
A kind of preparation method of pure natural animal feed additive, step 1, the quintessence oil that terpinol-4 content is 30-40% is loaded anti-
Answering still, open nitrogen cylinder, this nitrogen role is to the tea tree oil in reactor when chemical reaction, plays Stabilization.Then
Pressurization, in reactor during 0.2/CM3-1kg/CM3 pressure, is warming up to 30-40 DEG C, is incubated 50-60 minute；Allow pressure
With temperature action in Melaleuca Alternifolia tree oil, it is allowed to chemical reaction.Open oil circulating pump simultaneously, make oil continuous in reactor
Circulation, it is achieved the abundant reaction of tea tree oil.It is warming up to 40-70 DEG C again and is incubated 60 minutes；Pressure keeps 0.1/CM3-1kg/CM3
Pressure, is then heated up to 70-75 DEG C, is incubated 60 minutes；Remain in that 0.1/CM3-1kg/CM3 pressure, finally exist with cooling water
Pancake coil is cooled to room temperature.Stop the circulation of oil.Melaleuca Alternifolia tree oil is make use of wherein to have kind more than 120 to divide in this process
Son containing volatility, has been driven away impurity and unwanted composition, has been retained and has improved the composition of needs, it is possible to our needs of output
Containing high anti-oxidation ability, the product oil of immunity can be improved.Quintessence oil manufactured goods after being refined by the secondary of above-mentioned steps gained
Terpinol-4 numerical value content is 40-60%.This test data can be with 9790 type gas chromatograph detections.
Step 2, takes the quintessence oil that 20ml processes, and adds 1000 grams of attapulgites, or zeolite powder (ratio is quintessence oil: attapulgite
Powder or zeolite powder=1:100～1000), input three-dimensional mixer, uniform stirring 15 minutes, pack according to required weight with aluminium foil bag
(note: attapulgite must be 80 mesh or the above size of 80 mesh uniform), tinning seal, In Shade preservation (environment temperature
Degree should be less than 35 degree Celsius).
Step 3, takes the quintessence oil that 20ml processes, and adds 1000 grams of water and 3 grams of emulsifying agents, mixes with high-speed shearing machine or homogenizer
Homogenizing 30 minutes, contains with bottle type container.Seal In Shade preservation (ambient temperature should be less than 35 degree Celsius).
There is the characteristic improving immunity widely owing to Melaleuca Alternifolia tree is oily, by that analogy, according to animal food habit and nursing
Method, the additive of this invention gained, according to body weight, the feature of food-intake, after certain ratio adjusts, cattle can be given,
Sheep, duck, goose, pigeon, rabbit etc. domestic animal, birds and Aquatic product category feeding, equally can obtain good health effect.
Meanwhile, this invention is possible not only to by the form of powder, the form of water preparation, it is also possible to be fabricated to capsule and spherical form to dynamic
Thing eats.
Accompanying drawing 1 is daily ingestion amount and the body weight comparison diagram of the solid additive feeding live pig experiment utilizing this method to prepare.Abscissa is
Feeding the date, WOM vertical coordinate is day feeding amount.What solid line represented is the not edible additive adding this method for " matched group "
The pig growth situation of feedstuff, the additive feedstuff pig growth situation for " experimental group " edible addition this method that dotted line represents,
Two groups of live pigs are the live pig son on pig farm, Shang Tang town, Shihhung, Kiangsu Province county, and totally 26, two groups of live pigs are respectively 13, and the time is 2015
The breeding observing record on June to October 3.
Initial (June 28) average weight of matched group is 23 kilograms, TBW 299 kilograms；Experimental group initial (June 28
Day) average weight is 25.61 kilograms, TBW 333 kilograms.After three months (October 3), matched group TBW is 1353
Kilogram, put on weight 1054 kilograms 8 jin；Experimental group TBW is 1514 kilograms, puts on weight 1181 kilograms.
Experimental group live pig increased weight 10.9% than matched group live pig, feedstuff-meat ratio declines 0.023%.This test proves, utilizes we
The additive of method adds feeding in feedstuff for live pigs, can reduce feeding cost, promotes live pig health fast-growth.
Table 1 is the water preparation feedstuff utilizing this method to prepare and prepared by patented method adds vitamin E additive and common feeding is raw
The daily ingestion amount of pig experiment and body weight contrast.Table 1 is it can be seen that with three groups of live pig Experimental comparison, " experimental group " adds for adding
Agent is to quoting the 500 first-born pigs that water has been fed, and starting weight is 12338 kilograms, average 24.68 kilograms.
" VE experimental group ", for using " 2014104425119 " patented method to quoting the 500 first-born pigs that water is fed, plays starting weight 12340
Kilogram, average every body weight 24.676 kilograms.
" matched group ", for being not added with 495 first-born pigs of any additive extremely routine feeding of drinking-water, starting weight is 11645.5 public affairs
Jin, average average weight 23.53 kilograms.
After three groups are fed 90 days, 496 body weight of experimental group are 48382.5 kilograms average 97.54 kilograms；VE experimental group 495
Nose heave 48351 kilograms, average 97.68 kilograms.Matched group 486 is nose heave 41601.55 kilograms, average 85.60 kilograms.
Experimental group live pig and the live pig of VE group all increased weight more than 12% than matched group live pig, additive the most in the process of the present invention
The live pig fed and Patent No. " 2014104425119 ", entitled " a kind of Melaleuca Alternifolia tree oil feed additive preparation side
Method " add the quintessence oil of VE and feed and reach same effect, equally reduce feeding cost, promote the healthy fast-growth of live pig.
Table 1
Claims (2)
1. the preparation method of pure natural animal feed additive based on tea tree oil, is first the initial essence of 30-40% by terpinol-4 content
Oil loads reactor, is filled with nitrogen, keeps 0.1kg/M3 1kg/M3 pressure in reactor, through three intensifications, insulation, specifically
For:
1) it is warming up to 30-40 DEG C, is incubated 50-60 minute；
2) it is warming up to 40-70 DEG C and is incubated 60 minutes；
3) it is heated up to 70-75 DEG C, is incubated 60 minutes；
After three times the process of heating terminates, make quintessence oil be cooled to room temperature, be finished product quintessence oil；
It is characterized in that, following procedure of processing:
4) taking out the finished product quintessence oil processed, add attapulgite or zeolite powder, ratio is finished product quintessence oil: attapulgite or zeolite powder
=1:100～1000, obtains solid feed additive after stirring, load container and seal preservation；
5) directly being mixed with water and emulsifying agent by finished product quintessence oil, ratio is: finished product quintessence oil: water: emulsifying agent=20:1000:3, stirring
Obtain liquid feed additive after Jun Yun, load container and seal preservation.
2. the using method of pure natural animal feed additive as claimed in claim 1, it is characterised in that 1) solid feed is added
Agent mixes with solid feed, stirs, and ratio is: solid feed additive: solid feed=1.5:1000；2) liquid is raised
Feed additives adds in animal drinking water, and ratio is liquid feed additive: water=1:250～1000.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106376746A (en) * | 2016-08-31 | 2017-02-08 | 无锡正大生物股份有限公司 | Non-resistant piglet health premix and production method thereof |
| CN106666103A (en) * | 2017-01-11 | 2017-05-17 | 厦门百度科技开发股份有限公司 | Composite feed additive and feed containing additive |
| CN110679739A (en) * | 2019-07-26 | 2020-01-14 | 河源澳美农业科技有限公司 | Melaleuca alternifolia (Australia tea tree) tree residue powder biological feed |
| CN110771736A (en) * | 2019-11-01 | 2020-02-11 | 广西壮族自治区林业科学研究院 | Biological feed containing baeckea frutescens residue and cajeput residue and preparation method thereof |
| CN112617043A (en) * | 2020-06-09 | 2021-04-09 | 南京泛成生物科技有限公司 | Natural animal feed additive and preparation method thereof |
| WO2021160135A1 (en) * | 2020-02-10 | 2021-08-19 | 中国科学院兰州化学物理研究所 | Method for preparing natural antibacterial agent by using attapulgite pore channels to immobilize plant essential oil |
| WO2021203833A1 (en) * | 2020-04-10 | 2021-10-14 | 中国科学院兰州化学物理研究所 | Method for preparation of attapulgite-based ph-responsive antibacterial material |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106376746A (en) * | 2016-08-31 | 2017-02-08 | 无锡正大生物股份有限公司 | Non-resistant piglet health premix and production method thereof |
| CN106666103A (en) * | 2017-01-11 | 2017-05-17 | 厦门百度科技开发股份有限公司 | Composite feed additive and feed containing additive |
| CN110679739A (en) * | 2019-07-26 | 2020-01-14 | 河源澳美农业科技有限公司 | Melaleuca alternifolia (Australia tea tree) tree residue powder biological feed |
| CN110771736A (en) * | 2019-11-01 | 2020-02-11 | 广西壮族自治区林业科学研究院 | Biological feed containing baeckea frutescens residue and cajeput residue and preparation method thereof |
| WO2021160135A1 (en) * | 2020-02-10 | 2021-08-19 | 中国科学院兰州化学物理研究所 | Method for preparing natural antibacterial agent by using attapulgite pore channels to immobilize plant essential oil |
| WO2021203833A1 (en) * | 2020-04-10 | 2021-10-14 | 中国科学院兰州化学物理研究所 | Method for preparation of attapulgite-based ph-responsive antibacterial material |
| US11700849B2 (en) | 2020-04-10 | 2023-07-18 | Lanzhou Institute Of Chemical Physics, Chinese Academy Of Sciences | Method for preparation of attapulgite-based pH-responsive antibacterial material |
| CN112617043A (en) * | 2020-06-09 | 2021-04-09 | 南京泛成生物科技有限公司 | Natural animal feed additive and preparation method thereof |
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