CN104136371B - 制备沉淀二氧化硅的新颖的方法 - Google Patents

制备沉淀二氧化硅的新颖的方法 Download PDF

Info

Publication number
CN104136371B
CN104136371B CN201280070513.9A CN201280070513A CN104136371B CN 104136371 B CN104136371 B CN 104136371B CN 201280070513 A CN201280070513 A CN 201280070513A CN 104136371 B CN104136371 B CN 104136371B
Authority
CN
China
Prior art keywords
acid
concentration
mass
reaction medium
silicate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201280070513.9A
Other languages
English (en)
Chinese (zh)
Other versions
CN104136371A (zh
Inventor
M.克卢安
S.内沃
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Operations SAS
Original Assignee
Rhodia Operations SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from FR1104089A external-priority patent/FR2984871B1/fr
Priority claimed from FR1200217A external-priority patent/FR2985994B1/fr
Application filed by Rhodia Operations SAS filed Critical Rhodia Operations SAS
Publication of CN104136371A publication Critical patent/CN104136371A/zh
Application granted granted Critical
Publication of CN104136371B publication Critical patent/CN104136371B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/126—Preparation of silica of undetermined type
    • C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Paper (AREA)
CN201280070513.9A 2011-12-23 2012-12-19 制备沉淀二氧化硅的新颖的方法 Expired - Fee Related CN104136371B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
FR11/04089 2011-12-23
FR1104089A FR2984871B1 (fr) 2011-12-23 2011-12-23 Nouveau procede de preparation de silices
FR1200217A FR2985994B1 (fr) 2012-01-25 2012-01-25 Nouveaux procede de preparation de silices precipitees
FR12/00217 2012-01-25
PCT/EP2012/076206 WO2013092745A1 (fr) 2011-12-23 2012-12-19 Procede de preparation de silices precipitees

Publications (2)

Publication Number Publication Date
CN104136371A CN104136371A (zh) 2014-11-05
CN104136371B true CN104136371B (zh) 2017-03-15

Family

ID=47501255

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280070513.9A Expired - Fee Related CN104136371B (zh) 2011-12-23 2012-12-19 制备沉淀二氧化硅的新颖的方法

Country Status (14)

Country Link
US (1) US9550682B2 (ru)
EP (1) EP2794479B1 (ru)
JP (1) JP5868520B2 (ru)
KR (1) KR20140111297A (ru)
CN (1) CN104136371B (ru)
AU (1) AU2012357112A1 (ru)
BR (1) BR112014015235B1 (ru)
CA (1) CA2859570C (ru)
IN (1) IN2014CN04607A (ru)
MX (1) MX356674B (ru)
MY (1) MY180098A (ru)
RU (1) RU2607741C2 (ru)
TW (1) TWI498284B (ru)
WO (1) WO2013092745A1 (ru)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2984870B1 (fr) 2011-12-23 2014-03-21 Rhodia Operations Nouveau procede de preparation de silices precipitees.
FR2985991B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985992B1 (fr) 2012-01-25 2015-03-06 Rhodia Operations Nouveau procede de preparation de silices precitees
FR2985993B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985990B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres
FR3017609B1 (fr) 2014-02-14 2016-03-18 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
FR3017610B1 (fr) * 2014-02-14 2016-03-18 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
FR3018070B1 (fr) * 2014-02-28 2017-09-15 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
KR102603478B1 (ko) * 2017-05-05 2023-11-20 로디아 오퍼레이션스 침강 실리카 및 그의 제조 방법
EP3619164A1 (en) * 2017-05-05 2020-03-11 Rhodia Operations Precipitated silica and process for its manufacture
JP7490645B2 (ja) * 2018-11-08 2024-05-27 ローディア オペレーションズ 沈降シリカ及びその製造プロセス
KR20210088562A (ko) * 2018-11-08 2021-07-14 로디아 오퍼레이션스 침전 실리카 및 이의 제조 공정
CN109607555B (zh) * 2019-01-02 2019-08-09 广州市飞雪材料科技有限公司 一种高磨擦高透明牙膏用二氧化硅及其制备方法
CN109480097B (zh) * 2019-01-03 2022-02-01 山东联科科技股份有限公司 一种酸化剂载体用二氧化硅微球的制备方法
CA3235727A1 (en) 2021-10-26 2023-05-04 Evonik Operations Gmbh Precipitated silica, process for production thereof and use thereof
WO2023118282A1 (en) * 2021-12-23 2023-06-29 Rhodia Operations Tire elastomeric compositions comprising a precipitated silica
CN115571886B (zh) * 2022-10-14 2023-12-05 福建正盛无机材料股份有限公司 一种低吸油、低比表面积二氧化硅的制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1069244A (zh) * 1991-06-26 1993-02-24 罗纳·布朗克化学公司 沉淀二氧化硅新制备方法，新沉淀二氧化硅及其在弹性体增强过程中的应用

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1506330A (fr) 1966-05-24 1967-12-22 Fr Des Silicates Speciaux Sifr Perfectionnements apportés aux procédés de fabrication de silice et produits obtenus par ces procédés
DE3114493A1 (de) * 1981-04-10 1982-10-28 Degussa Ag, 6000 Frankfurt "faellungskieselsaeuren und verfahren zu ihrer herstellung"
DE3639845A1 (de) * 1986-11-21 1988-06-01 Degussa Faellungskieselsaeuren, verfahren zu ihrer herstellung und verwendung
DE19526476A1 (de) 1995-07-20 1997-01-23 Degussa Fällungskieselsäure
RU2179153C1 (ru) * 2000-06-07 2002-02-10 Закрытое акционерное общество "Хорс" Способ получения диоксида кремния
AU2002211736A1 (en) * 2000-10-13 2002-04-22 University Of Cincinnati Methods for synthesizing precipitated silica and use thereof
DE10112441A1 (de) * 2001-03-15 2002-09-19 Degussa Kieselsäure durch Fällung mit konstanter Alkalizahl und deren Verwendung
RU2270167C2 (ru) * 2001-08-13 2006-02-20 Родиа Шими Способ получения диоксидов кремния, диоксиды кремния с особым гранулометрическим распределением и/или распределением пор и их применение, в частности, для упрочнения полимеров
WO2010022544A1 (en) * 2008-09-01 2010-03-04 Evonik Degussa Gmbh Process for preparing precipitated silicas, precipitated silicas and their use
FR2949454B1 (fr) * 2009-09-03 2011-09-16 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2984870B1 (fr) 2011-12-23 2014-03-21 Rhodia Operations Nouveau procede de preparation de silices precipitees.
FR2985990B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres
FR2985992B1 (fr) 2012-01-25 2015-03-06 Rhodia Operations Nouveau procede de preparation de silices precitees
FR2985991B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985993B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1069244A (zh) * 1991-06-26 1993-02-24 罗纳·布朗克化学公司 沉淀二氧化硅新制备方法，新沉淀二氧化硅及其在弹性体增强过程中的应用

Also Published As

Publication number Publication date
BR112014015235A2 (pt) 2017-06-13
MY180098A (en) 2020-11-22
WO2013092745A1 (fr) 2013-06-27
CA2859570A1 (fr) 2013-06-27
AU2012357112A1 (en) 2014-07-10
MX2014007591A (es) 2015-03-19
TW201339095A (zh) 2013-10-01
CA2859570C (fr) 2016-10-18
CN104136371A (zh) 2014-11-05
TWI498284B (zh) 2015-09-01
BR112014015235A8 (pt) 2017-06-13
IN2014CN04607A (ru) 2015-09-18
BR112014015235B1 (pt) 2020-12-08
RU2014130284A (ru) 2016-02-10
KR20140111297A (ko) 2014-09-18
US20150266742A1 (en) 2015-09-24
US9550682B2 (en) 2017-01-24
EP2794479B1 (fr) 2020-04-08
EP2794479A1 (fr) 2014-10-29
RU2607741C2 (ru) 2017-01-10
JP5868520B2 (ja) 2016-02-24
MX356674B (es) 2018-06-08
JP2015506327A (ja) 2015-03-02

Similar Documents

Publication Publication Date Title
CN104136371B (zh) 制备沉淀二氧化硅的新颖的方法
JP5859144B2 (ja) 沈澱シリカ製造方法
KR950015028B1 (ko) 비이드 형태의 실리카, 이의 제조방법 및 엘라스토머 보강용 용도
CN104066681B (zh) 制备具有特定形态、微粒大小及孔隙度的沉淀二氧化硅的方法
MX2013000668A (es) Nuevo proceso de produccion de silice precipitado.
CN108137331A (zh) 用于制备硅酸盐的新颖方法及其用于制备沉淀二氧化硅的用途
US9695054B2 (en) Process for preparing precipitated silica
US10011494B2 (en) Process for preparing precipitated silica
JP3993872B2 (ja) 沈降シリカ及び燐酸塩から生成した組成物、並びに栄養特性をもつ液体支持材及び栄養特性をもつ固結防止剤としてのその使用
US10865114B2 (en) Process for preparing precipitated silica comprising a high compaction step
KR20200030618A (ko) 고온 스폴링 단계를 포함하는 침강 실리카의 제조 방법
US20150110700A1 (en) Process for preparing precipitated silica using a mixer or extruder
JP5868527B2 (ja) 沈澱シリカ製造方法
JP2015504843A (ja) 沈澱シリカの製造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170315

Termination date: 20211219