CN103992745A - Liquid shoe polish prepared by ginkgo leaf ketone extracted paste residual wastes and preparation method thereof - Google Patents
Liquid shoe polish prepared by ginkgo leaf ketone extracted paste residual wastes and preparation method thereof Download PDFInfo
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- CN103992745A CN103992745A CN201410207421.1A CN201410207421A CN103992745A CN 103992745 A CN103992745 A CN 103992745A CN 201410207421 A CN201410207421 A CN 201410207421A CN 103992745 A CN103992745 A CN 103992745A
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Abstract
The invention relates to a liquid shoe polish prepared by ginkgo leaf ketone extracted paste residual wastes and a preparation method thereof. The shoe polish comprises the following raw materials by mass percent: 60-80% of filtered and suction filtered ginkgo leaf ketone extracted paste residual wastes, 0.5-3% of solid paraffin, 0.5-3% of beewax, 0.5-15% of liquid paraffin, 1-15% of turpentine, 0.5-1% of surfactant, 0.5-1% of emulgator, 0.5-1% of silicon oil, 0.05-1% of natural essence, and 0.05-1% of glycerinum. The invention also relates to the preparation steps of the liquid shoe polish. The shoe polish has the characteristics and advantages of using the natural plant source ginkgo leaf residual wastes as the black raw material, having no dyes, no toxicity, and no odor, being bright and clean, good in polishing performance, and environment-friendly, having a simple preparation process and low cost, efficiently using the ginkgo leaf residual wastes, turning the waste into wealth, firmly coloring, being bright in color and luster, softening and protecting the leather, repairing shallow marks, being mould-proof and anti-microbial, being not prone to have dust, and being light-resistant, heat-resistant and good in stability.
Description
Technical field
The invention provides a kind of bilobanone and extract liquid shoe polish and preparation method prepared by paste tankage, belong to daily chemicals technical field, belong to concrete shoe polish research and development and the concrete technical field of producing.
Background technology
Shoe polish is protective material and the lustering agent of embrocating at leather shoes and leather surface, has the effect of waterproof, guard, enhancing leather surface gloss, cleaning, attractive in appearance and additive color complementary color, and daily life consumption is very big.Shoe polish is pressed textural classification, has solvent-borne type plaster body, emulsion type ointment body and liquid-type, and first two is traditional product, and liquid shoe polish is current domestic popular product innovation.Liquid shoe polish has not to be wiped from the feature such as bright, easy to carry, to save time, and the feature such as embrocates easily, liked by human consumer.About the main body of liquid shoe polish, there are reports and launch, and its main raw material is the mixture of wax emulsion and wax emulsion and synthetic resins etc.And it is also less or have no report on market, to take liquid shoe polish that plant-sourced tinting material is body material.
At present, the black liquor shoe polish on market, pigment major part used is chemical synthetic dye, or the extract of chemical industry waste material, mostly easily environment and human body are worked the mischief, therefore, under this background, develop a kind of plant-sourced dyestuff tool and be of great significance.Among the people to be collected to extract some ketones in a large number medicinal to do/medical in China for Ginkgo Leaf, its tankage after treatment, just can be used as a kind of plant-sourced dyestuff and adding shoe polish main component, the present invention proposes a kind of bilobanone and extracts liquid shoe polish and preparation method prepared by paste tankage, can solve shoe polish black raw material sources problem, realize innoxious and " turning waste into wealth " that shoe polish is produced.The paste tankage that this Ginkgo Leaf industrialization is extracted, black, oily, paste, pure natural, do not need to add other pigments or pigment, chemical industry waste material and tankage with respect to shoe polish main component general used, environmental protection degree is much higher, the main component of preparing as shoe polish, its cost is low, production technique is simple, working condition and equipment with meet and convenient operation, the production process cycle is short, efficiency is high, reduce a large amount of middle-chain and the complicacy of technique, there is very important DEVELOPMENT PROSPECT and wide market.
Summary of the invention
The present invention relates to a kind of bilobanone and extract liquid shoe polish and preparation method prepared by paste tankage.
Its composition comprises: Ginkgo Leaf ketone extracts paste tankage, solid paraffin, beeswax, whiteruss, turps and additive.
Described Ginkgo Leaf ketone extracts paste tankage and specifically refers to, the Ginkgo Leaf ketone after processing with suction filtration after filtration extracts paste tankage, and additive is specially five kinds of tensio-active agent, emulsifying agent and silicone oil, natural essence and glycerine.
Described shoe polish composition is specially: the Ginkgo Leaf ketone after processing with suction filtration after filtration extracts paste tankage 60-80%, solid paraffin 0.5-3%, beeswax 0.5-3%, whiteruss 0.5-15%, turps 1-15%, tensio-active agent, emulsifying agent and three kinds of each 0.5-1% of silicone oil, natural essence 0.05-1%, glycerine 0.05-1%, above mark is massfraction.
Ginkgo Leaf ketone after processing with suction filtration after filtration described in it extracts paste tankage, and what also added trace is weakly alkaline NaOH solution or dilute hydrochloric acid for regulating these tankage; Tensio-active agent water-soluble lanolin specifically wherein, emulsifying agent is the monomer of certain wax material specifically, or the mixture of wax material, or commercially available finished product emulsifying agent; Emulsifying agent is sorbester p17 specifically, and aforementioned weakly alkaline specifically refers to that pH value is between 7-11.
A preparation method for liquid shoe polish, step is as follows:
1. Ginkgo Leaf ketone extracts paste tankage raw material treatment step: with vacuum pump suction filtration, strainer, filter and the filtration of 100-800 eye mesh screen, remove solid granulates shape impurity, then according to concrete sample potential of hydrogen, by appropriate dilute hydrochloric acid or NaOH solution furnishing pH value, be the filtrate between 6-8, to prevent melanin deposition gathering.
2. the filtrate in is 1. heated concentratedly, steam in process and stir gently, mix, all the time temperature is controlled under the temperature condition that 100 C are slightly high, obtain mixing liquid.
3. in 2., in resulting black liquor, add successively solid paraffin 0.5-3% and beeswax 0.5-3%, stir gently and be heated to and melt, obtain liquid and be slightly gluey.
4. in being in colloidal liquid of 3. obtaining, add successively whiteruss 0.5-15% and 1-15% turps, stirring is mixed obtains black liquor.
5. in 4., in gained liquid, add successively water-soluble lanolin or stearic acid 0.5-1%, sorbester p17 or tween 0.5-1% and silicone oil 0.5-1%, thick black mixing liquid.
6. in the thick black mixing liquid 5. obtaining, add natural essence 0.05-1% and glycerine 0.05-1%, stirring is mixed, and can obtain finished product black liquor shoe polish.
Step 6. natural essence used is a kind of essential oil or several mixture of choosing from frequently seen plants natural essence oil or Common Chinese Herbs fragrance matter essential oil.
Being used for regulating shoe polish is whole weakly alkaline appropriate sodium hydroxide NaOH or dilute hydrochloric acid HCL, regulates pH=6-8, prevents melanin deposition gathering.
Ginkgo Leaf ketone of the present invention extracts paste tankage, refer to and take Ginkgo Leaf remaining paste tankage after raw material extracts letones, its character paste, is the oily liquids of black thickness, it has passed through filtration or suction filtration step, for there is no the homogeneous lotion of solid impurity.
Liquid shoe polish feature and advantage involved in the present invention are: 1. natural plant Ginkgo Leaf paste tankage are black raw material; 2. do not add dyestuff; 3. bright and clean beautiful, upper luminosity is good; 4. nontoxic, deodorizing, environmental protection; 4. technique preparation is simple, with low cost; 5. realized the efficient utilization of ginkgo paste tankage, turned waste into wealth; 6. firm coloration, color and luster is beautiful, good endurance; 7. softening protection leather, repairs shallow trace; 8. mildew-resistant is fungi-proofing; 9. fast light, heat-resisting, stability is better.
Experiment shows: after this shoe polish is coated on leather shoes upper, can reach the object of waterproof, expelling parasite, light, deodorizing and protection leather, having improved aesthetic appearance.
Embodiment
Embodiment 1
A kind of bilobanone of concrete preparation extracts liquid shoe polish and preparation method prepared by paste tankage, product preparation process and step are as follows: by Ginkgo Leaf paste tankage raw material, with strainer, filter or the filtration of 300 eye mesh screens, remove particulate contamination, then with appropriate rare HCl or NaOH, adjusting pH value is 6, prevents melanin deposition gathering.
Filtrate is heated concentrated, evaporate to dryness moisture and part volatile matter wherein, guarantees to remove that part is wherein poisonous, palatable substances, until moisture is by evaporate to dryness.Steam in process and stir gently, mix, all the time temperature is controlled under the temperature condition that 100 C are slightly high, obtain the mixing liquid of black thickness light.
By the mixing liquid of resulting black thickness light, add successively solid paraffin 2% and beeswax 2%, stir gently and be heated to and melt, obtain black colloidal liquid.
In black colloidal liquid, add successively whiteruss 5% and 10% turps, low temperature stirs to be mixed and obtains black liquor.
In gained black liquor, add successively lanolin 1%, sorbester p17 1% and silicone oil 1%, for emulsive oily or lipid-soluble substance, can obtain so thick black mixing liquid, this liquid is thick, and aterrimus is glossy shinny.
The glycerine that adds natural Mint Essence 0.05% and 0.05% in mixing liquid, stirring is mixed, and can obtain finished product black liquor shoe polish.
The proportioning of the shoe polish so obtaining is: the Ginkgo Leaf ketone after processing with suction filtration after filtration extracts paste tankage 77.9%, solid paraffin 2%, beeswax 2%, whiteruss 5%, turps 10%, three kinds of lanolin 1%, sorbester p17 1% and silicone oil each 1%, natural Mint Essence 0.05%, glycerine 0.05%, above mark is massfraction.
Embodiment 2
A kind of bilobanone of concrete preparation extracts liquid shoe polish and preparation method prepared by paste tankage, and product preparation process and step are as follows:
By Ginkgo Leaf paste tankage raw material, with strainer, filter or the filtration of 200 eye mesh screens, remove particulate contamination, then with appropriate rare HCl or NaOH, adjusting pH value is 8, prevents melanin deposition gathering.
Filtrate is heated concentrated, evaporate to dryness moisture and part volatile matter wherein, guarantees to remove that part is wherein poisonous, palatable substances, until moisture is by evaporate to dryness.Steam in process and stir gently, mix, all the time temperature is controlled under the temperature condition that 100 C are slightly high, obtain the mixing liquid of black thickness light.
By the mixing liquid of resulting black thickness light, add successively solid paraffin 3% and beeswax 3%, stir gently and be heated to and melt, obtain black colloidal liquid.
In black colloidal liquid, add successively whiteruss 6% and 8% turps, low temperature stirs to be mixed and obtains black liquor.
In gained black liquor, add successively stearic acid 0.5%, tween 0.5% and silicone oil 1%, for emulsive oily or lipid-soluble substance, can obtain so thick black mixing liquid, this liquid is thick, and aterrimus is glossy shinny.
The glycerine that adds natural rose essence 0.1% and 0.1% in mixing liquid, stirring is mixed, and can obtain finished product black liquor shoe polish.
The proportioning of the shoe polish so obtaining is: the Ginkgo Leaf ketone after processing with suction filtration after filtration extracts paste tankage 77.8%, solid paraffin 3%, beeswax 3%, whiteruss 6%, turps 8%, stearic acid 0.5%, tween 0.5% and silicone oil 1%, natural rose essence 0.1%, glycerine 0.1%, above mark is massfraction.
Finally it should be noted that: the above only, in order to technical scheme of the present invention to be described, is not intended to limit; Although the present invention is had been described in detail with reference to aforementioned, those of ordinary skill in the art is to be understood that: it still can be modified to aforementioned recorded technical scheme, or part technical characterictic is wherein equal to replacement; And these modifications or replacement do not make the essence of appropriate technical solution depart from the spirit and scope of technical solution of the present invention.
Claims (7)
1. the liquid shoe polish that prepared by bilobanone paste tankage, its composition comprises:
Ginkgo Leaf ketone extracts paste tankage, solid paraffin, beeswax, whiteruss, turps and additive.
2. the liquid shoe polish that prepared by a kind of bilobanone paste tankage as claimed in claim 1, is characterized in that:
Described Ginkgo Leaf ketone extracts paste tankage and specifically refers to, the Ginkgo Leaf ketone after processing with suction filtration after filtration extracts paste tankage, and additive is specially five kinds of tensio-active agent, emulsifying agent and silicone oil, natural essence and glycerine;
Described shoe polish composition is specially; Ginkgo Leaf ketone after processing with suction filtration after filtration extracts paste tankage 60-80%, solid paraffin 0.5-3%, beeswax 0.5-3%, whiteruss 0.5-15%, turps 1-15%, tensio-active agent, emulsifying agent and three kinds of each 0.5-1% of silicone oil, natural essence 0.05-1%, glycerine 0.05-1%, above mark is massfraction.
3. the liquid shoe polish that prepared by a kind of bilobanone paste tankage as claimed in claim 2, is characterized in that:
Ginkgo Leaf ketone after processing with suction filtration after filtration described in it extracts paste tankage, has passed through the processing that potential of hydrogen regulates, and what it had added trace in acid-alkali accommodation is weakly alkaline NaOH solution or dilute hydrochloric acid for regulating these tankage;
Specifically water-soluble lanolin or stearic acid of tensio-active agent wherein, emulsifying agent is the monomer of certain wax material specifically, or the mixture of wax material, or commercially available finished product emulsifying agent.
4. the liquid shoe polish that prepared by a kind of bilobanone paste tankage as claimed in claim 3, is characterized in that, emulsifying agent is sorbester p17 or tween specifically, and aforementioned weakly alkaline specifically refers to that pH value is between 7-11.
5. a preparation method for the liquid shoe polish that prepared by bilobanone paste tankage, step is as follows:
1. Ginkgo Leaf ketone extracts paste tankage raw material treatment step: with vacuum pump suction filtration, strainer, filter and the filtration of 100-800 eye mesh screen, remove solid granulates shape impurity, then according to concrete sample potential of hydrogen, by appropriate dilute hydrochloric acid or NaOH solution furnishing pH value, be the filtrate between 7-11, to prevent melanin deposition gathering;
2. the filtrate in is 1. heated concentratedly, steam in process and stir gently, mix, all the time temperature is controlled under the temperature condition that 100 C are slightly high, obtain mixing liquid;
3. in 2., in resulting black liquor, add successively solid paraffin 0.5-3% and beeswax 0.5-3%, stir gently and be heated to and melt, obtain liquid and be slightly gluey;
4. in being in colloidal liquid of 3. obtaining, add successively whiteruss 0.5-10% and 1-10% turps, stirring is mixed obtains black liquor;
5. in 4., in gained liquid, add successively water-soluble lanolin or stearic acid 0.5-1%, sorbester p17 or tween 0.5-1% and silicone oil 0.5-1%,, thick black mixing liquid;
6. in the thick black mixing liquid 5. obtaining, add natural essence 0.05-1% and glycerine 0.05-1%, stirring is mixed, and obtains finished product black liquor shoe polish.
6. the preparation method of the liquid shoe polish that as claimed in claim 5 prepared by a kind of bilobanone paste tankage, step 6. natural essence used is a kind of essential oil or several mixture of choosing from frequently seen plants natural essence oil or Common Chinese Herbs fragrance matter essential oil.
7. prepare as the method that in claim 4, shoe polish was used, its step is as follows:
1. Ginkgo Leaf ketone extracts paste tankage raw material treatment step: with vacuum pump suction filtration, strainer, filter and the filtration of 100-800 eye mesh screen, remove solid granulates shape impurity, then according to concrete sample potential of hydrogen, by appropriate dilute hydrochloric acid or NaOH solution furnishing pH value, be the filtrate between 6-8, to prevent melanin deposition gathering;
2. the filtrate in is 1. heated concentratedly, steam in process and stir gently, mix, all the time temperature is controlled under the temperature condition that 100 C are slightly high, obtain mixing liquid;
3. in 2., in resulting black liquor, add successively solid paraffin 0.5-3% and beeswax 0.5-3%, stir gently and be heated to and melt, obtain liquid and be slightly gluey;
4. in being in colloidal liquid of 3. obtaining, add successively whiteruss 0.5-10% and 1-10% turps, stirring is mixed obtains black liquor;
5. in 4., in gained liquid, add successively water-soluble lanolin or stearic acid 0.5-1%, sorbester p17 or tween 0.5-1% and silicone oil 0.5-1%,, thick black mixing liquid;
6. in the thick black mixing liquid 5. obtaining, add natural essence 0.05-1% and glycerine 0.05-1%, stirring is mixed, and obtains finished product black liquor shoe polish.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410207421.1A CN103992745B (en) | 2014-05-16 | 2014-05-16 | A kind ofly extract liquid shoe polish and preparation method prepared by paste tankage by bilobanone |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410207421.1A CN103992745B (en) | 2014-05-16 | 2014-05-16 | A kind ofly extract liquid shoe polish and preparation method prepared by paste tankage by bilobanone |
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| CN103992745A true CN103992745A (en) | 2014-08-20 |
| CN103992745B CN103992745B (en) | 2015-09-09 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105219539A (en) * | 2015-09-17 | 2016-01-06 | 广州佳伲思抗菌材料有限公司 | A kind of antimildew and antibacterial cleansing cream and preparation method thereof and application |
| CN106349951A (en) * | 2016-08-26 | 2017-01-25 | 李冬琼 | Shoe polish preparation method |
| CN106366941A (en) * | 2016-08-26 | 2017-02-01 | 李冬琼 | Processing technology of shoe polish |
| CN106366943A (en) * | 2016-08-26 | 2017-02-01 | 李冬琼 | Preparation method of liquid shoe polish |
| CN106366942A (en) * | 2016-08-26 | 2017-02-01 | 李冬琼 | Preparation method of fiber-containing liquid shoe polish |
| CN111218218A (en) * | 2019-12-02 | 2020-06-02 | 湖南康倍奇生物科技有限公司 | Method for producing shoe polish by using wastewater from gallic acid production |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103275621A (en) * | 2013-05-21 | 2013-09-04 | 苏州富通高新材料科技股份有限公司 | Chinese herbal medicine inset-prevention and antibiotic floor wax and preparation method thereof |
| CN103555208A (en) * | 2013-10-25 | 2014-02-05 | 卢逸凡 | Shoe polish |
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2014
- 2014-05-16 CN CN201410207421.1A patent/CN103992745B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103275621A (en) * | 2013-05-21 | 2013-09-04 | 苏州富通高新材料科技股份有限公司 | Chinese herbal medicine inset-prevention and antibiotic floor wax and preparation method thereof |
| CN103555208A (en) * | 2013-10-25 | 2014-02-05 | 卢逸凡 | Shoe polish |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105219539A (en) * | 2015-09-17 | 2016-01-06 | 广州佳伲思抗菌材料有限公司 | A kind of antimildew and antibacterial cleansing cream and preparation method thereof and application |
| CN106349951A (en) * | 2016-08-26 | 2017-01-25 | 李冬琼 | Shoe polish preparation method |
| CN106366941A (en) * | 2016-08-26 | 2017-02-01 | 李冬琼 | Processing technology of shoe polish |
| CN106366943A (en) * | 2016-08-26 | 2017-02-01 | 李冬琼 | Preparation method of liquid shoe polish |
| CN106366942A (en) * | 2016-08-26 | 2017-02-01 | 李冬琼 | Preparation method of fiber-containing liquid shoe polish |
| CN111218218A (en) * | 2019-12-02 | 2020-06-02 | 湖南康倍奇生物科技有限公司 | Method for producing shoe polish by using wastewater from gallic acid production |
| CN111218218B (en) * | 2019-12-02 | 2022-01-18 | 湖南利农五倍子产业发展有限公司 | Method for producing shoe polish by using wastewater from gallic acid production |
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| CN103992745B (en) | 2015-09-09 |
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