CN105219539A - A kind of antimildew and antibacterial cleansing cream and preparation method thereof and application - Google Patents
A kind of antimildew and antibacterial cleansing cream and preparation method thereof and application Download PDFInfo
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- CN105219539A CN105219539A CN201510595437.9A CN201510595437A CN105219539A CN 105219539 A CN105219539 A CN 105219539A CN 201510595437 A CN201510595437 A CN 201510595437A CN 105219539 A CN105219539 A CN 105219539A
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Abstract
The present invention discloses a kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 1 ~ 4 part; Emulsifying agent 8 ~ 16 parts; Wax material 15 ~ 30 parts; Silicone oil 8 ~ 12 parts; Glycerine 5 ~ 10 parts; 3 ~ 8 parts, lanolin; 1 ~ 6 part, guard albumen; Solvent 20 ~ 60 parts.The present invention also disclosed a kind of preparation method and application of antimildew and antibacterial cleansing cream.Antimildew and antibacterial cleansing cream prepared by the present invention, is creamy white, hardness is suitable, exquisiteness is even, the collocation of good stability, fragrant, composition rationally, is easily prepared and safety non-toxic, anti-mold effect are remarkable.Antimildew and antibacterial cleansing cream of the present invention is Multifunctional anti-fungus antibiotic cleaning cream, there is antimildew and antibacterial, clean decontamination, the several functions such as curing leather, can make that leather softness is flexible, gloss is soft, and the be full of cracks of antagonism leather aging and surface drying can be helped, dispel the mould of leather surface in a mouldy condition, mildew etc., long-actingly prevent going mouldy of leather.
Description
Technical field
The present invention relates to a kind of Leather mildew-proof field, be specifically related to a kind of antimildew and antibacterial cleansing cream and preparation method thereof and application.
Background technology
Leather surface has a kind of special grain layer, has natural graining and gloss, hand feel and drape, is favourably welcome.Some leather material limited source, the preparation section of leather is complicated, and technical requirements is high, then cost is high, needs effectively to protect, nurse, and extends its work-ing life.
Leatherware goods are stained with poly-dust, sweat stain, greasy dirt etc. than being easier under general environment condition, as unclean for a long time, easily mouldy and not easy to clean, and leather needs to obtain required nutritive ingredient simultaneously, just can softness, smooth, otherwise may ftracture, fold.Easily mouldy leatherware is through long-distance transport, and even hot and humid sea transport, allows mouldy increased risk, leatherware mouldy caused cannot shipment, even return goods, the problem such as fine, allow associated merchant worry endlessly, the problem therefore solving leatherware mouldy is very important.So far, a lot of for the method preventing leather mouldy, wherein embrocating mildew-resistant paste on leatherware surface is one of the most effective and maneuverable method.Analogous products on market are of a great variety, the material that most mildew-resistant paste contains all can have some to the toxic effect of human body and also mildew-resistant paste expensive.At present, both at home and abroad to the requirement increasingly stringent of environmental protection, the leather-like mildew-resistant paste of many widespread uses may be limited to use, therefore develop a kind of environmental protection, cost performance high, multi-functional Leather mildew-proof antibiotic cleaning cream is necessary.
Summary of the invention
The object of the invention is, in order to overcome above-mentioned defect, to provide a kind of antimildew and antibacterial cleansing cream and preparation method thereof and application.Technical scheme of the present invention is achieved in that a kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 1 ~ 4 part; Emulsifying agent 8 ~ 16 parts; Wax material 15 ~ 30 parts; Silicone oil 8 ~ 12 parts; Glycerine 5 ~ 10 parts; 3 ~ 8 parts, lanolin; 1 ~ 6 part, guard albumen; Solvent 20 ~ 60 parts.
Further, the raw material of following weight part is comprised: antimildew and antibacterial agent 2 parts; Emulsifying agent 12 ~ 16 parts; Wax material 25 ~ 28 parts; Silicone oil 9 ~ 10 parts; Glycerine 5 ~ 8 parts; 3 ~ 5 parts, lanolin; 1 ~ 2 part, guard albumen; Solvent 30 ~ 45 parts.
Further, the raw material of following weight part is comprised: antimildew and antibacterial agent 2 parts; Emulsifying agent 15 parts; Wax material 25 parts; Silicone oil 10 parts; Glycerine 8 parts; 5 parts, lanolin; 2 parts, guard albumen; Solvent 33 parts.
Preferably, the raw material of following weight part is comprised: antimildew and antibacterial agent 2 parts; Emulsifying agent 16 parts; Wax material 15 parts; Silicone oil 10 parts; Glycerine 10 parts; 5 parts, lanolin; 1 part, guard albumen; Solvent 40 parts.
Further, the spices 0.5 ~ 1 part of weight part is also comprised.
Further, 0.5 ~ 1 part, the sodium hydroxide of weight part is also comprised.
Further, described solvent comprises second alcohol and water, and the ratio of second alcohol and water is 1 ~ 3:2 ~ 5.
Further, antimildew and antibacterial agent is biological mildew inhibitor.
A preparation method for antimildew and antibacterial cleansing cream, specifically comprises the following steps:
1) be first placed in reactor by the wax material of described formula ratio and lanolin, 70 ~ 85 DEG C of water-baths, to melting completely, then add the solvent of formula ratio and mix, finally add the silicone oil of described formula ratio, glycerine and guard albumen and mix;
2) to step 1) add the emulsifying agent of described formula ratio in the solution that obtains, stir 10 ~ 25min at 35 ~ 40 DEG C, then constant temperature leaves standstill 8 ~ 20min;
3) to step 2) add the antimildew and antibacterial agent of described formula ratio in the solution that obtains, stir 20 ~ 30min at 65 ~ 75 DEG C and obtain paste;
4) by step 3) described in paste be cooled to room temperature after, filling.
The application of a kind of antimildew and antibacterial cleansing cream in Leather mildew-proof.
The raw material that the present invention prepares antimildew and antibacterial cleansing cream is all to the harmful ep-type material of human non-toxic.
Beeswax is to wax gland secretory product below worker bee belly; for edible natural is with can biodegradable characteristic; beeswax can be absorbed by leather part and form layer protecting film at leather surface; the pliability of leather can be strengthened and slow down the aging speed of leather; and beeswax and emulsion thereof have antibacterial and preservative activity; the storage life of the paste of preparation can be made to extend, simultaneously can play the effect of synergy disinfecting mouldproof with antimildew and antibacterial agent of the present invention.
Paraffin is a kind of mineral wax, and it obtains from crude distillation gained, has low irritability and good closure, can intercept and extremely evaporate, prevent leather dry and cracked; Synthetic wax tool has good wearability and the characteristic such as slipping, high-melting-point.
Carnauba wax is a kind of nontoxic pure natural wax, has high gloss, very easily emulsification, has good Oil keeping, uses carnauba wax can improve the glossiness of leather when using antimildew and antibacterial cleansing cream of the present invention.
Silicone oil is the general name of the polydimethylsiloxane of a series of differing molecular quality, and it is colourless transparent oil liquid, odorless, tasteless, stable chemical nature, and hydrophobicity is strong, has fabulous lubricant effect.
Antimildew and antibacterial cleansing cream second alcohol and water of the present invention is as solvent; due to the volatility of ethanol; during use, paste can form layer protecting film at leather surface fast, can prevent the loss of active substance from can completely cut off again the air of the profound mould of leather, reach the effect of effectively mildew-resistant fast.
Antimildew and antibacterial cleansing cream prepared by the present invention, white, thickness, harmless, antimildew and antibacterial agent and beeswax add the quality guaranteed period can improving self, the effect of long-acting mould-proof can be played again.The guard albumen added in paste, also can protect leather from the injury of other chemical substances to a certain extent.
The present invention compared with prior art has the following advantages:
1) lasting mildew-resistant and protection leather can be played, reduce leather nursing number of times.Can profound sterilization and maintenance leather, avoid traditional mould inhibitor and just carry out surface cleaning except mould, and fundamentally do not kill leather inside and to go mouldy the mould at position and repeatedly going mouldy of causing.
2) antimildew and antibacterial cleansing cream of the present invention uses ep-type material to make, and waits side effect to human non-toxic's evil.
3) there is maintenance, mildew-resistant, the several functions such as clean, the nursing of leather is once completed, be i.e. time saving and energy saving cost when again saving preparation and use.Can leather surface be cleaned, dispel mildew etc., highlight the gloss of leather simultaneously, make leather more attractive in appearance.Too increase the elasticity of leather simultaneously, extend the work-ing life of leather.
Embodiment
Below in conjunction with embodiments of the invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
A kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 1 ~ 4 part; Emulsifying agent 8 ~ 16 parts; Wax material 15 ~ 30 parts; Silicone oil 8 ~ 12 parts; Glycerine 5 ~ 10 parts; 3 ~ 8 parts, lanolin; 1 ~ 6 part, guard albumen; Solvent 20 ~ 60 parts.Also comprise spices 0.5 ~ 1 part and/or 0.5 ~ 1 part, the sodium hydroxide of weight part.
As preferably, a kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 2 parts; Emulsifying agent 12 ~ 16 parts; Wax material 25 ~ 28 parts; Silicone oil 9 ~ 10 parts; Glycerine 5 ~ 8 parts; 3 ~ 5 parts, lanolin; 1 ~ 2 part, guard albumen; Solvent 30 ~ 45 parts.
Solvent of the present invention comprises second alcohol and water, and the ratio of second alcohol and water is 1 ~ 3:2 ~ 5, and wherein ethanol is dehydrated alcohol, and water is distilled water.Emulsifying agent can select alkyl glycoside APG, olive emulsifying agent, tween-60, span-60, hexadecanol one or more.Wax material is one or more in beeswax, whiteruss, synthetic wax, carnauba wax.Antimildew and antibacterial agent can be biological mildew inhibitor, and this biological mildew inhibitor can be practised a ball game the mould inhibitor such as rhzomorph, Natta mycin for lactic acid; Spices is essence.
Embodiment 1
A kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: lactic acid is practised a ball game rhzomorph 1 part; Alkyl glycoside APG16 part; 2 parts, beeswax; Whiteruss 8 parts; Carnauba wax 5 parts; Silicone oil 8 parts; Glycerine 10 parts; 3 parts, lanolin; 6 parts, guard albumen; Ethanol 14 parts; 27 parts, water.
Concrete preparation method is as follows:
1) first the wax material (beeswax, whiteruss and carnauba wax) of formula ratio and lanolin are placed in reactor, 80 DEG C of water-baths are to melting completely, then add the solvent of formula ratio and mix, finally add the silicone oil of described formula ratio, glycerine and guard albumen and mix;
2) to step 1) add the emulsifying agent of formula ratio in the solution that obtains, stir 15min at 35 DEG C, then constant temperature leaves standstill 20min;
3) to step 2) lactic acid that adds formula ratio in the solution that obtains to practise a ball game rhzomorph, stirs 25min and obtain paste at 75 DEG C;
4) by step 3) after the paste that obtains is cooled to room temperature, filling.
Embodiment 2
A kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 4 parts; Alkyl glycoside APG8 part; 15 parts, beeswax; Carnauba wax 15 parts; Silicone oil 12 parts; Glycerine 5 parts; 8 parts, lanolin; 2 parts, guard albumen; 1 part, sodium hydroxide; Ethanol 5 parts; 25 parts, water.
Concrete preparation method is as follows:
1) first the wax material (beeswax and carnauba wax) of formula ratio and lanolin are placed in reactor, 70 DEG C of water-baths are to melting completely, then add the solvent of formula ratio and sodium hydroxide and mix, finally add the silicone oil of described formula ratio, glycerine and guard albumen and mix;
2) to step 1) add the emulsifying agent of formula ratio in the solution that obtains, stir 10min at 40 DEG C, then constant temperature leaves standstill 10min;
3) to step 2) add the antimildew and antibacterial agent of formula ratio in the solution that obtains, stir 25min at 75 DEG C, obtain paste;
4) by step 3) after the paste that obtains is cooled to room temperature, filling.
Embodiment 3
A kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 2 parts; Emulsifying agent 15 parts; Wax material 25 parts; Silicone oil 10%; Glycerine 8%; Lanolin 5%; Guard albumen 2%; Spices 0.5 part; Ethanol 20 parts; 13 parts, water.
Concrete preparation method is as follows:
1) be first placed in reactor by the wax material of formula ratio and lanolin, 80 DEG C of water-baths, to melting completely, then add the solvent of formula ratio and mix, finally add the silicone oil of described formula ratio, glycerine and guard albumen and mix;
2) to step 1) add the emulsifying agent of formula ratio in the solution that obtains, stir 25min at 35 DEG C, then constant temperature leaves standstill 20min;
3) to step 2) lactic acid that adds formula ratio in the solution that obtains to practise a ball game rhzomorph, stirs 25min and obtain paste at 70 DEG C;
4) by step 3) after the paste that obtains is cooled to room temperature, filling.
Embodiment 4
A kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 2 parts; Alkyl glycoside APG6 part; Tween-606 part; Synthetic wax 10 parts; Carnauba wax 18 parts; Silicone oil 9 parts; Glycerine 5 parts; 3 parts, lanolin; 1 part, guard albumen; Spices 1 part; 0.5 part, sodium hydroxide; Ethanol 15 parts; 25 parts, water.
Concrete preparation method is as follows:
1) first the wax material (synthetic wax and carnauba wax) of formula ratio and lanolin are placed in reactor, 70 DEG C of water-baths are to melting completely, then add the solvent of formula ratio and mix, finally add the silicone oil of described formula ratio, glycerine and guard albumen and mix;
2) to step 1) add the emulsifying agent of described formula ratio in the solution that obtains, stir 25min at 40 DEG C, then constant temperature leaves standstill 16min;
3) to step 2) add the antimildew and antibacterial agent of described formula ratio in the solution that obtains, stir 30min at 72 DEG C and obtain paste;
4) by step 3) after the paste that obtains is cooled to room temperature, filling.
Embodiment 5
A kind of antimildew and antibacterial cleansing cream, comprises the raw material of following weight part: antimildew and antibacterial agent 2 parts; Tween-608 part; Alkyl glycoside APG6 part; Tegin 55G 1 part; Hexadecanol 1 part; 14 parts, beeswax; Whiteruss 1 part; Silicone oil 10 parts; Glycerine 10 parts; 5 parts, lanolin; 1 part, guard albumen; 0.5 part, sodium hydroxide; 0.5 part, essence; Ethanol 15 parts; 25 parts, water.
Concrete preparation method is as follows:
1) first the wax material (beeswax and whiteruss) of formula ratio and lanolin are placed in reactor, 80 DEG C of water-baths are to melting completely, then add the solvent (second alcohol and water) of formula ratio and mix, finally add the silicone oil of described formula ratio, glycerine and guard albumen and mix;
2) to step 1) add the emulsifying agent (Tween-60, alkyl glycoside APG, Tegin 55G and hexadecanol) of formula ratio in the solution that obtains, stir 15min at 35 DEG C, then constant temperature leaves standstill 20min;
3) to step 2) add the antimildew and antibacterial agent of formula ratio in the solution that obtains, stir 25min at 75 DEG C and obtain paste;
4) by step 3) after the paste that obtains is cooled to room temperature, filling.
Antimildew and antibacterial cleansing cream prepared by embodiment 1 ~ 5 is all creamy white, fine and smooth even, fragrant, and has very high stability.
Leather mildew-proof measure of merit: bronze-colored pearly-lustre cladding (Di Xin furniture company limited) is cut into 5 × 5cm for subsequent use.Blank group is not for carrying out the cladding processed, and control group is the cladding wiped across with yellow space board fur clothing nursing ointment antimildew and antibacterial cream, and experimental group 1 ~ 5 is carry out by embodiment 1 ~ 5 cladding that wipes across respectively.To be positioned on the culture plate that is coated with and mixes mould (aspergillus niger, Penicillum glaucum, aspergillus versicolor and flavus) (often group has 3 repetitions) under above-mentioned cladding aseptic condition, the culture dish being placed with cladding is placed in 28 DEG C, 14d is cultivated under relative humidity 90% condition, culture dish taking-up after cultivating is observed and recorded experimental result, judges to carry out mildew-resistant ranking according to the evaluation criteria shown in table 1 simultaneously.
Table 1 sample mildew-resistant grading standard
Table 2 sample mildew-resistant grade
As known in table 2, when not processing cladding cultivate cladding area after 14d 74.6% all length have mildew, 13.3% length of the control group cladding area of wiping yellow space board fur clothing nursing ointment antimildew and antibacterial cream has mildew, and use the experimental group of the antimildew and antibacterial cleansing cream of embodiments of the invention 1 ~ 5 all not have mildew to grow, mildew-resistant grade reaches 0 grade, and culture plate does not also grow mould with cladding contact site, effectively prevent the growth and breeding of mould.
The application of a kind of antimildew and antibacterial cleansing cream of the present invention in cladding: utilize antimildew and antibacterial cleansing cream wiping cladding of the present invention, effectively can dispel the bacterial plaque of leather surface, when antimildew and antibacterial cleansing cream coats leather surface, without granular sensation, leather surface is glossy.Because paste is the color that oyster white can not change leather itself, so applied widely, be not only applicable to dark leather and be applicable to light-colored leather yet.Antimildew and antibacterial cleansing cream room temperature left standstill after 6 months, and smell is unchanged, and during use, anti-mold effect is constant.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. an antimildew and antibacterial cleansing cream, is characterized in that, comprises the raw material of following weight part: antimildew and antibacterial agent 1 ~ 4 part; Emulsifying agent 8 ~ 16 parts; Wax material 15 ~ 30 parts; Silicone oil 8 ~ 12 parts; Glycerine 5 ~ 10 parts; 3 ~ 8 parts, lanolin; 1 ~ 6 part, guard albumen; Solvent 20 ~ 60 parts.
2. antimildew and antibacterial cleansing cream according to claim 1, is characterized in that, comprises the raw material of following weight part: antimildew and antibacterial agent 2 parts; Emulsifying agent 12 ~ 16 parts; Wax material 25 ~ 28 parts; Silicone oil 9 ~ 10 parts; Glycerine 5 ~ 8 parts; 3 ~ 5 parts, lanolin; 1 ~ 2 part, guard albumen; Solvent 30 ~ 45 parts.
3. antimildew and antibacterial cleansing cream according to claim 1, is characterized in that, comprises the raw material of following weight part: antimildew and antibacterial agent 2 parts; Emulsifying agent 15 parts; Wax material 25 parts; Silicone oil 10 parts; Glycerine 8 parts; 5 parts, lanolin; 2 parts, guard albumen; Solvent 33 parts.
4. antimildew and antibacterial cleansing cream according to claim 1, is characterized in that, comprises the raw material of following weight part: antimildew and antibacterial agent 2 parts; Emulsifying agent 16 parts; Wax material 15 parts; Silicone oil 10 parts; Glycerine 10 parts; 5 parts, lanolin; 1 part, guard albumen; Solvent 40 parts.
5. the antimildew and antibacterial cleansing cream according to any one of Claims 1 to 4, is characterized in that, also comprises the spices 0.5 ~ 1 part of weight part.
6. the antimildew and antibacterial cleansing cream according to any one of Claims 1 to 4, is characterized in that, also comprises 0.5 ~ 1 part, the sodium hydroxide of weight part.
7. the antimildew and antibacterial cleansing cream according to any one of Claims 1 to 4, is characterized in that, described solvent comprises second alcohol and water, and the ratio of second alcohol and water is 1 ~ 3:2 ~ 5.
8. antimildew and antibacterial cleansing cream according to claim 1, is characterized in that, antimildew and antibacterial agent is biological mildew inhibitor.
9. a preparation method for antimildew and antibacterial cleansing cream according to claim 1, is characterized in that, specifically comprise the following steps:
1) be first placed in reactor by the wax material of described formula ratio and lanolin, 70 ~ 85 DEG C of water-baths, to melting completely, then add the solvent of formula ratio and mix, finally add the silicone oil of described formula ratio, glycerine and guard albumen and mix;
2) to step 1) add the emulsifying agent of described formula ratio in the solution that obtains, stir 10 ~ 25min at 35 ~ 40 DEG C, then constant temperature leaves standstill 8 ~ 20min;
3) to step 2) add the antimildew and antibacterial agent of described formula ratio in the solution that obtains, stir 20 ~ 30min at 65 ~ 75 DEG C and obtain paste;
4) by step 3) described in paste be cooled to room temperature after, filling.
10. the application of antimildew and antibacterial cleansing cream in Leather mildew-proof prepared according to claim 1.
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| CN201510595437.9A CN105219539A (en) | 2015-09-17 | 2015-09-17 | A kind of antimildew and antibacterial cleansing cream and preparation method thereof and application |
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| CN106148579A (en) * | 2016-08-30 | 2016-11-23 | 晋江市永建皮革制品有限公司 | A kind of antibacterial leather of resistance to wet rubbing and processing technology thereof |
| CN108485843A (en) * | 2018-03-05 | 2018-09-04 | 苏州绿叶日用品有限公司 | One kind removing mould detergent |
| CN110684603A (en) * | 2019-09-26 | 2020-01-14 | 广东中联邦精细化工有限公司 | Leather cleaning agent and preparation method thereof |
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