CN104840408A - Quail egg hydrolysate containing hand cream and preparation method for same - Google Patents
Quail egg hydrolysate containing hand cream and preparation method for same Download PDFInfo
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Abstract
The invention belongs to the field of cosmetics, and particularly relates to quail egg hydrolysate containing hand cream, which comprises the following raw materials in percentage by mass: 10 to 20 percent of glycerin, 5 to 10 percent of quail egg hydrolysate, 5 to 10 percent of mineral oil, 2 to 5 percent of isopropyl palmitate, 2 to 5 percent of polydimethylsiloxane, 1 to 3 percent of shea butter, 1 to 3 percent of cetearyl alcohol, 5 to 10 percent of sorbitol, 1 to 3 percent of jojoba oil, 25 to 45 percent of de-ionized water and 0.05 to 0.2 percent of phenoxyethanol. According to the quail egg hydrolysate containing hand cream, the quail egg hydrolysate is employed as an active ingredient, the hand cream contains rich substances such as keratin, lysine, vitamin B2 and vitamin B1, and glycerin, sorbitol, the oily ingredient mineral oil, isopropyl palmitate, polydimethylsiloxane, shea butter, cetearyl alcohol and jojoba oil are properly mixed, so that the hand cream has the effects of moistening skin, resisting bacteria, preserving moisture and enhancing skin elasticity.
Description
Technical field
The present invention relates to a kind of hand cream, especially a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution and preparation method thereof.
Background technology
There is fowl egg resource the abundantest in the world in China, and fowl egg output is sure to occupy No. 1 in the world.Ovum Coturnicis japonicae contains rich in protein, lysine, vitamin B2, vitamin B1, keeps fit the effect such as brain-strengthening, rich flesh skin care, has been widely used in health food, but its application in cosmetics is few.
Summary of the invention
Technical problem to be solved by this invention is the deficiency that exists for above-mentioned prior art and provides a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution and preparation method thereof, with Ovum Coturnicis japonicae hydrolyzed solution for active component, there is the effect of skin moistening, antibacterial, moisturizing, enhancing skin elasticity.
The technical scheme that the problem that the present invention is the above-mentioned proposition of solution adopts is:
Containing a hand cream for Ovum Coturnicis japonicae hydrolyzed solution, its raw material by mass percentage, comprises following component: glycerol 10 ~ 20%, Ovum Coturnicis japonicae hydrolyzed solution 5 ~ 10%, Dormant oils 5 ~ 10%, isopropyl palmitate 2 ~ 5%, polydimethylsiloxane 2 ~ 5%, shea butter 1 ~ 3%, cetearyl alcohol 1 ~ 3%, sorbitol 5 ~ 10%, Jojoba oil 1 ~ 3%, deionized water 25 ~ 45%, phenoxyethanol 0.05 ~ 0.2%.
By such scheme, the mass fraction of described Ovum Coturnicis japonicae hydrolyzed solution is 60% ~ 70%.
By such scheme, Quail Egg Powder enzymolysis obtains by described Ovum Coturnicis japonicae hydrolyzed solution.
By such scheme, the concrete preparation method of described Ovum Coturnicis japonicae hydrolyzed solution is: get the cleaning of new fresh quail egg and remove dirt, shell, obtain Quail Egg Powder after immersing NaOH solution sterilization; Add enzyme and water by described Quail Egg Powder, in 45 DEG C ~ 55 DEG C enzymolysis 4 ~ 5 hours, namely obtain Ovum Coturnicis japonicae hydrolyzed solution.Wherein, described enzyme is neutral papain, and the quality of neutral protease is 0.1% ~ 0.5% of described Ovum Coturnicis japonicae hydrolyzed solution; Described NaOH solution mass concentration is 2% ~ 5%, and disinfecting time is 5 ~ 10min.
The preparation method of the above-mentioned hand cream containing Ovum Coturnicis japonicae hydrolyzed solution, comprises the steps:
1) by mass percentage, following raw material is taken: glycerol 10 ~ 20%, Ovum Coturnicis japonicae hydrolyzed solution 5 ~ 10%, Dormant oils 5 ~ 10%, isopropyl palmitate 2 ~ 5%, polydimethylsiloxane 2 ~ 5%, shea butter 1 ~ 3%, cetearyl alcohol 1 ~ 3%, sorbitol 5 ~ 10%, Jojoba oil 1 ~ 3%, deionized water 25 ~ 45%, phenoxyethanol 0.05 ~ 0.2%, for subsequent use;
2) by Dormant oils, isopropyl palmitate, polydimethylsiloxane, shea butter, cetearyl alcohol, Jojoba oil mixing, 80 ~ 85 DEG C are then warming up to, insulation 20 ~ 30min;
3) glycerol, sorbitol, deionized water are mixed and are warming up to 80 ~ 85 DEG C, insulation 20 ~ 30min, then adds step (2) gained material and wherein carries out emulsifying homogeneous;
4) until step 3) gained temperature of charge is down to after below 50 DEG C, adds Ovum Coturnicis japonicae hydrolyzed solution and phenoxyethanol stirs, and obtains the hand cream containing Ovum Coturnicis japonicae hydrolyzed solution.
By such scheme, described step 3) in the speed of emulsifying homogeneous be 2000 ~ 3000r/min, the time is advisable with 5 ~ 10min.
By such scheme, described step 4) the middle speed 100 ~ 300r/min stirred, the time is advisable with 10 ~ 30min.
Hand cream containing Ovum Coturnicis japonicae hydrolyzed solution of the present invention, its feature is: Ovum Coturnicis japonicae is through the hydrolysis of protease appropriateness, deactivation injurious factor and protease inhibitor also obtain has bioactive polypeptide, biologically active polypeptide has hormonal regulation, enzyme level, antibacterial, prolongation cell survival, keep the different physiological roles such as cell viability, be more conducive to skin and absorb.The present invention just with Ovum Coturnicis japonicae hydrolyzed solution for active component, with Carnis Coturnicis japonicae enzymolysis solution for main prolongation cell survival, frivolous glycerol and sorbitol, Dormant oils is selected to be moisturizing system, add siliceous polydimethylsiloxane, isopropyl palmitate is forwards composition, make it have good ductility, screening characteristics and clearly spend, have good affinity with skin, easily absorb by skin histology, make skin emolliency; Add pure natural plant oils and fats shea butter, superpower antioxidant effect, gentle non-stimulated, and Jojoba oil main component is unsaturated higher alcohol and fatty acid, there is good stability, very easily merge with skin, there is non-oxidizability free from worldly cares, cetearyl alcohol then fully can ensure the stable of oil-in-water type emulsion body, there is suppression greasy feeling, reduce wax class raw material stickiness, the effect of true emulsion, the skin moistening of the comprehensive degree of depth of skin, antibacterial, moisturizing, enhancing skin elasticity, crease-resistant, antioxidative effect are provided, gentle non-stimulated.
Detailed description of the invention
In order to understand the present invention better, illustrate content of the present invention further below in conjunction with embodiment, but the present invention is not only confined to the following examples.
In embodiment, glycerol is pharmaceutical grade, content>=99.9%; Dormant oils is cosmetic level white mineral oil; Isopropyl palmitate outward appearance is colourless transparent oil liquid, containing ester amount>=99%; Polydimethylsiloxane is cosmetics-stage transparency liquid; Shea butter is oil-soluble white solid; Cetearyl alcohol is cosmetics-stage solid; The as clear as crystal oily liquids of Jojoba oil cosmetics-stage, acid number≤1.0mgKOH/g, peroxide value≤5.0meq O
2/ Kg.
Embodiment 1
Containing a hand cream for Ovum Coturnicis japonicae hydrolyzed solution, its raw material by mass percentage, comprises following component: glycerol 10%, Ovum Coturnicis japonicae hydrolyzed solution 10%, Dormant oils 10%, isopropyl palmitate 5%, polydimethylsiloxane 5%, shea butter 3%, cetearyl alcohol 3%, sorbitol 10%, Jojoba oil 3%, deionized water 40.95%, phenoxyethanol 0.05%.
The mass fraction of the hydrolyzed solution of Carnis Coturnicis japonicae described in the present embodiment is about 60%, and concrete preparation method is: get the cleaning of new fresh quail egg and remove dirt, after immersing 5wt%NaOH solution disinfection, 5min shells and obtains Quail Egg Powder; The neutral papain of 40g water and 0.1g will be added in 60g Quail Egg Powder, in 45 DEG C of stirred in water bath enzymolysis 4 hours, namely obtain Ovum Coturnicis japonicae hydrolyzed solution.
The preparation method of the above-mentioned hand cream containing Ovum Coturnicis japonicae hydrolyzed solution, comprises the steps:
1) by mass percentage, following raw material is taken: glycerol 10%, Ovum Coturnicis japonicae hydrolyzed solution 10%, Dormant oils 10%, isopropyl palmitate 5%, polydimethylsiloxane 5%, shea butter 3%, cetearyl alcohol 3%, sorbitol 10%, Jojoba oil 3%, deionized water 40.95%, phenoxyethanol 0.05%, for subsequent use;
2) by Dormant oils, isopropyl palmitate, polydimethylsiloxane, shea butter, cetearyl alcohol, Jojoba oil mixing, 80 DEG C are then warming up to, insulation 30min;
3) glycerol, sorbitol, deionized water are mixed and are warming up to 80 DEG C, insulation 30min, then adds wherein by step (2) gained material, opens emulsifying homogeneous machine, adopts 3000r/min homogenizing 8min;
4) until step 3) after gained temperature of charge is down to 45 DEG C, add Ovum Coturnicis japonicae hydrolyzed solution and phenoxyethanol stirs 15min to evenly with speed 150r/min, obtain the hand cream containing Ovum Coturnicis japonicae hydrolyzed solution.
Embodiment 2
Containing a hand cream for Ovum Coturnicis japonicae hydrolyzed solution, its raw material by mass percentage, comprises following component: glycerol 20%, Ovum Coturnicis japonicae hydrolyzed solution 10%, Dormant oils 10%, isopropyl palmitate 5%, polydimethylsiloxane 5%, shea butter 3%, cetearyl alcohol 3%, sorbitol 10%, Jojoba oil 3%, deionized water 30.95%, phenoxyethanol 0.05%.
The mass fraction of the hydrolyzed solution of Carnis Coturnicis japonicae described in the present embodiment is about 70%, and concrete preparation method is: get the cleaning of new fresh quail egg and remove dirt, after immersing 5wt%NaOH solution disinfection, 10min shells and obtains Quail Egg Powder; The neutral papain of 30g water and 0.5g will be added in 70g Quail Egg Powder, in 45 DEG C of stirred in water bath enzymolysis 4 hours, namely obtain Ovum Coturnicis japonicae hydrolyzed solution.
The preparation method of the above-mentioned hand cream containing Ovum Coturnicis japonicae hydrolyzed solution, comprises the steps:
1) by mass percentage, following raw material is taken: glycerol 20%, Ovum Coturnicis japonicae hydrolyzed solution 10%, Dormant oils 10%, isopropyl palmitate 5%, polydimethylsiloxane 5%, shea butter 3%, cetearyl alcohol 3%, sorbitol 10%, Jojoba oil 3%, deionized water 30.95%, phenoxyethanol 0.05%, for subsequent use;
2) by Dormant oils, isopropyl palmitate, polydimethylsiloxane, shea butter, cetearyl alcohol, Jojoba oil mixing, 85 DEG C are then warming up to, insulation 20min;
3) glycerol, sorbitol, deionized water are mixed and are warming up to 85 DEG C, insulation 20min, then adds wherein by step (2) gained material, opens emulsifying homogeneous machine, adopts 2500r/min homogenizing 10min;
4) until step 3) after gained temperature of charge is down to 40 DEG C, add Ovum Coturnicis japonicae hydrolyzed solution and phenoxyethanol stirs 15min to evenly with speed 200r/min, obtain the hand cream containing Ovum Coturnicis japonicae hydrolyzed solution.
Embodiment 3
Containing a hand cream for Ovum Coturnicis japonicae hydrolyzed solution, its raw material by mass percentage, comprises following component: glycerol 20%, Ovum Coturnicis japonicae hydrolyzed solution 20%, Dormant oils 10%, isopropyl palmitate 5%, polydimethylsiloxane 5%, shea butter 3%, cetearyl alcohol 3%, sorbitol 10%, Jojoba oil 3%, deionized water 30.95%, phenoxyethanol 0.05%.
The mass fraction of the hydrolyzed solution of Carnis Coturnicis japonicae described in the present embodiment is about 60%, and concrete preparation method is: get the cleaning of new fresh quail egg and remove dirt, after immersing 5wt%NaOH solution disinfection, 10min shells and obtains Quail Egg Powder; The neutral papain of 40g water and 0.5g will be added in 60g Quail Egg Powder, in 45 DEG C of stirred in water bath enzymolysis 5 hours, namely obtain Ovum Coturnicis japonicae hydrolyzed solution.
The preparation method of the above-mentioned hand cream containing Ovum Coturnicis japonicae hydrolyzed solution, comprises the steps:
1) by mass percentage, take following raw material: glycerol 20%, Ovum Coturnicis japonicae hydrolyzed solution 20%, Dormant oils 10%, isopropyl palmitate 5%, polydimethylsiloxane 5%, shea butter 3%, cetearyl alcohol 3%, sorbitol 10%, Jojoba oil 3%, deionized water 30.95%, phenoxyethanol 0.05%;
2) by Dormant oils, isopropyl palmitate, polydimethylsiloxane, shea butter, cetearyl alcohol, Jojoba oil mixing, 85 DEG C are then warming up to, insulation 20min;
3) glycerol, sorbitol, deionized water are mixed and are warming up to 85 DEG C, insulation 20min, then adds wherein by step (2) gained material, opens emulsifying homogeneous machine, adopts 3000r/min homogenizing 10min;
4) until step 3) after gained temperature of charge is down to 30 DEG C, add Ovum Coturnicis japonicae hydrolyzed solution and phenoxyethanol stirs 20min to evenly with speed 200r/min, obtain the hand cream containing Ovum Coturnicis japonicae hydrolyzed solution.
The present invention stablizes containing the hand cream product stock of Ovum Coturnicis japonicae hydrolyzed solution, test specimen is placed in color-comparison tube, be placed in 40 ± 2 DEG C of constant incubators respectively and place 48h with-20 DEG C of refrigerators, return to room temperature to observe, send out phenomenon thick without oil-water separation and mastic, homogeneous, lasting fragrance, the heat-resisting cold tolerance of product is qualified.
Result of use is evaluated
The present invention is carried out to the result of use test of following project containing the hand cream product of Ovum Coturnicis japonicae hydrolyzed solution, and increase controlled trial, wherein matched group is certain brand hand cream commercially available, and result such as table 1 shows, scoring mechanism, wherein fine 9 ~ 10 points of effect are carried out in the evaluation of each project; Better 7 ~ 8 points of effect; General 5 ~ 6 points of effect; Poor 3 ~ 4 points of effect; Poor effect 1 ~ 2 point.
Whether 1, spreadability: whether product is easily sprawled in the process of smearing, can play informal voucher.
2, permeability (assimilation effect): in use, whether oils and fats wherein and active component etc. easily penetrate into skin to product.
3, moistness: whether product gives skin moisturizing sense.
4, greasy feeling: product use process in or without excessive greasy feeling.
5, direct usability: the situation of product above indices in use;
6, later stage usability: the situation of product above indices after using 10min.
Result of use method of testing is: experimenter's recipient site skin is all without exception, does not also smear any external preparation, dries, be coated on hand by hand cream after washing one's hands.The tested crowd often organized is: age 20-40 year, number 60 people, men and women half and half, gives respectively often to organize experimenter's mass-sending and to be rivals in a contest the hand cream of answering, and service time is 30 days, fills in the unified questionnaire formulated to evaluate after using, and evaluation result adopts average mark.
Table 1
| Project testing | Spreadability | Permeability | Moistness | Greasy feeling | Direct usability | Later stage usability |
| Product of the present invention | 9.5 | 9 | 10 | 10 | 10 | 9 |
| Matched group | 6 | 6 | 7 | 4 | 7 | 5 |
As seen from the above table, the hand cream product containing Ovum Coturnicis japonicae hydrolyzed solution of the present invention has excellent screening characteristics, smears in process and is easy to sprawl, and can not play informal voucher; And oils and fats wherein and active component etc. easily penetrate into skin, give skin moisturizing sense, but greasy feeling can not be produced, and effect is lasting.
The above is only the preferred embodiment of the present invention, it should be pointed out that for the person of ordinary skill of the art, and without departing from the concept of the premise of the invention, can also make some improvement and conversion, these all belong to protection scope of the present invention.
Claims (8)
1., containing a hand cream for Ovum Coturnicis japonicae hydrolyzed solution, the raw material that it is characterized in that it by mass percentage, comprises following component: glycerol 10 ~ 20%, Ovum Coturnicis japonicae hydrolyzed solution 5 ~ 10%, Dormant oils 5 ~ 10%, isopropyl palmitate 2 ~ 5%, polydimethylsiloxane 2 ~ 5%, shea butter 1 ~ 3%, cetearyl alcohol 1 ~ 3%, sorbitol 5 ~ 10%, Jojoba oil 1 ~ 3%, deionized water 25 ~ 45%, phenoxyethanol 0.05 ~ 0.2%.
2. a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution according to claim 1, is characterized in that the mass fraction of described Ovum Coturnicis japonicae hydrolyzed solution is 60% ~ 70%.
3. a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution according to claim 1, is characterized in that Quail Egg Powder enzymolysis obtains by described Ovum Coturnicis japonicae hydrolyzed solution.
4. a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution according to claim 1, is characterized in that the concrete preparation method of described Ovum Coturnicis japonicae hydrolyzed solution is: get the cleaning of new fresh quail egg and remove dirt, shell, obtain Quail Egg Powder after sterilization; Add enzyme and water by described Quail Egg Powder, in 45 DEG C ~ 55 DEG C enzymolysis 4 ~ 5 hours, namely obtain Ovum Coturnicis japonicae hydrolyzed solution.
5. a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution according to claim 4, it is characterized in that described enzyme is neutral papain, the quality of neutral protease is 0.1% ~ 0.5% of described Ovum Coturnicis japonicae hydrolyzed solution.
6. the preparation method of a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution according to claim 1, is characterized in that it comprises the steps:
1) by mass percentage, following raw material is taken: glycerol 10 ~ 20%, Ovum Coturnicis japonicae hydrolyzed solution 5 ~ 10%, Dormant oils 5 ~ 10%, isopropyl palmitate 2 ~ 5%, polydimethylsiloxane 2 ~ 5%, shea butter 1 ~ 3%, cetearyl alcohol 1 ~ 3%, sorbitol 5 ~ 10%, Jojoba oil 1 ~ 3%, deionized water 25 ~ 45%, phenoxyethanol 0.05 ~ 0.2%, for subsequent use;
2) by Dormant oils, isopropyl palmitate, polydimethylsiloxane, shea butter, cetearyl alcohol, Jojoba oil mixing, 80 ~ 85 DEG C are then warming up to, insulation 20 ~ 30min;
3) glycerol, sorbitol, deionized water are mixed and are warming up to 80 ~ 85 DEG C, insulation 20 ~ 30min, then adds step (2) gained material and wherein carries out emulsifying homogeneous;
4) until step 3) gained temperature of charge is down to after below 50 DEG C, adds Ovum Coturnicis japonicae hydrolyzed solution and phenoxyethanol stirs, and obtains the hand cream containing Ovum Coturnicis japonicae hydrolyzed solution.
7. the preparation method of a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution according to claim 6, is characterized in that described step 3) in the speed of emulsifying homogeneous be 2000 ~ 3000r/min, the time is 5 ~ 10min.
8. the preparation method of a kind of hand cream containing Ovum Coturnicis japonicae hydrolyzed solution according to claim 6, is characterized in that described step 4) the middle speed 100 ~ 300r/min stirred, the time is 10 ~ 30min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510264362.6A CN104840408B (en) | 2015-05-21 | 2015-05-21 | A kind of hand lotion of the hydrolyzate containing quail egg and preparation method thereof |
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| CN201510264362.6A CN104840408B (en) | 2015-05-21 | 2015-05-21 | A kind of hand lotion of the hydrolyzate containing quail egg and preparation method thereof |
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Cited By (3)
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| CN105125464A (en) * | 2015-09-22 | 2015-12-09 | 夏放军 | Eye cream and preparation method thereof |
| CN106265428A (en) * | 2016-08-24 | 2017-01-04 | 湖北神丹健康食品有限公司 | Ovum Gallus domesticus album skin protection facial cream |
| CN113208989A (en) * | 2021-03-31 | 2021-08-06 | 湖北神丹健康食品有限公司 | Preserved egg gel paste and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105125464A (en) * | 2015-09-22 | 2015-12-09 | 夏放军 | Eye cream and preparation method thereof |
| CN106265428A (en) * | 2016-08-24 | 2017-01-04 | 湖北神丹健康食品有限公司 | Ovum Gallus domesticus album skin protection facial cream |
| CN113208989A (en) * | 2021-03-31 | 2021-08-06 | 湖北神丹健康食品有限公司 | Preserved egg gel paste and preparation method thereof |
| CN113208989B (en) * | 2021-03-31 | 2023-06-27 | 湖北神丹健康食品有限公司 | Preserved egg gel paste and preparation method thereof |
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| CN104840408B (en) | 2017-12-08 |
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