CN106974857A - A kind of antibacterial mildy wash - Google Patents
A kind of antibacterial mildy wash Download PDFInfo
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- CN106974857A CN106974857A CN201710192429.9A CN201710192429A CN106974857A CN 106974857 A CN106974857 A CN 106974857A CN 201710192429 A CN201710192429 A CN 201710192429A CN 106974857 A CN106974857 A CN 106974857A
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- antibacterial
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a kind of antibacterial mildy wash, mainly include the compositions such as 0.5 2.5 parts of locust tree flower extract, 1.1 2.8 parts of sea-buckthorn seed extract, 0.1 0.5 parts of thyme essential oil.Locust tree flower extract inhibiting bacteria and diminishing inflammation, nutrition skin；Thyme essential oil destroys bacterioprotein structure, reaches bactericidal effect；Seabuckthorn seeds extraction of substance broad-spectrum antibacterial, three Plant Extracts compounding uses, synergy, maintenance one makes this product have significant antibacterial face-nursing function；And the surfactant provided has excellent foaming power, clean power and degreasing power, is aided with the emollient of moist pro-skin, each composition coordinative role, excitant is small, the use of rear skin is not in dry and astringent, tight feeling, safe.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of antibacterial mildy wash.
Background technology
Mildy wash is that sales volume rises faster class face cleaning product in recent years, and its decontamination mechanism is to utilize surface-active
Agent reduces the surface tension of dirt, dirt is removed by the effect such as wetting, scattered, foaming, emulsification, because of the surfactant of compounding
Difference, foaming power, cleaning strength and excitant are all different.In addition, human body face is exposed in atmosphere, dust, particle, You Haiqi
Body can all be damaged to skin, cause inflammation, and the presence of various bacteriums also increases inflammation odds, so
A inhibiting bacteria and diminishing inflammation face cleaning product is researched and developed, is necessary in skin-protection product.
At present, on the market there is the problem of table surfactant compatibility is improper in face cleaning product, cleaning effect can be caused bad；
Or in order to reach certain effect, the harmful substance of infringement skin is added, such skin care item, security is extremely low；In inhibiting bacteria and diminishing inflammation
The big medicine of side effect is added in product, is used for a long time, skin can be made to produce drug resistance, skin interior tissue is damaged, causes more
Big skin hidden danger.
The content of the invention
In view of the above-mentioned problems, the present invention provides a kind of gentle, safe and efficient antibacterial mildy wash.
To reach the effect above, the present invention is adopted the following technical scheme that：
A kind of described antibacterial mildy wash mainly include 0.2-3 parts of locust tree flower extract, 0.1-3 parts of sea-buckthorn seed extract,
0.01-1 parts of thyme essential oil.
Preferably, the mildy wash mainly include 0.5-2.5 parts of locust tree flower extract, 1.1-2.8 parts of sea-buckthorn seed extract,
0.1-0.5 parts of thyme essential oil.
The locust tree flower extract and sea-buckthorn seed extract are prepared by the following method：Pagoda Flower, seabuckthorn seeds are mixed and cut
Tumblied Dry under the conditions of broken latter 40-60 DEG C；The material body of above-mentioned drying is added in 60%-80% ethanol, using frequency
The ultrasonication that rate is 20kHZ 3-5 minutes, then reflux extraction 5-12h, filter off residue, by filtrate 6000r/min-8000r/
15-30min is centrifuged under the conditions of min and obtains the Pagoda Flower, sea-buckthorn seed extract mixed liquor.
The mildy wash also includes following component：0.5-2 parts of surfactant, 1-3 parts of emulsifying agent, thickener 0.05-0.3
Part, 0.01-0.5 parts of preservative, 5-9 parts of emollient, 15-40 parts of glycerine, 0.02-0.3 parts of potassium hydroxide, 1-3 parts of stearic acid.
Further, the surfactant is sodium lauryl sulfate, alkyl sulfate, lauroyl ether sodium sulfate, 12
At least one of sodium alkyl sulfate.
Further, the emulsifying agent is myristic acid, methyl sesquistearate, PEG-20 methyl sesquialters
At least one of stearate.
Further, the thickener be carbomer, xanthans, hydroxyethyl cellulose, sodium carboxymethylcellulose in extremely
Few one kind.
Further, the preservative is at least one of Phenoxyethanol, sodium benzoate, methyl hydroxybenzoate, Nipasol.
Further, the emollient is saualane, cetostearyl alcohol, dimethyl silicone polymer, Butyrospermum parkii fruit fat, hydrogen
Change at least one of jojoba oil, polydimethyl siloxanes/polydimethy siloxanes alcohol.
The present invention also provides the preparation method of antibacterial mildy wash, comprises the following steps：By emulsifying agent, emollient input oil phase
In pot, 70-85 DEG C is heated to, waits all components to be incubated after dissolving, A phases is made；By glycerine, stearic acid, thickener and deionization
Water is put into aqueous phase pot successively, is heated to 70-85 DEG C, insulation 15-30min makes it fully dissolve, and B phases are made；A phases, B is interdependent
Secondary to be pumped into emulsification pot, homogeneous 5-15min, stir speed (S.S.) is 2000-4000r/min, then insulated and stirred 15-45min, is stirred
Speed is mixed for 30-50r/min；40-45 DEG C is cooled to, potassium hydroxide is added, stirs；Add locust tree flower extract, sea-buckthorn
Seed extract, thyme essential oil, preservative, stir, and obtain the antibacterial mildy wash.
Following introduction is done to the fractions of the present invention：
Contain higher protein, trace element, vitamins and other nutritious components in locust tree flower extract, also containing substantial amounts of
Flavonoids specific function composition, mainly including rutin, robinin, cyanidenon, Quercetin etc..Pagoda Flower contains 10%~
20% rutin, it has significant anti-inflammatory, effect that is antiviral, suppressing aldose reductase activity；Cyanidenon has anti-
Bacterium, anti-inflammatory, spasmolysis, suppression enzyme, a variety of effects such as anti-oxidant.In addition, the ortho-aminobenzoic acid formicester contained in spending, nerol, virtue
Camphor tree alcohol, benzylalcohol etc. have beauty care effect, are a kind of rare health-care and skin-care good merchantable brands.
Main bacteriostatic compound is phenols in thyme essential oil, and phenols can pass through hydrogen bond or thin with the protein on cell membrane
Water interaction mode is combined, and destroys the integrality of protein structure, makes protein denaturation or activity reduction, cytoplasma membrane
Permeability increase, causes iuntercellular content mutually to ooze, and causes bacterial cell physiological dysfunction even dead.
Contain abundant bioactive substance, predominantly phytosterol, Flavonoid substances, plant in seabuckthorn seeds extraction of substance
Phosphatide and vitamin C, to staphylococcus aureus, bacillus subtilis, Escherichia coli and pseudomonas aeruginosa have stronger
Bacteriostasis.Wherein phytosterol is the main active of performance bacteriostasis in sea-buckthorn seed extract.
The device have the advantages that as follows：(1) locust tree flower extract inhibiting bacteria and diminishing inflammation, nutrition skin；Thyme essential oil
Bacterioprotein structure is destroyed, bactericidal effect is reached；Seabuckthorn seeds extraction of substance broad-spectrum antibacterial, three Plant Extracts compounding uses,
Synergy, maintenance one makes this product have significant antibacterial face-nursing function；(2) the surfactant tool that the present invention is provided
There are excellent foaming power, clean power and degreasing power, be aided with the emollient of moist pro-skin so that this product is salubrious, uses rear skin
It is not in dry and astringent, tight feeling；(3) plant component and other base-material compatibilities of the invention are good so that mildy wash of the invention
Stability is good.And each composition coordinative role, excitant is small, safe.
Embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.
The following component title occurred in text is INCI (Internation NomenclaureCosmetic
Ingredent, i.e. international cosmetic raw material name) institute to defined title：Polydimethyl siloxanes/polydimethy siloxanes
Alcohol.
The antibacterial mildy wash formula of the invention of the embodiment of the present invention 1~5 is shown in Table one
The preparation method of the antibacterial mildy wash of embodiment 1~5 comprises the following steps：By myristic acid, methyl times semihard
In resin acid ester, PEG-20 methyl sesquistearates, saualane, cetostearyl alcohol, dimethyl silicone polymer, Butyrospermum parkii
Fruit fat, hydrogenated jojoba oil, polydimethyl siloxanes/polydimethy siloxanes alcohol, sodium lauryl sulfate, alkyl sulfate, the moon
In osmanthus acyl ether sodium sulfate, lauryl sodium sulfate input oil phase pot, 70-85 DEG C is heated to, waits all components to be incubated after dissolving, system
Obtain A phases；Glycerine, stearic acid, carbomer, xanthans, hydroxyethyl cellulose, sodium carboxymethylcellulose and deionized water are thrown successively
Enter in aqueous phase pot, be heated to 70-85 DEG C, insulation 15-30min makes it fully dissolve, and B phases are made；A phases, B phases are pumped into successively
Emulsify in pot, homogeneous 5-15min, stir speed (S.S.) is 2000-4000r/min, then insulated and stirred 15-45min, and stir speed (S.S.) is
30-50r/min；40-45 DEG C is cooled to, potassium hydroxide is added, stirs；Add locust tree flower extract, sea-buckthorn seed extract,
Thyme essential oil, Phenoxyethanol, sodium benzoate, methyl hydroxybenzoate, Nipasol, stir, and obtain the antibacterial mildy wash.
Comparative example 1
Difference with embodiment 1 is not add locust tree flower extract, and other preparation conditions and method are same as Example 1.
Comparative example 2
Difference with embodiment 1 is not add sea-buckthorn seed extract, and other preparation conditions and method are same as Example 1.
Comparative example 3
Difference with embodiment 1 is not add thyme essential oil, and other preparation conditions and method are same as Example 1.
Comparative example 4
Difference with embodiment 1 is not add locust tree flower extract, sea-buckthorn seed extract and thyme essential oil, other preparations
Condition and method are same as Example 1.
Comparative example 5
Difference with embodiment 1 is that Pagoda Flower extract weight number is 2.6 parts, other preparation conditions and method and implementation
Example 1 is identical.
Skin Irritation Test
(1) test specimen：The antibacterial mildy wash of embodiment 1；
(2) experimental animal：Small white mouse
(3) 24h shaves off small white mouse back cervical vertebra diamond wool before testing, unhairing scope or so 2cm × 2cm, and side is used for
Experiment, side is used to compare, and skin is cleaned using warm water, then wipes test specimen on a side test skin, wipes daily
Wipe 1 time, 1h observes skin wound repair after wiping, continuous to wipe 7 days.
(4) result of the test：, never there is erythema oedema etc. using the antibacterial mildy wash of embodiment 1 in 7 days Skin Irritation Tests
Etc. stimulate the reaction.
Antibacterial sterilizing test
The protective system efficiency evaluation side that this experiment is recommended with reference to U.S.'s cosmetics, toilet articles and essence association (CTFA)
Method, is tested with the CTFA classical sterilizing single challenges of 28 days by a definite date recommended.
1. microorganism is used in challenge：Dermatophyte (including fungi, candida albicans, mould, bacterium)
2. the mode and quantity of inoculation
(1) mode of inoculation：Using combined inoculation.Because the microorganism of nature has the characteristics of mixed life is lived together, mix
Splice grafting kind meets the situation of actual pollution.
(2) quantity of inoculation：Each strain is inoculated in suitable culture medium, in 28 DEG C (fungies), 36 DEG C (candida albicans),
Cultivated in 28 DEG C (mould), 37 DEG C of (bacterium) incubators.Fungi, candida albicans, mycotic culture 72 hours, Bacteria Culture 48 hours
Afterwards, select typical bacterium colony and certain density fungi, candida albicans, mould, bacterium mixing are made in the fluid nutrient medium of sterilizing
Suspension, is placed in refrigerator cold-storage standby.Fungi, candida albicans, every gram of suspension bacteria containing amount of mould are 1 × 105CFU/g or CFU/ml；
Every gram of suspension bacteria containing amount of bacterium is 1 × 106CFU/g or CFU/ml.
3. Microbial Challenge is tested
Experimental example 1~5 and the antibacterial mildy wash 100ml of comparative example 1~5 are measured, in the container for adding sterilizing, mixing is added true
Bacterium, candida albicans, mould, bacterial suspension, fully mix.Every gram of sample is 1 × 10 containing fungi, candida albicans, mould amount5CFU/g
Or CFU/ml；Amount of bacteria is 1 × 106CFU/g or CFU/ml.It is subsequently placed at 28 DEG C.Connect bacterium 0,7,14,21,28 days take
Sample is analyzed：10ml samples accurately are measured, are added in the conical flask containing glass pellet and 90ml sterile salines, fully shaking
Mix, this suspension is 1：10 dilutions, then press 1 with physiological saline again：10 dilute successively.At 28 DEG C of fungi cultivate 72 hours,
Cultivate 72 hours, cultivated 48 hours at 37 DEG C of bacterium, by flat board tilt-pour process at culture 72 hours, 28 DEG C of mould at 36 DEG C of candida albicans
Bacteria containing amount in count samples.
4. evaluation method
Show in 28 days samples containing fungi, candida albicans, mould or bacterium at 10CFU/g~100CFU/g (CFU/ml)
The sample has stronger suppression to kill effect to dermatophyte, is tested by challenging, 1000CFU/g (CFU/m1) was dropped at the 7th day
It is considered as below and passes through, other be considered as does not pass through.
5. experimental result
In inoculation 0,7,14, sampling detection in 2l and 28 day, experimental example 1~5 and the antibacterial milk sample of washing one's face of comparative example 1~6
Antibacterial sterilizing test result is shown in Table two.
Table two
From table two, the fungistatic effect of embodiment 1~5 is higher than comparative example 1~5, and the fungistatic effect of embodiment 1 is best；
Comparative example 5 without bacteriostatic activity, is understood in antibacterial mildy wash of the invention, locust tree with other embodiment and comparative example contrast substantially
Flower extract, sea-buckthorn seed extract, thyme essential oil are principle active component；Comparative example 1 is differed only in not with embodiment 1
Locust tree flower extract is added, as a result composition compatibility changes completely, and fungistatic effect is very poor, loses synergistic function；Comparative example 2
Sea-buckthorn seed extract is not added with differing only in for embodiment 1, as a result composition compatibility changes completely, and fungistatic effect is very poor,
Synergistic function is lost, comparative example 3 similarly, is contrasted from comparative example 1~3 with embodiment 1, in antibacterial mildy wash of the invention
Locust tree flower extract, sea-buckthorn seed extract, thyme essential oil Synergistic, there is remarkable result in terms of inhibiting bacteria and diminishing inflammation.
Inhibiting bacteria and diminishing inflammation efficacy validation
Experiment purpose：Disappeared by the antibacterial of antibacterial mildy wash obtained in comparative analysis the various embodiments described above and comparative example
Scorching effect.
Experimental subjects：The 550 26-35 Sui volunteer with whelk, volunteer's facial area has papule, redness, skin
Greasy, pore is thick, inflammatory reaction is obvious, the warts symptom such as continuous repeatedly.
Selection standard:Glucocorticoid, dimension A classes medicine, antibiotic etc. are taken in clinical observation the last fortnight, and in the observation period
Between without using said medicine；No drinking during observation, excessively pungent stimulation group food is not eaten.
Experimental method：550 people are randomly divided into 11 groups, every group of 50 people correspond to embodiment 1~5 respectively, comparative example 1~5,
Control group, control group is the outstanding commercially available antibacterial mildy wash of fungistatic effect.Patient daily sooner or later by Irrigation it is clean after will carry
The appropriate mildy wash supplied is evenly coated on the face and then cleaned up, and continuing 30d must not be interrupted.
Inhibiting bacteria and diminishing inflammation：Base more all disappears for volunteer's rear inflammatory fash on probation, pigmentation is only stayed, without new fash；It is aobvious
Imitate as inflammatory deflorescence more than 70%, new fash is less than 5；It is effectively the new fash of more than inflammatory deflorescence 30%-60%
It is few 10；It is invalid for inflammatory deflorescence less than 29% or without significant change, or even aggravate.
Experimental result see the table below three
Table three
The inhibiting bacteria and diminishing inflammation of the antibacterial mildy wash of the visible embodiment 1~5 of table three averagely cure rate and effective efficiency are 37.2% He
97.6% far above comparative example 1~5 and the cure rate and effective percentage of control group, it is seen that antibacterial mildy wash of the invention is in inhibiting bacteria and diminishing inflammation
Upper effect is notable；Comparative example 1 is not added with locust tree flower extract with differing only in for embodiment 1, and as a result composition compatibility is complete
Change, fungistatic effect is very poor, loses synergistic function；The differing only in of comparative example 2 and embodiment 1 is not added with seabuckthorn seeds and carried
Take thing, as a result composition compatibility changes completely, and fungistatic effect is very poor, lose synergistic function, comparative example 3 similarly, by contrasting
Example 1~3 contrasts visible with embodiment 1, locust tree flower extract, sea-buckthorn seed extract, thyme essence in antibacterial mildy wash of the invention
Oily Synergistic, there is remarkable result in terms of inhibiting bacteria and diminishing inflammation.
Upper embodiment only illustrates embodiment of the present invention, does not have any formal limitation to the present invention；It is any
Professional and technical personnel is engaged in, all has the ability to make some changes using the technology contents disclosed or modifies, become as equivalent
The equivalent embodiment of change, according to the technology of the present invention essence, simply modification, equivalent variations and modification is carried out to the present invention, is belonged to
In the range of technical solution of the present invention.
Claims (10)
1. a kind of antibacterial mildy wash, it is characterised in that the mildy wash mainly includes 0.2-3 parts of locust tree flower extract, seabuckthorn seeds
0.1-3 parts of extract, 0.01-1 parts of thyme essential oil.
2. a kind of antibacterial mildy wash according to claim 1, it is characterised in that the mildy wash is mainly carried including Pagoda Flower
Take 0.5-2.5 parts of thing, 1.1-2.8 parts of sea-buckthorn seed extract, 0.1-0.5 parts of thyme essential oil.
3. a kind of antibacterial mildy wash according to claim 1 or 2, it is characterised in that the locust tree flower extract and seabuckthorn seeds
Extract is prepared by the following method：Pagoda Flower, seabuckthorn seeds are mixed and Tumblied Dry after chopping under the conditions of 40-60 DEG C；Will
The material body of above-mentioned drying is added in 60%-80% ethanol, uses frequency for 20kHZ ultrasonication 3-5 minutes, then return
Stream extraction 5-12h, filter off residue, will under the conditions of filtrate 6000r/min-8000r/min centrifuge 15-30min obtain the Pagoda Flower,
Sea-buckthorn seed extract mixed liquor.
4. a kind of antibacterial mildy wash, it is characterised in that the mildy wash also includes following component：
0.5-2 parts of surfactant
1-3 parts of emulsifying agent
0.05-0.3 parts of thickener
0.01-0.5 parts of preservative
5-9 parts of emollient
15-40 parts of glycerine
0.02-0.3 parts of potassium hydroxide
1-3 parts of stearic acid.
5. a kind of antibacterial mildy wash according to claim 4, it is characterised in that the surfactant is sulfuric acid laurate
At least one of sodium, alkyl sulfate, lauroyl ether sodium sulfate, lauryl sodium sulfate.
6. a kind of antibacterial mildy wash according to claim 4, it is characterised in that the emulsifying agent is myristic acid, methyl
At least one of glucose sesquistearate, PEG-20 methyl sesquistearates.
7. a kind of antibacterial mildy wash according to claim 4, it is characterised in that the thickener be carbomer, xanthans,
At least one of hydroxyethyl cellulose, sodium carboxymethylcellulose.
8. a kind of antibacterial mildy wash according to claim 4, it is characterised in that the preservative is Phenoxyethanol, benzene first
At least one of sour sodium, methyl hydroxybenzoate, Nipasol.
9. a kind of antibacterial mildy wash according to claim 4, it is characterised in that the emollient is saualane, spermaceti is hard
Lipidol, dimethyl silicone polymer, Butyrospermum parkii fruit fat, hydrogenated jojoba oil, polydimethyl siloxanes/polydimethy siloxanes alcohol
At least one of.
10. a kind of method for preparing the antibacterial mildy wash as described in claim any one of 1-9, it is characterised in that the preparation side
Method comprises the following steps：By in emulsifying agent, emollient, surfactant input oil phase pot, 70-85 DEG C is heated to, all groups are waited
Divide after dissolving and be incubated, A phases are made；Glycerine, stearic acid, thickener and deionized water are put into aqueous phase pot successively, 70- is heated to
85 DEG C, insulation 15-30min makes it fully dissolve, and B phases are made；A phases, B phases are pumped into emulsification pot successively, homogeneous 5-
15min, stir speed (S.S.) is 2000-4000r/min, then insulated and stirred 15-45min, and stir speed (S.S.) is 30-50r/min；Cooling
To 40-45 DEG C, potassium hydroxide is added, is stirred；Add locust tree flower extract, sea-buckthorn seed extract, thyme essential oil, anti-corrosion
Agent, stirs, and obtains the antibacterial mildy wash.
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|---|---|---|---|
| CN201710192429.9A CN106974857A (en) | 2017-03-28 | 2017-03-28 | A kind of antibacterial mildy wash |
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| Application Number | Priority Date | Filing Date | Title |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014069A (en) * | 2018-02-01 | 2018-05-11 | 广州鹰远生物科技有限公司 | A kind of facial cleanser containing Flos persicae extract |
| CN113398057A (en) * | 2020-12-22 | 2021-09-17 | 重庆中佳信健康管理有限公司 | Bacteriostatic agent and preparation method thereof |
-
2017
- 2017-03-28 CN CN201710192429.9A patent/CN106974857A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014069A (en) * | 2018-02-01 | 2018-05-11 | 广州鹰远生物科技有限公司 | A kind of facial cleanser containing Flos persicae extract |
| CN113398057A (en) * | 2020-12-22 | 2021-09-17 | 重庆中佳信健康管理有限公司 | Bacteriostatic agent and preparation method thereof |
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