CN109846756A - A kind of moisturizing emulsion of the extract containing beeswax and preparation method thereof - Google Patents

A kind of moisturizing emulsion of the extract containing beeswax and preparation method thereof Download PDF

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Publication number
CN109846756A
CN109846756A CN201910102705.7A CN201910102705A CN109846756A CN 109846756 A CN109846756 A CN 109846756A CN 201910102705 A CN201910102705 A CN 201910102705A CN 109846756 A CN109846756 A CN 109846756A
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parts
beeswax
component
heating
extract
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CN201910102705.7A
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Chinese (zh)
Inventor
吴明珠
罗煚亓
龙星昕
谢燕清
段益琴
周永福
李应
罗羽辰
赵辉
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Chongqing Industry Polytechnic College
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Chongqing Industry Polytechnic College
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Priority to CN201910102705.7A priority Critical patent/CN109846756A/en
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Abstract

The present invention discloses a kind of moisturizing emulsion and preparation method thereof of extract containing beeswax, it is calculated as mass fraction by 0.3-2.0 parts of beeswax extracts, 0.1-2.0 parts of saualanes, 1.0-5.0 parts of reed fragrant plant glue, 1.0-3.0 parts of stearic acid, 0.5-3.0 parts of octyldodecanols, 1.0-4.0 part hexadecanol polyoxyethylene ether, 0.1-0.4 parts of methyl formates, 0.05-0.2 parts of methylcellulose, 0.5-2.0 parts of glycerol, 0.3-1.0 parts of cellulose E, 0.5-2.0 portions of trehaloses, 0.05-0.2 parts of Sodium Hyaluronates, 0.05-0.2 parts of card waves 940, 0.1-0.2 parts of essence and 50-100 parts of deionized water compositions, the present invention is added to animal fat saualane, insect excretions beeswax Can and transparent ester acid sodium improve water lock, the nourishing, whitening acne-removing of lotion, subcutaneous tissue situation can be improved, make skin rich in elastic force, promote skin soft and moist.Vitamin E anti-inflammatory, antibacterial antiallergy in lotion, oxidation resistant effect can promote skin metabolism, wrinkle resistant crease-resistant, nonirritant.

Description

A kind of moisturizing emulsion of the extract containing beeswax and preparation method thereof
Technical field
The present invention relates to beauty and skin care technical fields, and in particular to a kind of moisturizing emulsion of the extract containing beeswax and its preparation Method.
Background technique
Water shortage is the basic reason of skin aging.When air themperature reduces, keratoderma cannot be adjusted enough in time Moisturizing factor, the decline of grease gland liveness, grease, moisture decline on the face, skin will appear tight phenomenon and microgroove.Moisturizing is By using skin care item, moisturizes the skin and prevent skin evaporation, improves microcirculation, enhance the process of skin wettability.Skin is protected Wet there are two types of methods, and one is outer skin care item of the painting containing moisturizing factor;Be for second take in professional food in nutrition from Body synthesizes hyaluronic acid, plays the effect of whole body moisturizing.But optimal moisturizing is first moisturizing moisturizing again, realizes that skin and moisturizing produce The good interaction of product.Since both hands are chronically exposed to outside, it is easy by shadows such as seasonal variations, environmental pollution, acid and alkali substances It rings, causes the skin problems such as the intensification of coarse, loose, skin lines and fibr tissue aging, the fracture of both hands skin compared with other portions Position it is more prominent, at present the general hand lotion moisture-keeping function time is shorter, percutaneous absorption is poor, additive not environmentally, cannot reach Maintenance skin, pure natural oxidation resistant effect are moistened for a long time.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of moisturizing emulsion and preparation method thereof of extract containing beeswax.
Technical solution is as follows: a kind of moisturizing emulsion of the extract containing beeswax, key is composed of the following components: with weight Measure part meter, by 0.3-2.0 parts of beeswax extracts, 0.1-2.0 parts of saualanes, 1.0-5.0 parts of reed fragrant plant glue, 1.0-3.0 parts of stearic acid, 0.5-3.0 parts of octyldodecanols, 1.0-4.0 parts of hexadecanol polyoxyethylene ether, 0.1-0.4 parts of methyl formates, 0.05-0.2 parts Methylcellulose, 0.5-2.0 part glycerol, E, 0.5-2.0 portions of trehaloses of 0.3-1.0 parts of celluloses, 0.05-0.2 parts of hyaluronic acids Sodium, 0.05-0.2 parts of card waves 940,0.1-0.2 parts of essence and 50-100 parts of deionized water compositions.
A kind of preparation method of the moisturizing emulsion of the extract containing beeswax, key are to sequentially include the following steps:
S1: beeswax extract is prepared;
S2: weighing reed fragrant plant peptization solution in deionized water by mass fraction, and stirring fusion obtains component A;
S3: beeswax extract, stearic acid, octyldodecanol, saualane and hexadecanol polyoxy second are weighed by mass fraction Alkene ether, heating for dissolving obtain B component;
S4: weighing methyl formate, methylcellulose, glycerol, cellulose E, trehalose by mass fraction and be added in component A, Heating stirring makes it dissolve to obtain component C;
S5: gained B component is added in component C and obtains milky D component;
S6: continuing after heating and stirring D component 20-30min, by mass fraction be added Sodium Hyaluronate after its dissolution after again Card wave 940 is added, stops being added after card wave 940 all dissolution, essence is added and continues stirring to essence and dissolves.
Above-mentioned technical proposal using beeswax extract, saualane and vitamin E as additive, with reed fragrant plant glue, transparent ester acid sodium, Glycerol is the lotion of moisturizer.The main component of beeswax is esters, fatty acid and carbohydrate, still containing a small amount of moisture, fatty alcohol, wave Hair oil, pigment, vitamin, minerals etc..The antimicrobial component being rich in beeswax can inhibit and kill the bacterium of skin surface and energy Promote Skin Cell regeneration;A variety of inoxidizability ingredients that beeswax contains can effectively clear free radical extra in vivo;Beeswax contains The ingredients such as some vitamin, aromatic substance, it is soft and moist to be able to maintain skin.In addition, beeswax extract is also easy to incorporate oil-in-water body In system.Beeswax extract not only increases emulsion emulsifiers effect, and lotion is also made to have good moisturizing, sterilization, myogenic, anti-oxidant The effects of.Sodium Hyaluronate has stable moisture-keeping function, while can remove epidermis and be irradiated the active oxygen generated by ultraviolet light certainly By base, the skin corium of skin also may penetrate into, keep the moisture in skin, promote the conjunction of dermal collagen and elastomer At playing beauty and face-nursing function to prevent skin aging.Saualane is closest to a kind of lipid of human sebaceous, has Stronger affinity, while can combine together with the sebum film of human body, inhibit the peroxidating of skin lipid, skin can be infiltrated through, And promote the metabolism of skin base cell, to delay skin aging.
The method that beeswax extract is prepared in S1 is as follows:
(1) it is fitted into gauze bag after crushing 1kg honeycomb, 700mL deionized water is added, is heated to boiling, it then will dress There is the gauze bag of honeycomb to continue heating into the water until boiling again;
(2) gauze bag is taken out, squeezes the beeswax that gauze bag keeps it internal and flow into boiling water, takes out bee after boiling water is cooling Wax;
(3) boiling in beaker is boiled again, then again continues gauze bag into the water to heat up to boiling again, It takes out gauze bag and squeezes the honeycomb that keeps it internal again all is squeezed out and enter in boiling water, by beeswax therein after boiling water cooling It takes out;
(4) beeswax obtained twice is dissolved to mixing at 65-85 DEG C, obtains beeswax extract after its cooling.
Heating for dissolving temperature in S3 is 65-90 DEG C.
Heating stirring temperature in S4 is 65-90 DEG C.
Antipyretic solution temperature in S3 is 85 DEG C, and the heating stirring temperature in S4 is 85 DEG C, and the mixing time in S6 is 25min。
The utility model has the advantages that using beeswax and its emulsion in the present invention to have antibacterial and antisepsis, while beeswax is easy to melt Enter in oil-in-water system, lotion is made to have the function of fabulous emulsification and moisturizing, can also be formed in skin surface a kind of non- It the protective film of occlusive and compatible with other compositions in lotion can will not cause allergic reaction.Sodium Hyaluronate has stable guarantor Wet effect, while the active oxygen radical that epidermis is generated by ultraviolet light irradiation can be removed, it also may penetrate into the skin corium of skin, protect The moisture in skin is held, the synthesis of dermal collagen and elastomer is promoted, to prevent skin aging, play beauty and support Face effect.Saualane is a kind of lipid of closest human sebaceous, has stronger affinity, while can be with the sebum of human body Film combines together, inhibits the peroxidating of skin lipid, can infiltrate through skin, and promotes the metabolism of skin base cell, right Delay skin aging.In conclusion this product has fabulous moisturizing and activates Elastic fibers, its hardening, skin is prevented Dry and cracked, decortication effect, and skin can be infiltrated through to promote the metabolism of skin base cell, delaying skin declines Always, so that skin is stayed pale moist, reduces wrinkle.
Specific embodiment
Below with reference to embodiment, the invention will be further described.
Embodiment 1, a kind of moisturizing emulsion of the extract containing beeswax are by mass, composed of the following components:
Beeswax extract 0.9g, saualane 1g, reed fragrant plant glue 2g, stearic acid 1.1g, octyldodecanol 1g, hexadecanol polyoxy Vinethene 1g, methyl formate 0.2g, methylcellulose 0.1g, glycerol 0.7g, vitamin E 0.8g, trehalose 0.7g, hyalomitome Sour sodium 0.05g, card wave 940 0.06g, essence 0.1g, deionized water 50g.
Preparation method is as follows:
S1: preparing beeswax extract, and process is as follows:
(1) it is fitted into gauze bag after crushing 1kg honeycomb, 700mL deionized water is added, is heated to boiling, it then will dress There is the gauze bag of honeycomb to continue heating into the water until boiling again;
(2) gauze bag is taken out, squeezes the beeswax that gauze bag keeps it internal and flow into boiling water, takes out bee after boiling water is cooling Wax;
(3) boiling in beaker is boiled again, then again continues gauze bag into the water to heat up to boiling again, It takes out gauze bag and squeezes the honeycomb that keeps it internal again all is squeezed out and enter in boiling water, by beeswax therein after boiling water cooling It takes out;
(4) beeswax obtained twice is dissolved to mixing at 65 DEG C, obtains beeswax extract after its cooling;
S2: in deionized water by reed fragrant plant peptization solution, stirring fusion obtains component A;
S3: by beeswax extract, stearic acid, octyldodecanol, saualane and hexadecanol polyoxyethylene ether, 65 are heated to DEG C dissolution obtains B component;
S4: methyl formate, methylcellulose, glycerol, cellulose E, trehalose are added in component A, are heated to 65 DEG C simultaneously It stirs to dissolve to obtain component C;
S5: gained B component is added in component C and obtains milky D component;
S6: continuing at 65 DEG C after heating and stirring D component 25min, and Sodium Hyaluronate is added and adds after its dissolution Card wave 940 stops heating after card wave 940 all dissolution, and essence is added and continues stirring to essence and dissolves.
Embodiment 2, a kind of moisturizing emulsion of the extract containing beeswax are by mass, composed of the following components:
Beeswax extract 0.7g, saualane 1g, reed fragrant plant glue 2.5g, stearic acid 1.7g, octyldodecanol 0.5g, hexadecanol Polyoxyethylene ether 1.5g, methyl formate 0.2g, methylcellulose 0.17g, glycerol 1g, vitamin E 0.5g, trehalose 0.6g, thoroughly Bright matter acid sodium 0.1g, card wave 940 0.05g, essence 0.1g, deionized water 70g.
Preparation method is as follows:
S1: preparing beeswax extract, and process is as follows:
(1) it is fitted into gauze bag after crushing 1kg honeycomb, 700mL deionized water is added, is heated to boiling, it then will dress There is the gauze bag of honeycomb to continue heating into the water until boiling again;
(2) gauze bag is taken out, squeezes the beeswax that gauze bag keeps it internal and flow into boiling water, takes out bee after boiling water is cooling Wax;
(3) boiling in beaker is boiled again, then again continues gauze bag into the water to heat up to boiling again, It takes out gauze bag and squeezes the honeycomb that keeps it internal again all is squeezed out and enter in boiling water, by beeswax therein after boiling water cooling It takes out;
(4) beeswax obtained twice is dissolved to mixing at 85 DEG C, obtains beeswax extract after its cooling;
S2: in deionized water by reed fragrant plant peptization solution, stirring fusion obtains component A;
S3: by beeswax extract, stearic acid, octyldodecanol, saualane and hexadecanol polyoxyethylene ether, 85 are heated to DEG C dissolution obtains B component;
S4: methyl formate, methylcellulose, glycerol, cellulose E, trehalose are added in component A, are heated to 85 DEG C simultaneously It stirs to dissolve to obtain component C;
S5: gained B component is added in component C and obtains milky D component;
S6: continuing at 85 DEG C after heating and stirring D component 25min, and Sodium Hyaluronate is added and adds after its dissolution Card wave 940 stops heating after card wave 940 all dissolution, and essence is added and continues stirring to essence and dissolves.
Embodiment 3, a kind of moisturizing emulsion of the extract containing beeswax are by mass, composed of the following components:
Beeswax extract 0.3g, saualane 0.1g, reed fragrant plant glue 1.0g, stearic acid 1.0g, octyldodecanol 3.0g, 16 Alcohol polyoxyethylene ether 4.0g, methyl formate 0.1g, methylcellulose 0.05g, glycerol 0.5g, vitamin E 0.3g, trehalose 0.5g, Sodium Hyaluronate 0.2g, card wave 940 0.05g, essence 0.2g, deionized water 100g.
Preparation method is as follows:
S1: preparing beeswax extract, and process is as follows:
(1) it is fitted into gauze bag after crushing 1kg honeycomb, 700mL deionized water is added, is heated to boiling, it then will dress There is the gauze bag of honeycomb to continue heating into the water until boiling again;
(2) gauze bag is taken out, squeezes the beeswax that gauze bag keeps it internal and flow into boiling water, takes out bee after boiling water is cooling Wax;
(3) boiling in beaker is boiled again, then again continues gauze bag into the water to heat up to boiling again, It takes out gauze bag and squeezes the honeycomb that keeps it internal again all is squeezed out and enter in boiling water, by beeswax therein after boiling water cooling It takes out;
(4) beeswax obtained twice is dissolved to mixing at 75 DEG C, obtains beeswax extract after its cooling;
S2: in deionized water by reed fragrant plant peptization solution, stirring fusion obtains component A;
S3: by beeswax extract, stearic acid, octyldodecanol, saualane and hexadecanol polyoxyethylene ether, 90 are heated to DEG C dissolution obtains B component;
S4: methyl formate, methylcellulose, glycerol, cellulose E, trehalose are added in component A, are heated to 90 DEG C simultaneously It stirs to dissolve to obtain component C;
S5: gained B component is added in component C and obtains milky D component;
S6: continuing at 90 DEG C after heating and stirring D component 30min, and Sodium Hyaluronate is added and adds after its dissolution Card wave 940 stops heating after card wave 940 all dissolution, and essence is added and continues stirring to essence and dissolves.
Embodiment 4, a kind of moisturizing emulsion of the extract containing beeswax are by mass, composed of the following components:
Beeswax extract 2.0g, saualane 2.0g, reed fragrant plant glue 5.0g, stearic acid 3.0g, octyldodecanol 1.5g, 16 Alcohol polyoxyethylene ether 2.0g, methyl formate 0.4g, methylcellulose 0.2g, glycerol 2.0g, vitamin e1 .0g, trehalose 2.0g, Sodium Hyaluronate 0.1g, card wave 940 0.2g, essence 0.1g, deionized water 80g.
Preparation side of the preparation method in addition to stirring D component 20min difference in step S6, in other steps and embodiment 3 Method is identical, no longer repeats one by one.
The product of Example 1-4 preparation carries out emulsification system respectively and stablizes experiment, while buying commercially available product and opposing Than test, test method and result are as follows:
Lotion products storage obtained in embodiment 1-4 for 24 hours after, take 4 each 4mL of finished product in 4 small-sized centrifuge tubes of 1mL In, after being placed in electro-heating standing-temperature cultivator (38 ± 1) DEG C heat preservation 1h, move into centrifuge.Setting centrifuge speed is 2000r/ Lotion is observed after min, 30min and lamination occurs, and no lamination occurs.The same test method in commercial product occurs Lamination.It can be seen that its emulsifying effectiveness is more preferable using moisturizing emulsion prepared by the present invention, it is unlikely to deteriorate.
The product of Example 1-2 preparation carries out moisturizing test respectively, while buying commercial product and comparing test, surveys Method for testing and result are as follows:
Selecting the age is male totally 16 of 18-22 years old, and be randomly divided into 4 groups: example 1 group (is prepared using embodiment 1 Lotion), 2 groups of embodiment (lotion prepared using embodiment 2), comparative example group (using certain commercially available brand lotion), blank pair According to group (not using any lotion).Every group of 4 people, subject's right hand are labeled as tested area, and subject cleans after hand using correspondence The lotion of group is tested by testing staff using moisture content of skin respectively after using this group of lotion 0h, 0.5h, 1h, 1.5h, 2h The hand skin water content of the different zones of instrument test subject 5 times, test result takes test data average value, as a result such as table 1 It is shown.
1 moisturizing of table test
Spread product Humidity after 0h Humidity after 0.5h Humidity after 1h Humidity after 1.5h Humidity after 2h
Example 1 group 49% 41% 33% 35% 33%
2 groups of embodiment 54% 45% 43% 40% 38%
Comparative example group 46% 33% 33% 33% 31%
Blank control group 22% 21% 21% 21% 21%
As it can be seen from table 1 after smearing lotion two hours of commercially available certain brand, the average moisture content of tester's skin with The blank control group difference for not smearing lotion is not significant, and after having smeared products of the present invention, the skin water of testee Point content rises rapidly, and as the variation of time is higher than comparative example group and blank control group always, it can be seen that the present invention The moisturizing emulsion of offer has good moistening effect.
Finally, it should be noted that foregoing description is only the preferred embodiment of the present invention, the ordinary skill people of this field Member under the inspiration of the present invention, without prejudice to the purpose of the present invention and the claims, can make multiple similar tables Show, such transformation is fallen within the scope of protection of the present invention.

Claims (6)

1. a kind of moisturizing emulsion of extract containing beeswax, it is characterised in that composed of the following components: in parts by weight, by 0.3- 2.0 parts of beeswax extracts, 0.1-2.0 parts of saualanes, 1.0-5.0 parts of reed fragrant plant glue, 1.0-3.0 parts of stearic acid, 0.5-3.0 parts of octyls Dodecanol, 1.0-4.0 parts of hexadecanol polyoxyethylene ether, 0.1-0.4 parts of methyl formates, 0.05-0.2 parts of methylcellulose, 0.5-2.0 parts of glycerol, E, 0.5-2.0 portions of trehaloses of 0.3-1.0 parts of celluloses, 0.05-0.2 parts of Sodium Hyaluronates, 0.05-0.2 Part card wave 940,0.1-0.2 parts of essence and 50-100 parts of deionized waters compositions.
2. a kind of preparation method of the moisturizing emulsion of the extract according to claim 1 containing beeswax, it is characterised in that by with Lower step carries out:
S1: beeswax extract is prepared;
S2: weighing reed fragrant plant peptization solution in deionized water by mass fraction, and stirring fusion obtains component A;
S3: weighing beeswax extract, stearic acid, octyldodecanol, saualane and hexadecanol polyoxyethylene ether by mass fraction, Heating for dissolving obtains B component;
S4: weighing methyl formate, methylcellulose, glycerol, cellulose E, trehalose by mass fraction and be added in component A, heating It stirs to dissolve to obtain component C;
S5: gained B component is added in component C and obtains milky D component;
S6: continuing after heating and stirring D component 20-30min, and Sodium Hyaluronate is added by mass fraction.Add again after its dissolution Enter card wave 940, stop heating after card wave 940 all dissolution, essence is added and continues stirring to essence and dissolves.
3. a kind of preparation method of the moisturizing emulsion of extract containing beeswax according to claim 2, it is characterised in that: in S1 The method for preparing beeswax extract is as follows:
(1) it is fitted into gauze bag after crushing 1kg honeycomb, 700mL deionized water is added, is heated to boiling, then bee will be housed The gauze bag of nest continues heating until boiling again into the water;
(2) gauze bag is taken out, squeezes the beeswax that gauze bag keeps it internal and flow into boiling water, takes out beeswax after boiling water is cooling;
(3) boiling in beaker is boiled again, then gauze bag is continued into heating until boiling again again into the water, is taken out Gauze bag, which squeezes the honeycomb that keeps it internal again all is squeezed out, to be entered in boiling water, takes beeswax therein after boiling water is cooling Out;
(4) beeswax obtained twice is dissolved to mixing at 65-85 DEG C, obtains beeswax extract after its cooling.
4. a kind of preparation method of the moisturizing emulsion of extract containing beeswax according to claim 2 or 3, it is characterised in that: Heating for dissolving temperature in S3 is 65-90 DEG C.
5. a kind of preparation method of the moisturizing emulsion of extract containing beeswax according to claim 4, it is characterised in that: in S4 Heating stirring temperature be 65-90 DEG C.
6. a kind of preparation method of the moisturizing emulsion of extract containing beeswax according to claim 2, it is characterised in that: in S3 Heating for dissolving temperature be 85 DEG C, heating stirring temperature in S4 is 85 DEG C, and the mixing time in S6 is 25min.
CN201910102705.7A 2019-02-01 2019-02-01 A kind of moisturizing emulsion of the extract containing beeswax and preparation method thereof Pending CN109846756A (en)

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CN112795312A (en) * 2021-01-27 2021-05-14 徐嘉程 Preparation method of water-based nano material for woodware veneer
CN115518008A (en) * 2022-08-24 2022-12-27 芜湖职业技术学院 Grape skin pigment lip balm and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN112795312A (en) * 2021-01-27 2021-05-14 徐嘉程 Preparation method of water-based nano material for woodware veneer
CN115518008A (en) * 2022-08-24 2022-12-27 芜湖职业技术学院 Grape skin pigment lip balm and preparation method thereof

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