CN106366942A - Preparation method of fiber-containing liquid shoe polish - Google Patents
Preparation method of fiber-containing liquid shoe polish Download PDFInfo
- Publication number
- CN106366942A CN106366942A CN201610737243.2A CN201610737243A CN106366942A CN 106366942 A CN106366942 A CN 106366942A CN 201610737243 A CN201610737243 A CN 201610737243A CN 106366942 A CN106366942 A CN 106366942A
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- CN
- China
- Prior art keywords
- liquid
- fiber
- mass percent
- shoe polish
- preparation
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/08—Other polishing compositions based on wax
- C09G1/10—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin
- C09G1/12—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin mixtures of wax and silicon-containing polycondensates
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Treatment And Processing Of Natural Fur Or Leather (AREA)
Abstract
The invention discloses a preparation method of a fiber-containing liquid shoe polish. The preparation method comprises the steps that 1, a black dye is prepared into black liquid; 2, solid paraffin and beewax are mixed and added to the black liquid, stirring and heating are performed to achieve fusion, and colloidal liquid is obtained; 3, stearic acid and silicone oil are added to the colloidal liquid, and sticky mixed liquid is prepared, wherein the mass percent of the stearic acid in the mixed liquid is 0.2-0.3%; 4, natural fiber is put in water, ultrasonic treatment is performed, the ultrasonic treatment time is 1-2 hours, the ultrasonic treatment frequency is 50-70 KHz, heating is further performed while ultrasonic treatment, the heating temperature is 100-120 DEG C, the treated fiber with the length of 100-200 microns is obtained, drying is performed, then the treated fiber is added to the mixed liquid, and even stirring is performed. The prepared shoe polish has a good leather shoe cleaning effect.
Description
Technical field
The present invention relates to a kind of preparation method of the liquid shoe polish containing fiber.
Background technology
Shoe polish is to embrocate in the protective agent of leather shoes and leather surface and glazing agent, has waterproof, guard, strengthens leather surface
Gloss, cleaning, the effect of attractive in appearance and additive color complementary color, daily life consumption is very big.Textural classification pressed by shoe polish, has solvent-borne type plaster
Body, emulsion type ointment body and liquid type, first two is traditional product, and liquid shoe polish is domestic at present popular new product.Liquid
Body shoe polish have do not wipe from bright, easy to carry, save time the features such as, the features such as embrocate easy, deep liked by consumer.With regard to liquid
The main body of shoe polish, there are reports and launch, and its primary raw material is wax emulsion and the mixing of wax emulsion and synthetic resin
Thing etc..But existing shoe polish need to be improved to the clean effect of leather shoes.
Content of the invention
For above-mentioned technical problem, the present invention has designed and developed a kind of good shoe polish of cleaning effect.
Present invention offer technical scheme below:
A kind of preparation method of the liquid shoe polish containing fiber, comprising:
Black dyes is modulated into black liquor by step (1)；
Step (2) adds hard paraffin and Cera Flava mixing to black liquor, is stirred and heated to merge, obtains glue
Liquid, wherein, mass percent in black liquor for the hard paraffin is 4～5%, percent mass in black liquor for the Cera Flava
Than for 4～5%；
Step (3) adds stearic acid and silicone oil in colloidal liquid, makes thick mixing liquid, and wherein, stearic acid exists
Mass percent in mixing liquid is 0.2～0.3%, and mass percent in mixing liquid for the silicone oil is 0.1～0.2%；
Natural fiber is placed in water by step (4), carries out supersound process, the time of supersound process is 1～2h, supersound process
Frequency be 50～70khz, also heated while supersound process, heating-up temperature be 100～120 DEG C, obtaining length is
Fiber after 100～120 μm of process, is dried, and afterwards the fiber after processing is added the fiber to mixing liquid, after process
Mass percent in mixing liquid is 0.7～0.9%, stirs.
Preferably, in the described preparation method containing the liquid shoe polish of fiber, in described step (2), hard paraffin
Mass percent in black liquor is 4.5%, and mass percent in black liquor for the Cera Flava is 4.5%.
Preferably, in the described preparation method containing the liquid shoe polish of fiber, in described step (3), stearic acid exists
Mass percent in mixing liquid is 0.2%, and mass percent in mixing liquid for the silicone oil is 0.1%.
Preferably, in the described preparation method containing the liquid shoe polish of fiber, in described step (4), after process
The length of fiber is 100～110 μm.
The preparation-obtained shoe polish of the present invention is good to the clean effect of leather shoes.
Specific embodiment
The present invention is described in further detail below, with make those skilled in the art with reference to specification word being capable of evidence
To implement.
The present invention provides a kind of preparation method of the liquid shoe polish containing fiber, comprising:
Black dyes is modulated into black liquor by step (1)；
Step (2) adds hard paraffin and Cera Flava mixing to black liquor, is stirred and heated to merge, obtains glue
Liquid, wherein, mass percent in black liquor for the hard paraffin is 4～5%, percent mass in black liquor for the Cera Flava
Than for 4～5%；
Step (3) adds stearic acid and silicone oil in colloidal liquid, makes thick mixing liquid, and wherein, stearic acid exists
Mass percent in mixing liquid is 0.2～0.3%, and mass percent in mixing liquid for the silicone oil is 0.1～0.2%；
Natural fiber is placed in water by step (4), carries out supersound process, the time of supersound process is 1～2h, supersound process
Frequency be 50～70khz, also heated while supersound process, heating-up temperature be 100～120 DEG C, obtaining length is
Fiber after 100～200 μm of process, is dried, and afterwards the fiber after processing is added the fiber to mixing liquid, after process
Mass percent in mixing liquid is 0.7～0.9%, stirs.
The present invention with the addition of in shoe polish has the fiber that length is 100～200 μm.When wiping leather shoes using shoe polish, fine
Dimension composition plays the effect of wiping to the surface of leather shoes, thus improving the clean effect to leather shoes.Chi due to fibre composition
Leather shoes will not be damaged by very little only micron order.
In the present invention, the processing method of natural fiber is, carries out supersound process to natural fiber, and by accurately setting
The time of supersound process and the frequency of supersound process, come length and the diameter of the fiber after control process.Based on aforesaid operations bar
Part, uniformly, the length difference between fiber after process is away from ± 5 μm for the distribution of lengths of the fiber after process.And supersound process
The outer surface that the fiber after process can be made becomes coarse, makes the fiber after process relatively stable and is evenly dispersed in shoe polish
In bulk composition.
The present invention is also heated while supersound process, and heating-up temperature is 100～120 DEG C, through surpassing for a long time
Sonication and heating, can make the fiber after process form the form of curling, rather than rectilinear form.So contribute to promoting
So that the fiber after process is more stably dispersed in the bulk composition of shoe polish, and be difficult to settle from the bulk composition of shoe polish or divide
From.
Preferably, in the described preparation method containing the liquid shoe polish of fiber, in described step (2), hard paraffin
Mass percent in black liquor is 4.5%, and mass percent in black liquor for the Cera Flava is 4.5%.
Preferably, in the described preparation method containing the liquid shoe polish of fiber, in described step (3), stearic acid exists
Mass percent in mixing liquid is 0.2%, and mass percent in mixing liquid for the silicone oil is 0.1%.
Preferably, in the described preparation method containing the liquid shoe polish of fiber, in described step (4), after process
The length of fiber is 100～110 μm.
Although embodiment of the present invention is disclosed as above, it is not restricted to listed in description and embodiment
With, it can be applied to various suitable the field of the invention completely, for those skilled in the art, can be easily
Realize other modification, therefore under the general concept being limited without departing substantially from claim and equivalency range, the present invention does not limit
In specific details.
Claims (4)
1. a kind of preparation method of the liquid shoe polish containing fiber is it is characterised in that include:
Black dyes is modulated into black liquor by step (1)；
Step (2) adds hard paraffin and Cera Flava mixing to black liquor, is stirred and heated to merge, obtains Colloidal fluid
Body, wherein, mass percent in black liquor for the hard paraffin is 4～5%, mass percent in black liquor for the Cera Flava
For 4～5%；
Step (3) adds stearic acid and silicone oil in colloidal liquid, makes thick mixing liquid, and wherein, stearic acid is in mixing
Mass percent in liquid is 0.2～0.3%, and mass percent in mixing liquid for the silicone oil is 0.1～0.2%；
Natural fiber is placed in water by step (4), carries out supersound process, the time of supersound process is 1～2h, the frequency of supersound process
Rate be 50～70khz, also heated while supersound process, heating-up temperature be 100～120 DEG C, obtain length be 100～
Fiber after 120 μm of process, is dried, and adds the fiber after processing to mixing liquid afterwards, the fiber after process is mixed
The mass percent closed in liquid is 0.7～0.9%, stirs.
2. the preparation method of the liquid shoe polish containing fiber as claimed in claim 1 is it is characterised in that in described step (2),
Mass percent in black liquor for the hard paraffin is 4.5%, and mass percent in black liquor for the Cera Flava is 4.5%.
3. the preparation method of the liquid shoe polish containing fiber as claimed in claim 1 is it is characterised in that in described step (3),
Mass percent in mixing liquid for the stearic acid is 0.2%, and mass percent in mixing liquid for the silicone oil is 0.1%.
4. the preparation method of the liquid shoe polish containing fiber as claimed in claim 1 is it is characterised in that in described step (4),
The length of the fiber after process is 100～110 μm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610737243.2A CN106366942A (en) | 2016-08-26 | 2016-08-26 | Preparation method of fiber-containing liquid shoe polish |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610737243.2A CN106366942A (en) | 2016-08-26 | 2016-08-26 | Preparation method of fiber-containing liquid shoe polish |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106366942A true CN106366942A (en) | 2017-02-01 |
Family
ID=57903025
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610737243.2A Pending CN106366942A (en) | 2016-08-26 | 2016-08-26 | Preparation method of fiber-containing liquid shoe polish |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106366942A (en) |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5614005A (en) * | 1996-04-01 | 1997-03-25 | Leung; Ricky | Water resistant shoe polish |
| CN102464948A (en) * | 2010-11-01 | 2012-05-23 | 罗朝雯 | Blacking and its preparation method |
| CN102993980A (en) * | 2012-11-21 | 2013-03-27 | 吴江市得可利纺织品有限公司 | Brightening agent for leather and preparation method for same |
| CN103275621A (en) * | 2013-05-21 | 2013-09-04 | 苏州富通高新材料科技股份有限公司 | Chinese herbal medicine inset-prevention and antibiotic floor wax and preparation method thereof |
| CN103992745A (en) * | 2014-05-16 | 2014-08-20 | 临沂大学 | Liquid shoe polish prepared by ginkgo leaf ketone extracted paste residual wastes and preparation method thereof |
| CN104356952A (en) * | 2014-10-19 | 2015-02-18 | 青岛拓联信息技术有限公司 | Efficient decontaminating and cleaning shoe polish |
| CN104419546A (en) * | 2013-08-28 | 2015-03-18 | 青岛医防消毒专业技术中心 | Leather product cleaning agent |
| CN104479562A (en) * | 2014-12-23 | 2015-04-01 | 艾金富 | Leather brightener |
| CN104592899A (en) * | 2015-01-20 | 2015-05-06 | 安徽斯瑞尔阀门有限公司 | Special composite polishing powder for valve flange and preparation method of composite polishing powder |
| CN105038608A (en) * | 2015-06-18 | 2015-11-11 | 上海飞尔实业有限公司 | Glass polishing agent |
-
2016
- 2016-08-26 CN CN201610737243.2A patent/CN106366942A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5614005A (en) * | 1996-04-01 | 1997-03-25 | Leung; Ricky | Water resistant shoe polish |
| CN102464948A (en) * | 2010-11-01 | 2012-05-23 | 罗朝雯 | Blacking and its preparation method |
| CN102993980A (en) * | 2012-11-21 | 2013-03-27 | 吴江市得可利纺织品有限公司 | Brightening agent for leather and preparation method for same |
| CN103275621A (en) * | 2013-05-21 | 2013-09-04 | 苏州富通高新材料科技股份有限公司 | Chinese herbal medicine inset-prevention and antibiotic floor wax and preparation method thereof |
| CN104419546A (en) * | 2013-08-28 | 2015-03-18 | 青岛医防消毒专业技术中心 | Leather product cleaning agent |
| CN103992745A (en) * | 2014-05-16 | 2014-08-20 | 临沂大学 | Liquid shoe polish prepared by ginkgo leaf ketone extracted paste residual wastes and preparation method thereof |
| CN104356952A (en) * | 2014-10-19 | 2015-02-18 | 青岛拓联信息技术有限公司 | Efficient decontaminating and cleaning shoe polish |
| CN104479562A (en) * | 2014-12-23 | 2015-04-01 | 艾金富 | Leather brightener |
| CN104592899A (en) * | 2015-01-20 | 2015-05-06 | 安徽斯瑞尔阀门有限公司 | Special composite polishing powder for valve flange and preparation method of composite polishing powder |
| CN105038608A (en) * | 2015-06-18 | 2015-11-11 | 上海飞尔实业有限公司 | Glass polishing agent |
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Application publication date: 20170201 |
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