CN106554719B - A kind of oil colour - Google Patents

A kind of oil colour Download PDF

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Publication number
CN106554719B
CN106554719B CN201610968681.XA CN201610968681A CN106554719B CN 106554719 B CN106554719 B CN 106554719B CN 201610968681 A CN201610968681 A CN 201610968681A CN 106554719 B CN106554719 B CN 106554719B
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China
Prior art keywords
oil
added
colour
cera alba
monoglyceride
Prior art date
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CN201610968681.XA
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Chinese (zh)
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CN106554719A (en
Inventor
赵松松
洪梅
颜秀花
吴永泽
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SHUYANG PHOENIX PAINT COLOR CO Ltd
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SHUYANG PHOENIX PAINT COLOR CO Ltd
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Priority to CN201610968681.XA priority Critical patent/CN106554719B/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/005—Drying oils
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/06—Waxes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/06—Artists' paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group

Abstract

The invention discloses a kind of oil colours, by weight percentage include following component, linseed oil 22.85 ~ 52.9, cera alba 1-3%, monoglyceride 1-3%, desiccant 0.1-0.2%, barium sulfate 15-50%, pigment powder 5-30%.The non-stimulated smell of the pigment, it is safe and non-toxic, human body can be directly contacted, good water solubility is possessed, thus have the characteristics that easy cleaning, it is green product.It solves existing oil colour and glues the technical problems such as pen, oil powder separation, drawing quality can be improved, save material and reduce environmental pollution.

Description

A kind of oil colour
Technical field
The present invention relates to pigment, in particular to a kind of oil colour.
Background technique
As the increasingly upgrading that artist requires painting material, especially oil colour are that artist passes on paint The painting material most doted on, unstable quality caused by vegetable oil and paint filler are easily separated in traditional oil painting pigment are traditional The oil colour viscosity of auxiliary rheological agents (rilanit special, beeswax, stearic acid etc.) production is big, easily produces in artist's painting process Raw viscous stagnant phenomenon of pen.
Summary of the invention
In order to overcome drawbacks described above, the present invention provides a kind of oil colour, modest viscosity, painting effect is good.
The invention is realized by the following technical scheme:
A kind of oil colour includes following component by weight percentage,
Linseed oil 22.85 ~ 52.9%
Cera alba 1-3%
Monoglyceride 1-3%
Desiccant 0.1-0.2%
Barium sulfate 15-50%
Pigment powder 5-30%.
A kind of preparation method of oil colour, includes the following steps:
(1) it takes linseed oil 2.8 ~ 2.9% to be added in reaction kettle, 80 DEG C of set temperature, cera alba 1 ~ 3% is added while stirring With monoglyceride 1 ~ 3%, after being heated to 75 DEG C, continue stirring 20 minutes, all melts to cera alba and monoglyceride, release, cooling is standby With；
(2) linseed oil 20 ~ 50% is added in material cylinder, sequentially adds desiccant while stirring under the revolving speed of 200r/min 0.1 ~ 0.2%, barium sulfate 15 ~ 50%, pigment powder 5 ~ 30%, 400r/min disperse 20 minutes, and the semi-finished product that step (1) obtains are added, It is smooth that pulp surface is dispersed under the revolving speed of 800 r/min, no particle is then sent to hydraulic grinder and is ground to fineness and is less than 30 μm, obtain oil colour.
Beneficial effects of the present invention:
The present invention provides a kind of new oil colours, and non-stimulated smell is safe and non-toxic, can directly contact human body, possess Good water solubility, thus have the characteristics that easy cleaning, it is green product.It solves existing oil colour and glues pen, oil powder The technical problems such as separation can be improved drawing quality, save material and reduce environmental pollution.Glycerin monostearate therein is to people Body nonhazardous has good emulsifiability, each component in oil colour can be made to form uniformly mixed dispersion, reduces System viscosity, viscosity 3000-5000P, drying time 5-7 days, oil colour was soft, flexible, can also improve its guarantor's type energy Power.
Specific embodiment
Embodiment 1
(1) it takes linseed oil 2.9% to be added in reaction kettle, 80 DEG C of set temperature, cera alba 1 is added while stirring and list is sweet Ester 1 after being heated to 75 DEG C, continues stirring 20% minute, all melts to cera alba and monoglyceride, releases, cooling is spare；
(2) linseed oil 50% is added in material cylinder, sequentially adds desiccant while stirring under the revolving speed of 200r/min 0.1%, barium sulfate 15%, pigment powder 30%, 400r/min disperse 20 minutes, the semi-finished product that step (1) obtains are added, in 800 r/ It is smooth that pulp surface is dispersed under the revolving speed of min, no particle is then sent to hydraulic grinder and is ground to fineness less than 30 μm, obtains Oil colour.
Pigment technology index made from the present embodiment:
Color difference (color difference meter) Δ E 0.98
40 μm of fineness (Hegman grind gage)
Tinting strength, tinting power 102%
Density 1.5g/cm3
Covering power 102%
I grades of fastness rate
Viscosity 5000P
Drying time 6 days
Embodiment 2
(1) it takes linseed oil 2.85% to be added in reaction kettle, 80 DEG C of set temperature, cera alba 2% and list is added while stirring Sweet ester 2% after being heated to 75 DEG C, continues stirring 20 minutes, all melts to cera alba and monoglyceride, releases, cooling is spare；
(2) linseed oil 20% is added in material cylinder, sequentially adds desiccant while stirring under the revolving speed of 200r/min 0.15%, barium sulfate 48%, pigment powder 25%, 400r/min disperse 20 minutes, the semi-finished product that step (1) obtains are added, in 800 r/ It is smooth that pulp surface is dispersed under the revolving speed of min, no particle is then sent to hydraulic grinder and is ground to fineness less than 30 μm, obtains Oil colour.
Technical indicator:
Color difference (color difference meter) Δ E 0.95
39 μm of fineness (Hegman grind gage)
Tinting strength, tinting power 105%
Density 2.0g/cm3
Covering power 105%
I grades of fastness rate
Viscosity 3000P
Drying time 6 days
Embodiment 3
(1) it takes linseed oil 2.8% to be added in reaction kettle, 80 DEG C of set temperature, cera alba 3% is added while stirring and list is sweet Ester 3% after being heated to 75 DEG C, continues stirring 20 minutes, all melts to cera alba and monoglyceride, releases, cooling is spare；
(2) linseed oil 36% is added in material cylinder, sequentially adds desiccant while stirring under the revolving speed of 200r/min 0.2%, barium sulfate 50%, pigment powder 5%, 400r/min disperse 20 minutes, the semi-finished product that step (1) obtains are added, in 800 r/ It is smooth that pulp surface is dispersed under the revolving speed of min, no particle is then sent to hydraulic grinder and is ground to fineness less than 30 μm, obtains Oil colour.
Technical indicator:
Color difference (color difference meter) Δ E 0.89
39 μm of fineness (Hegman grind gage)
Tinting strength, tinting power 102%
Density 1.8g/cm3
Covering power 102%
I grades of fastness rate
Viscosity 5000P
Drying time 7 days
In each embodiment implementation process, pigment powder, filler, various auxiliary agents should be put into dispersion machine according to formula rate In, speed of strict control dispersion machine, forms good rotation nest during this, determines that the addition of material is suitable according to material properties Sequence.Dispersion forms the surface of smooth and beautiful appearance and the lotion of exquisiteness to oil colour completely.
Strict temperature control in dispersion process, when preventing activation temperature excessively high, auxiliary rheological agents control rheological property and disappear, but Dispersion temperature can not be too low, prevents dispersion not exclusively, the too low effect that cannot give full play to auxiliary rheological agents of activation temperature, so that Influence the lotion form and the storage stability in later period of product.

Claims (1)

1. a kind of oil colour, it is characterised in that: it by weight percentage include following component,
Linseed oil 22.85 ~ 52.9%
Cera alba 1-3%
Monoglyceride 1-3%
Desiccant 0.1-0.2%
Barium sulfate 15-50%
Pigment powder 5-30%；
A kind of preparation method of oil colour, includes the following steps:
(1) it takes linseed oil 2.8 ~ 2.9% to be added in reaction kettle, 80 DEG C of set temperature, cera alba 1 ~ 3% and list is added while stirring Sweet ester 1 ~ 3% after being heated to 75 DEG C, continues stirring 20 minutes, all melts to cera alba and monoglyceride, releases, cooling is spare；
(2) in material cylinder be added linseed oil 20 ~ 50%, sequentially added while stirring under the revolving speed of 200r/min desiccant 0.1 ~ 0.2%, barium sulfate 15 ~ 50%, pigment powder 5 ~ 30%, 400r/min disperse 20 minutes, and the semi-finished product that step (1) obtains are added, It is smooth that pulp surface is dispersed under the revolving speed of 800 r/min, no particle is then sent to hydraulic grinder and is ground to fineness less than 30 μm, obtain oil colour.
CN201610968681.XA 2016-10-28 2016-10-28 A kind of oil colour Active CN106554719B (en)

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CN106554719B true CN106554719B (en) 2019-07-12

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106995660B (en) * 2017-06-02 2019-04-05 中国科学院包头稀土研发中心 A kind of novel rare-earth oil colour and preparation method thereof
CN111393916A (en) * 2020-05-25 2020-07-10 苏州德加画材科技有限公司 Antistatic aging-resistant oil painting pigment
CN111925679B (en) * 2020-08-20 2021-08-17 新乡学院 Oil painting pigment for fine arts
CN115584154A (en) * 2022-10-08 2023-01-10 天长市嘉丰美术用品有限公司 Preparation process of water-soluble oil painting pigment

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102816478A (en) * 2012-09-11 2012-12-12 上海实业马利画材有限公司 Application of thixotropic agent in museum-level oil paint pigment connecting material
CN104275963A (en) * 2013-07-09 2015-01-14 修森经贸发展(上海)有限公司 Environment-friendly scrawling bar for children
CN105440764A (en) * 2015-12-27 2016-03-30 青岛大方智慧网络科技有限公司 Waterproof oil paint

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102816478A (en) * 2012-09-11 2012-12-12 上海实业马利画材有限公司 Application of thixotropic agent in museum-level oil paint pigment connecting material
CN104275963A (en) * 2013-07-09 2015-01-14 修森经贸发展(上海)有限公司 Environment-friendly scrawling bar for children
CN105440764A (en) * 2015-12-27 2016-03-30 青岛大方智慧网络科技有限公司 Waterproof oil paint

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