CN106554719A - A kind of oil colour - Google Patents

A kind of oil colour Download PDF

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Publication number
CN106554719A
CN106554719A CN201610968681.XA CN201610968681A CN106554719A CN 106554719 A CN106554719 A CN 106554719A CN 201610968681 A CN201610968681 A CN 201610968681A CN 106554719 A CN106554719 A CN 106554719A
Authority
CN
China
Prior art keywords
oil colour
oleum lini
stirring
monoglyceride
cera alba
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610968681.XA
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Chinese (zh)
Other versions
CN106554719B (en
Inventor
赵松松
洪梅
颜秀花
吴永泽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHUYANG PHOENIX PAINT COLOR CO Ltd
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SHUYANG PHOENIX PAINT COLOR CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by SHUYANG PHOENIX PAINT COLOR CO Ltd filed Critical SHUYANG PHOENIX PAINT COLOR CO Ltd
Priority to CN201610968681.XA priority Critical patent/CN106554719B/en
Publication of CN106554719A publication Critical patent/CN106554719A/en
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Publication of CN106554719B publication Critical patent/CN106554719B/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/005—Drying oils
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/06—Waxes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/06—Artists' paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group

Abstract

The invention discloses a kind of oil colour, by weight percentage including following component, oleum lini 22.85 ~ 52.9, cera alba 1 3%, monoglyceride 1 3%, desiccant 0.1 0.2%, barium sulfate 15 50%, pigment powder 5 30%.The non-stimulated abnormal smells from the patient of the pigment, safety non-toxic, can directly contact human body, the features such as possessing good water solublity, thus there is easy cleaning, be Green Product.The technical barriers such as the viscous pen of existing oil colour, oil meal separation are solved, drawing quality can be improved, material is saved and reduced environmental pollution.

Description

A kind of oil colour
Technical field
The present invention relates to pigment, more particularly to a kind of oil colour.
Background technology
As the increasingly upgrading that artist is required to painting material, particularly oil colour are artist succession paints The painting material most doted on, caused by traditional oil painting pigment, vegetable oil and paint filler are easily separated, quality is unstable, traditional Auxiliary rheological agents（Castor oil hydrogenated, Cera Flava, stearic acid etc.）The oil colour viscosity of production is big, easily produces in artist painting process Stagnant phenomenon of raw viscous pen.
The content of the invention
In order to overcome drawbacks described above, the invention provides a kind of oil colour, modest viscosity, painting effect are good.
The present invention is achieved through the following technical solutions：
A kind of oil colour, by weight percentage including following component,
Oleum lini 22.85 ~ 52.9
Cera alba 1-3%
Monoglyceride 1-3%
Desiccant 0.1-0.2%
Barium sulfate 15-50%
Pigment powder 5-30%.
A kind of preparation method of oil colour, comprises the steps：
（1）Take oleum lini 2.8 ~ 2.9 to be added in reactor, 80 DEG C of design temperature, add cera alba 1 ~ 3 and list sweet while stirring Fat 1 ~ 3, after being heated to 75 DEG C, continues stirring 20 minutes, treats that cera alba and monoglyceride all melt, releases, cool down standby；
（2）Oleum lini 20 ~ 50 is added in material cylinder, sequentially added under the rotating speed of 200r/min while stirring desiccant 0.1 ~ 0.2nd, barium sulfate 15 ~ 50, pigment powder 5 ~ 30,400r/min disperse 20 minutes, add step（1）The semi-finished product of acquisition, 800 Pulp surface is dispersed under the rotating speed of r/min smooth, without granule, be then sent to hydraulic pressure grinder and fineness be ground to less than 30 m, Obtain oil colour.
Beneficial effects of the present invention：
The invention provides a kind of new oil colour, non-stimulated abnormal smells from the patient, safety non-toxic, can directly contact human body, possess good Water solublity, thus have easy cleaning the features such as, be Green Product.Solve the viscous pen of existing oil colour, oil meal to separate Deng technical barrier, drawing quality can be improved, material is saved and is reduced environmental pollution.Glyceryl monostearate therein to human body without Poison, with good emulsifiability, the dispersion of each component formation mix homogeneously in oil colour can be made, system is reduced Viscosity, viscosity 3000-5000P, 5-7 days drying time, oil colour is soft, flexible, can also improve its guarantor's type ability.
Specific embodiment
Embodiment 1
（1）Take oleum lini 2.9 to be added in reactor, 80 DEG C of design temperature, add cera alba 1 and monoglyceride 1 while stirring, plus Heat continues stirring 20 minutes to after 75 DEG C, treats that cera alba and monoglyceride all melt, releases, cool down standby；
（2）Oleum lini 50 is added in material cylinder, desiccant 0.1, sulphuric acid is sequentially added under the rotating speed of 200r/min while stirring Barium 15, pigment powder 30,400r/min disperse 20 minutes, add step（1）The semi-finished product of acquisition, under the rotating speed of 800 r/min Be dispersed to pulp surface smooth, without granule, be then sent to hydraulic pressure grinder and fineness be ground to less than 30 m, obtain oil colour.
Pigment technology index obtained in the present embodiment：
Aberration（Color difference meter) Δ E 0.98
Fineness（Hegman grind gage） 40µm
Tinting strength, tinting power 102%
Density 1.5g/cm
Covering power 102%
Fastness rate I levels
Viscosity 5000P
6 days drying times
Embodiment 2
（1）Take oleum lini 2.85 to be added in reactor, 80 DEG C of design temperature, add cera alba 2 and monoglyceride 2 while stirring, After being heated to 75 DEG C, continue stirring 20 minutes, treat that cera alba and monoglyceride all melt, release, cool down standby；
（2）Oleum lini 20 is added in material cylinder, desiccant 0.15, sulphuric acid is sequentially added under the rotating speed of 200r/min while stirring Barium 48, pigment powder 25,400r/min disperse 20 minutes, add step（1）The semi-finished product of acquisition, under the rotating speed of 800 r/min Be dispersed to pulp surface smooth, without granule, be then sent to hydraulic pressure grinder and fineness be ground to less than 30 m, obtain oil colour.
Technical specification：
Aberration（Color difference meter) Δ E 0.95
Fineness（Hegman grind gage） 39µm
Tinting strength, tinting power 105%
Density 2.0g/cm
Covering power 105%
Fastness rate I levels
Viscosity 3000P
6 days drying times
Embodiment 3
（1）Take oleum lini 2.8 to be added in reactor, 80 DEG C of design temperature, add cera alba 3 and monoglyceride 3 while stirring, plus Heat continues stirring 20 minutes to after 75 DEG C, treats that cera alba and monoglyceride all melt, releases, cool down standby；
（2）Oleum lini 36 is added in material cylinder, desiccant 0.2, sulphuric acid is sequentially added under the rotating speed of 200r/min while stirring Barium 50, pigment powder 5,400r/min disperse 20 minutes, add step（1）The semi-finished product of acquisition, divide under the rotating speed of 800 r/min Be dissipated to pulp surface smooth, without granule, be then sent to hydraulic pressure grinder and fineness be ground to less than 30 m, obtain oil colour.
Technical specification：
Aberration（Color difference meter) Δ E 0.89
Fineness（Hegman grind gage） 39µm
Tinting strength, tinting power 102%
Density 1.8g/cm
Covering power 102%
Fastness rate I levels
Viscosity 5000P
7 days drying times
In each embodiment implementation process, pigment powder, filler, various auxiliary agents should be put in dispersion machine according to formula proportion, this During strict control dispersion machine speed, form good rotation nest, determine the order of addition of material according to material propertiess.Dispersion Form the surface of smooth and beautiful appearance and the mastic of exquisiteness completely to oil colour.
Strict temperature control in dispersive process, when preventing activation temperature too high, auxiliary rheological agents control rheological property disappears, but Dispersion temperature can not be too low, prevents dispersion incomplete, the too low effect that can not give full play to auxiliary rheological agents of activation temperature, so that Affect the mastic form and the storage stability in later stage of product.

Claims (2)

1. a kind of oil colour, it is characterised in that：Include following component by weight percentage,
Oleum lini 22.85 ~ 52.9
Cera alba 1-3%
Monoglyceride 1-3%
Desiccant 0.1-0.2%
Barium sulfate 15-50%
Pigment powder 5-30%.
2. a kind of preparation method of oil colour according to claim 1, comprises the steps：
（1）Take oleum lini 2.8 ~ 2.9 to be added in reactor, 80 DEG C of design temperature, add cera alba 1 ~ 3 and list sweet while stirring Fat 1 ~ 3, after being heated to 75 DEG C, continues stirring 20 minutes, treats that cera alba and monoglyceride all melt, releases, cool down standby；
（2）Oleum lini 20 ~ 50 is added in material cylinder, sequentially added under the rotating speed of 200r/min while stirring desiccant 0.1 ~ 0.2nd, barium sulfate 15 ~ 50, pigment powder 5 ~ 30,400r/min disperse 20 minutes, add step（1）The semi-finished product of acquisition, 800 Pulp surface is dispersed under the rotating speed of r/min smooth, without granule, be then sent to hydraulic pressure grinder and fineness be ground to less than 30 m, Obtain oil colour.
CN201610968681.XA 2016-10-28 2016-10-28 A kind of oil colour Active CN106554719B (en)

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Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
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CN106554719A true CN106554719A (en) 2017-04-05
CN106554719B CN106554719B (en) 2019-07-12

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106995660A (en) * 2017-06-02 2017-08-01 中国科学院包头稀土研发中心 A kind of novel rare-earth oil colour and preparation method thereof
CN111393916A (en) * 2020-05-25 2020-07-10 苏州德加画材科技有限公司 Antistatic aging-resistant oil painting pigment
CN111925679A (en) * 2020-08-20 2020-11-13 新乡学院 Oil painting pigment for fine arts
CN115584154A (en) * 2022-10-08 2023-01-10 天长市嘉丰美术用品有限公司 Preparation process of water-soluble oil painting pigment

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102816478A (en) * 2012-09-11 2012-12-12 上海实业马利画材有限公司 Application of thixotropic agent in museum-level oil paint pigment connecting material
CN104275963A (en) * 2013-07-09 2015-01-14 修森经贸发展(上海)有限公司 Environment-friendly scrawling bar for children
CN105440764A (en) * 2015-12-27 2016-03-30 青岛大方智慧网络科技有限公司 Waterproof oil paint

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102816478A (en) * 2012-09-11 2012-12-12 上海实业马利画材有限公司 Application of thixotropic agent in museum-level oil paint pigment connecting material
CN104275963A (en) * 2013-07-09 2015-01-14 修森经贸发展(上海)有限公司 Environment-friendly scrawling bar for children
CN105440764A (en) * 2015-12-27 2016-03-30 青岛大方智慧网络科技有限公司 Waterproof oil paint

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106995660A (en) * 2017-06-02 2017-08-01 中国科学院包头稀土研发中心 A kind of novel rare-earth oil colour and preparation method thereof
CN106995660B (en) * 2017-06-02 2019-04-05 中国科学院包头稀土研发中心 A kind of novel rare-earth oil colour and preparation method thereof
CN111393916A (en) * 2020-05-25 2020-07-10 苏州德加画材科技有限公司 Antistatic aging-resistant oil painting pigment
CN111925679A (en) * 2020-08-20 2020-11-13 新乡学院 Oil painting pigment for fine arts
CN111925679B (en) * 2020-08-20 2021-08-17 新乡学院 Oil painting pigment for fine arts
CN115584154A (en) * 2022-10-08 2023-01-10 天长市嘉丰美术用品有限公司 Preparation process of water-soluble oil painting pigment

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