CN103948523A - 木瓜有效组分的制备方法与用途 - Google Patents
木瓜有效组分的制备方法与用途 Download PDFInfo
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- CN103948523A CN103948523A CN201410135643.7A CN201410135643A CN103948523A CN 103948523 A CN103948523 A CN 103948523A CN 201410135643 A CN201410135643 A CN 201410135643A CN 103948523 A CN103948523 A CN 103948523A
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- Prior art keywords
- fructus chaenomelis
- active component
- preparation
- ethanol
- papaya
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 235000009467 Carica papaya Nutrition 0.000 title claims abstract description 13
- 241000219173 Carica Species 0.000 title claims abstract 6
- 239000000203 mixture Substances 0.000 title abstract description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000011347 resin Substances 0.000 claims abstract description 11
- 229920005989 resin Polymers 0.000 claims abstract description 11
- 238000000605 extraction Methods 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 239000003480 eluent Substances 0.000 claims description 19
- 238000002481 ethanol extraction Methods 0.000 claims description 12
- 239000003463 adsorbent Substances 0.000 claims description 9
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 9
- 239000002537 cosmetic Substances 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 5
- 230000003064 anti-oxidating effect Effects 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 8
- 239000003814 drug Substances 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 230000003647 oxidation Effects 0.000 abstract description 4
- 238000007254 oxidation reaction Methods 0.000 abstract description 4
- 230000035772 mutation Effects 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000009759 skin aging Effects 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract 2
- 238000001179 sorption measurement Methods 0.000 abstract 2
- XBZYWSMVVKYHQN-MYPRUECHSA-N (4as,6as,6br,8ar,9r,10s,12ar,12br,14bs)-10-hydroxy-2,2,6a,6b,9,12a-hexamethyl-9-[(sulfooxy)methyl]-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,12b,13,14b-icosahydropicene-4a-carboxylic acid Chemical compound C1C[C@H](O)[C@@](C)(COS(O)(=O)=O)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CCC(C)(C)C[C@H]5C4=CC[C@@H]3[C@]21C XBZYWSMVVKYHQN-MYPRUECHSA-N 0.000 abstract 1
- 230000032683 aging Effects 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000007865 diluting Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 34
- 238000012360 testing method Methods 0.000 description 15
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- 239000000523 sample Substances 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 10
- 230000031700 light absorption Effects 0.000 description 10
- 239000012153 distilled water Substances 0.000 description 9
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 8
- 240000006432 Carica papaya Species 0.000 description 7
- 238000002835 absorbance Methods 0.000 description 6
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 description 6
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 5
- 235000013399 edible fruits Nutrition 0.000 description 5
- 239000000284 extract Substances 0.000 description 5
- 150000003648 triterpenes Chemical class 0.000 description 5
- 240000001592 Amaranthus caudatus Species 0.000 description 4
- 235000009328 Amaranthus caudatus Nutrition 0.000 description 4
- -1 DPPH free radical Chemical class 0.000 description 4
- OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical compound [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 description 4
- 229960000583 acetic acid Drugs 0.000 description 4
- 235000012735 amaranth Nutrition 0.000 description 4
- 239000004178 amaranth Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000012362 glacial acetic acid Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000000872 buffer Substances 0.000 description 3
- 238000010790 dilution Methods 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- DCYOBGZUOMKFPA-UHFFFAOYSA-N iron(2+);iron(3+);octadecacyanide Chemical compound [Fe+2].[Fe+2].[Fe+2].[Fe+3].[Fe+3].[Fe+3].[Fe+3].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] DCYOBGZUOMKFPA-UHFFFAOYSA-N 0.000 description 3
- 229960003351 prussian blue Drugs 0.000 description 3
- 239000013225 prussian blue Substances 0.000 description 3
- 229940079877 pyrogallol Drugs 0.000 description 3
- 150000003254 radicals Chemical class 0.000 description 3
- 230000002000 scavenging effect Effects 0.000 description 3
- QKNYBSVHEMOAJP-UHFFFAOYSA-N 2-amino-2-(hydroxymethyl)propane-1,3-diol;hydron;chloride Chemical compound Cl.OCC(N)(CO)CO QKNYBSVHEMOAJP-UHFFFAOYSA-N 0.000 description 2
- 240000000425 Chaenomeles speciosa Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 2
- 206010047601 Vitamin B1 deficiency Diseases 0.000 description 2
- 229960005070 ascorbic acid Drugs 0.000 description 2
- 235000010323 ascorbic acid Nutrition 0.000 description 2
- 239000011668 ascorbic acid Substances 0.000 description 2
- 208000002894 beriberi Diseases 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 150000002215 flavonoids Chemical class 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
- 235000013402 health food Nutrition 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 210000003205 muscle Anatomy 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 239000000276 potassium ferrocyanide Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 230000002040 relaxant effect Effects 0.000 description 2
- 229930182490 saponin Natural products 0.000 description 2
- 150000007949 saponins Chemical class 0.000 description 2
- 235000017709 saponins Nutrition 0.000 description 2
- 235000018553 tannin Nutrition 0.000 description 2
- 239000001648 tannin Substances 0.000 description 2
- 229920001864 tannin Polymers 0.000 description 2
- 210000002435 tendon Anatomy 0.000 description 2
- XOGGUFAVLNCTRS-UHFFFAOYSA-N tetrapotassium;iron(2+);hexacyanide Chemical compound [K+].[K+].[K+].[K+].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] XOGGUFAVLNCTRS-UHFFFAOYSA-N 0.000 description 2
- 208000006820 Arthralgia Diseases 0.000 description 1
- 208000006770 Ascorbic Acid Deficiency Diseases 0.000 description 1
- 235000006264 Asimina triloba Nutrition 0.000 description 1
- 241001507936 Chaenomeles Species 0.000 description 1
- 240000008918 Chaenomeles cathayensis Species 0.000 description 1
- 206010008631 Cholera Diseases 0.000 description 1
- 206010010904 Convulsion Diseases 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 208000004232 Enteritis Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010062575 Muscle contracture Diseases 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 235000014443 Pyrus communis Nutrition 0.000 description 1
- 244000047670 Viola x wittrockiana Species 0.000 description 1
- 235000004031 Viola x wittrockiana Nutrition 0.000 description 1
- 206010047623 Vitamin C deficiency Diseases 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000006286 aqueous extract Substances 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 239000012490 blank solution Substances 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000009514 concussion Effects 0.000 description 1
- 208000006111 contracture Diseases 0.000 description 1
- 230000036461 convulsion Effects 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 230000007760 free radical scavenging Effects 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 235000019990 fruit wine Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 210000000629 knee joint Anatomy 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 239000008363 phosphate buffer Substances 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000013641 positive control Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 208000010233 scurvy Diseases 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- YNJBWRMUSHSURL-UHFFFAOYSA-N trichloroacetic acid Chemical compound OC(=O)C(Cl)(Cl)Cl YNJBWRMUSHSURL-UHFFFAOYSA-N 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Description
产品 | 所得木瓜有效组分中三萜含量 |
实施例1 | 13.6% |
实施例2 | 13.8% |
实施例3 | 13.5% |
对比例3 | 8.3% |
对比例4 | 7.5% |
对比例5 | 7.8% |
对比例6 | 9.1% |
对比例7 | 8.8% |
对比例8 | 8.1% |
Claims (8)
Priority Applications (1)
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CN201410135643.7A CN103948523B (zh) | 2014-04-04 | 2014-04-04 | 木瓜有效组分的制备方法与用途 |
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CN201410135643.7A CN103948523B (zh) | 2014-04-04 | 2014-04-04 | 木瓜有效组分的制备方法与用途 |
Publications (2)
Publication Number | Publication Date |
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CN103948523A true CN103948523A (zh) | 2014-07-30 |
CN103948523B CN103948523B (zh) | 2017-05-17 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108902929A (zh) * | 2018-08-22 | 2018-11-30 | 合肥工业大学 | 宣木瓜灵芝孢子粉片剂及其制备方法和应用 |
CN108969438A (zh) * | 2018-08-23 | 2018-12-11 | 广东幸美化妆品股份有限公司 | 含有白芨提取物、白花木瓜提取物和仙鹤草提取物的抗皱霜及其制备方法 |
CN109221382A (zh) * | 2018-08-22 | 2019-01-18 | 合肥工业大学 | 宣木瓜提取物及其制备方法和应用 |
CN115105543A (zh) * | 2022-04-01 | 2022-09-27 | 三峡大学 | 木瓜总三萜在制备抗胃衰老药物中的应用 |
Citations (5)
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JP2008174526A (ja) * | 2007-01-22 | 2008-07-31 | Naris Cosmetics Co Ltd | アレルゲン不活化剤、及びそれを含有する皮膚外用剤、又はアレルゲン不活化用製品 |
CN102258598A (zh) * | 2010-05-24 | 2011-11-30 | 魏伟 | 以木瓜有效部位制成的药物、其制备方法及其应用 |
CN103054972A (zh) * | 2012-12-20 | 2013-04-24 | 蚌埠丰原涂山制药有限公司 | 一种从木瓜中提取齐墩果酸和熊果酸的方法 |
KR101264005B1 (ko) * | 2011-03-11 | 2013-05-13 | 어봉우 | 관절염 치료용 한방 액상 발효 조성물의 제조방법 |
CN103638141A (zh) * | 2013-12-12 | 2014-03-19 | 三峡大学 | 木瓜提取物及其制备方法与它的用途 |
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2014
- 2014-04-04 CN CN201410135643.7A patent/CN103948523B/zh active Active
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JP2008174526A (ja) * | 2007-01-22 | 2008-07-31 | Naris Cosmetics Co Ltd | アレルゲン不活化剤、及びそれを含有する皮膚外用剤、又はアレルゲン不活化用製品 |
CN102258598A (zh) * | 2010-05-24 | 2011-11-30 | 魏伟 | 以木瓜有效部位制成的药物、其制备方法及其应用 |
KR101264005B1 (ko) * | 2011-03-11 | 2013-05-13 | 어봉우 | 관절염 치료용 한방 액상 발효 조성물의 제조방법 |
CN103054972A (zh) * | 2012-12-20 | 2013-04-24 | 蚌埠丰原涂山制药有限公司 | 一种从木瓜中提取齐墩果酸和熊果酸的方法 |
CN103638141A (zh) * | 2013-12-12 | 2014-03-19 | 三峡大学 | 木瓜提取物及其制备方法与它的用途 |
Non-Patent Citations (2)
Title |
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屈晓清: "宣木瓜中三萜酸的提取分离及其体外抑菌性研究", 《中国优秀硕士学位论文全文数据库工程科技I辑(月刊)》 * |
盛侠: "宣木瓜中齐墩果酸的提取分离及其抗氧化作用的研究", 《中国优秀硕士学位论文全文数据库工程科技I辑(月刊)》 * |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108902929A (zh) * | 2018-08-22 | 2018-11-30 | 合肥工业大学 | 宣木瓜灵芝孢子粉片剂及其制备方法和应用 |
CN109221382A (zh) * | 2018-08-22 | 2019-01-18 | 合肥工业大学 | 宣木瓜提取物及其制备方法和应用 |
CN108969438A (zh) * | 2018-08-23 | 2018-12-11 | 广东幸美化妆品股份有限公司 | 含有白芨提取物、白花木瓜提取物和仙鹤草提取物的抗皱霜及其制备方法 |
CN108969438B (zh) * | 2018-08-23 | 2021-09-21 | 广东幸美化妆品股份有限公司 | 含有白芨提取物、白花木瓜提取物和仙鹤草提取物的抗皱霜及其制备方法 |
CN115105543A (zh) * | 2022-04-01 | 2022-09-27 | 三峡大学 | 木瓜总三萜在制备抗胃衰老药物中的应用 |
CN115105543B (zh) * | 2022-04-01 | 2023-10-27 | 三峡大学 | 木瓜总三萜在制备抗胃衰老药物中的应用 |
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Effective date of registration: 20170811 Address after: 510080, No. 81, B, C, D and E, No. 15, agriculture and forestry road, Yuexiu District, Guangzhou, Guangdong Co-patentee after: KINGWAY COSMETICS TECHNOLOGY GUANGZHOU CO., LTD. Patentee after: Guangdong Xing Mei cosmetics limited company Address before: 510000, No. 81, B, C, D and E, No. 15, agriculture and forestry road, Yuexiu District, Guangzhou, Guangdong Patentee before: Guangdong Xing Mei cosmetics limited company |
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Effective date of registration: 20190121 Address after: 510080 B, C, D, E, 15 floor, 81 Nong Lin Road, Yuexiu District, Guangzhou, Guangdong. Patentee after: Guangdong Xing Mei cosmetics limited company Address before: 510080 B, C, D, E, 15 floor, 81 Nong Lin Road, Yuexiu District, Guangzhou, Guangdong. Co-patentee before: KINGWAY COSMETICS TECHNOLOGY GUANGZHOU CO., LTD. Patentee before: Guangdong Xing Mei cosmetics limited company |
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Address after: 510062 room a329, No. 64, Zhixin South Road, Yuexiu District, Guangzhou City, Guangdong Province Patentee after: H&B COSMETICS CORPORATION CO.,LTD. Address before: 510080 B, C, D, E, 15 floor, 81 Nong Lin Road, Yuexiu District, Guangzhou, Guangdong. Patentee before: H&B COSMETICS CORPORATION CO.,LTD. |
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