CN103877602B - Taxus chinensis solid air freshener and preparation formula and preparation method thereof - Google Patents
Taxus chinensis solid air freshener and preparation formula and preparation method thereof Download PDFInfo
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- CN103877602B CN103877602B CN201410120778.6A CN201410120778A CN103877602B CN 103877602 B CN103877602 B CN 103877602B CN 201410120778 A CN201410120778 A CN 201410120778A CN 103877602 B CN103877602 B CN 103877602B
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Abstract
The invention provides a taxus chinensis solid air freshener and a preparation formula and a preparation method thereof and belongs to the technical field of daily-use chemical products. The preparation method comprises the following steps: preparing a homogenate; preparing a base solution; curing and forming and the like. The formula comprises the following components in parts by weight: 1.5-3.5% of a gel, 1.1-5.0% of a preservative, 0-1.0% of taxus chinensis essence and the balance of the base solution. The base solution is extracted from upper oil phase of a distillate or part of or all lower water phase of the distillate of the homogenate. The homogenate is prepared by homogenizing smashed branches and leaves of taxus chinensis plant branches and leaves, water and non-volatile inorganic acid. The taxus chinensis solid air freshener provided by the invention has the functions of strongly preventing insomnia, relieving nervousness, tranquilizing and allaying excitement and dispelling insects.
Description
Technical field
The present invention relates to a kind of Ramulus et folium taxi cuspidatae solid air freshening agent and its manufacture formula and manufacture method, belong to daily-use chemical industry
Product technical field.
Background technology
At present the flavor type of air freshener class product on the market is based on the common fragrance of a flower, hay-scented and fruit perfume,
Individually using high megaphanerophyte branch and leaf abnormal smells from the patient as the few of odor type, without clear as the air of main body using natural Ramulus et folium taxi cuspidatae fragrance
New agent product.The flavor component of air freshener class product, great majority by chemical industry synthesis, allotment, do not contain natural carrying merely
Take active substance or content is very low.The flavor component of air freshener primarily serves the effect for covering abnormal flavour in air, typically not
Containing terpenes, alkaloidss active skull cap components, not with effects of tranquilizing and allaying excitement, not with insect-expelling function.
People are through long-term exploration, it is proposed that various solutions, Chinese patent [application number：
201310035244.9] a kind of health perfume product of taxus chinensis essential oil and Ramulus et folium taxi cuspidatae extract for raw material, the perfume are disclosed
Health perfume product of the product with taxus chinensis essential oil and Ramulus et folium taxi cuspidatae extract as raw material are by essence, spice, solvent and 1-30% Semen Phaseolis
China fir quintessence oil and Ramulus et folium taxi cuspidatae extract are made.The program will not cause side effect to human body, can for a long time as daily perfume, and air is clear
New agent is used.
But such scheme does not clearly provide the extraction process of Ramulus et folium taxi cuspidatae extract, and the taxus chinensis essential oil in the formula
Liposoluble substance is with Ramulus et folium taxi cuspidatae extract, volatility is poor；Although not being given containing materials such as ethanol, water in formula
Which kind of surfactant solubilising, homogenizing are carried out using, therefore, when such scheme is used as air freshener, exist uniform
Property is the shortcomings of poor, volatility is poor, production cost is high.
The content of the invention
The purpose of the present invention is for the problems referred to above, there is provided a kind of easy to implement, and the Ramulus et folium taxi cuspidatae solid of superior product quality is empty
Gas freshener manufacture method.
It is a further object of the present invention to provide a kind of contain natural volatile ingredient, with tranquillizing and allaying excitement and insect-expelling function
Ramulus et folium taxi cuspidatae solid air freshening agent.
The present invention has again a purpose to be to provide a kind of compatibility rationally, and cost is relatively low, and the Ramulus et folium taxi cuspidatae solid of superior product quality is empty
The manufacture formula of gas freshener.
To reach above-mentioned purpose, the present invention adopts following technical proposals：
A kind of manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent, this method is comprised the following steps：
A, prepare homogenate：The branch and leaf of Chinese yew genus plants are crushed after drying, branch and leaf ground product is obtained；Branch and leaf are crushed
Thing mixes with suitable quantity of water, adds appropriate non-volatile inorganic acid, is homogenized after swelling, obtains homogenate；
B, prepare basal liquid：Homogenate is passed through into steam distillation, condensation obtains distillation, then distillation standing is divided
Layer, takes the upper oil phase and part or all of lower floor's water phase of distillation, obtains basal liquid；
C, curing molding：Add gel and preservative in basal liquid, be mixed and heated to be completely dissolved, obtain liquid and mix
Compound；Pour above-mentioned liquefied mixture in mould cooling shaping, Ramulus et folium taxi cuspidatae solid air freshening agent is obtained final product after the demoulding.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step, described branch and leaf ground product with
The mass ratio of water is 1:3-1:6；The addition of described non-volatile inorganic acid is the 0.01-1.0% of homogenate gross mass.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step, the branch and leaf of Chinese yew genus plants
Jing 60-80 DEG C crushed after being dried, crosses 50-80 mesh sieves, obtains branch and leaf ground product.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in stepb, distillation time is 30-240 point
Clock, condenses the rear stopping distillation of volume 1-5 times that the distillation for obtaining reaches homogenate；Lower floor's water phase body in described basal liquid
Product is 20-50 times of upper oil phase volume.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step C, described gel is OK a karaoke club
Any one or a few mixture of glue, agar or alginate；Described preservative is tween, formaldehyde or benzoic acid
Any one or a few mixture.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step C, the addition of described gel
Measure as the 1.5-3.5% of liquefied mixture gross weight；The addition of described tween is the 0.5- of liquefied mixture gross weight
2.0%；The addition of described formaldehyde is the 0.5-1.5% of liquefied mixture gross weight；The addition of described benzoic acid is
The 0.1-1.5% of liquefied mixture gross weight；The 0- that addition is liquefied mixture gross weight is also added with described basal liquid
1.0% Ramulus et folium taxi cuspidatae essence.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step C, after being heated to being completely dissolved,
Liquefied mixture is cooled to into 50-70 DEG C, then above-mentioned liquefied mixture is poured in mould.
A kind of Ramulus et folium taxi cuspidatae solid air freshening according to obtained in the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent
Agent.
A kind of manufacture formula of Ramulus et folium taxi cuspidatae solid air freshening agent, this formula includes the component of following mass fractions：Gel
Agent 1.5-3.5%；Preservative 1.1-5.0%；Ramulus et folium taxi cuspidatae essence 0-1.0%, balance of basal liquid；Described basal liquid takes from homogenate
The distillation upper oil phase of liquid and part or all of lower floor's water phase, described homogenate is by the branch including Chinese yew genus plants branch and leaf
Leaf ground product, water and non-volatile inorganic acid Jing homogenate is made.
In the manufacture formula of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, the mass ratio of described branch and leaf ground product and water
For 1:3-1:6, the addition of described non-volatile inorganic acid is the 0.01-1.0% of homogenate gross mass, and what condensation was obtained evaporates
Go out thing and reach to stop distillation after volume 1-5 times of homogenate and the lower floor's water phase volume in basal liquid is upper oil phase volume
20-50 times；Described gel is any one or a few mixture of carrageenan, agar or alginate；Described is anti-
Rotten agent is any one or a few mixture of tween, formaldehyde or benzoic acid, and the addition of described gel accounts for this
The 1.5-3.5% of total formula weight；The addition of described tween accounts for the 0.5-2.0% of this total formula weight；Described formaldehyde
Addition accounts for the 0.5-1.5% of this total formula weight；The addition of described benzoic acid accounts for the 0.1- of this total formula weight
1.5%；The addition of described Ramulus et folium taxi cuspidatae essence accounts for the 0-1.0% of this total formula weight.
Compared with prior art, it is an advantage of the current invention that：
1st, the blank that the present invention has been filled up in existing air freshener products type, for it extra functional characteristic is provided.
2nd, can be produced containing natural volatile ingredient using this method, with strength anti-insomnia, keeping tensions down emotion,
Effect of tranquillizing and allaying excitement, and have the solid air freshener of certain insect-expelling function concurrently.
Specific embodiment
Embodiment 1
A kind of manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent, this method is comprised the following steps：
A, prepare homogenate：The branch and leaf of Chinese yew genus plants are crushed after drying, branch and leaf ground product is obtained；Branch and leaf are crushed
Thing mixes with suitable quantity of water, adds appropriate non-volatile inorganic acid, is homogenized after swelling, obtains homogenate；
B, prepare basal liquid：Homogenate is passed through into steam distillation, condensation obtains distillation, then distillation standing is divided
Layer, takes the upper oil phase and part or all of lower floor's water phase of distillation, obtains basal liquid；
C, curing molding：Add gel and preservative in basal liquid, be mixed and heated to be completely dissolved, obtain liquid and mix
Compound；Pour above-mentioned liquefied mixture in mould cooling shaping, Ramulus et folium taxi cuspidatae solid air freshening agent is obtained final product after the demoulding.
Preferably, in step, described branch and leaf ground product is 1 with the mass ratio of water:3-1:6, preferably 1:4, it is described
Non-volatile inorganic acid addition for homogenate gross mass 0.01-1.0%, preferably 0.5%.
Preferably, in step, the branch and leaf Jing 60-80 DEG C crushed after being dried of Chinese yew genus plants, leads to and is preferably 65-70
It is dried between DEG C, crosses 50-80 mesh sieves, obtains branch and leaf ground product.
Preferably, in stepb, distillation time is 30-240 minutes, condenses the body that the distillation for obtaining reaches homogenate
Stop distillation after 1-5 times of product；Under normal circumstances, distillation time determines according to the volume of distillation, in the present embodiment, when evaporating
Go out object product when reaching 3-4 times of homogenate volume, you can stop distillation, be considered as distillation completely, when distillation time is 30-
When 240 minutes, the lower floor's water phase volume in basal liquid is 20-50 times of upper oil phase volume.
Preferably, in step C, described gel is any one or a few of carrageenan, agar or alginate
Mixture；Described preservative is any one or a few mixture of tween, formaldehyde or benzoic acid.
Tween both can make profit be more easy to mixing as surfactant again as preservative, reach the work of solubilising
With so that the effective ingredient of Chinese yew genus plants is evenly distributed in water.
Preferably, in step C, the addition of described gel is the 1.5-3.5% of liquefied mixture gross weight；Institute
The addition of the tween stated is the 0.5-2.0% of liquefied mixture gross weight；The addition of described formaldehyde is that liquefied mixture is total
The 0.5-1.5% of weight；The addition of described benzoic acid is the 0.1-1.5% of liquefied mixture gross weight；Described basis
The Ramulus et folium taxi cuspidatae essence of the 0-1.0% that addition is liquefied mixture gross weight is also added with liquid.
Preferably, in step C, after being heated to being completely dissolved, liquefied mixture is cooled to into 50-70 DEG C, it is furthermore preferred that
60 DEG C are cooled to, then above-mentioned liquefied mixture is poured in mould.
A kind of Ramulus et folium taxi cuspidatae solid air freshening according to obtained in the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent
Agent.
A kind of manufacture formula of Ramulus et folium taxi cuspidatae solid air freshening agent, this formula includes the component of following mass fractions：Gel
Agent 1.5-3.5%；Preservative 1.1-5.0%；Ramulus et folium taxi cuspidatae essence 0-1.0%, balance of basal liquid；Described basal liquid takes from homogenate
The distillation upper oil phase of liquid and part or all of lower floor's water phase, described homogenate is by the branch including Chinese yew genus plants branch and leaf
Leaf ground product, water and non-volatile inorganic acid Jing homogenate is made.
Preferably, described branch and leaf ground product is 1 with the mass ratio of water:3-1:6, it is furthermore preferred that mass ratio is 1:4, institute
The addition of the non-volatile inorganic acid stated is the 0.01-1.0% of homogenate gross mass, it is furthermore preferred that non-volatile inorganic acid
Addition is the 0.5% of homogenate gross mass, after condensing preferably 3-4 times of volume 1-5 times that the distillation for obtaining reaches homogenate
Lower floor's water phase volume in stopping distillation and basal liquid is 20-50 times of upper oil phase volume；Described gel be carrageenan,
Any one or a few mixture of agar or alginate；Described preservative appointing for tween, formaldehyde or benzoic acid
Anticipate the mixture of one or more, and the addition of described gel accounts for the 1.5-3.5% of this total formula weight；Described tells
The addition of temperature accounts for the 0.5-2.0% of this total formula weight；The addition of described formaldehyde accounts for the 0.5- of this total formula weight
1.5%；The addition of described benzoic acid accounts for the 0.1-1.5% of this total formula weight；The addition of described Ramulus et folium taxi cuspidatae essence
Account for the 0-1.0% of this total formula weight.
Above-mentioned non-volatile inorganic acid is any one of sulphuric acid, phosphoric acid or its mixture, and wherein sulphuric acid is generally selected
The concentrated sulphuric acid of commercially available 98%, phosphoric acid selects commercially available 85% phosphoric acid, it is of course also possible to above-mentioned non-volatile inorganic acid is dilute
Use after releasing.
Embodiment 2-5
Embodiment herein and the course of work of embodiment 1, operation principle is essentially identical, and difference is, in step
C, curing molding：Add gel in basal liquid different with the mass number of preservative, refer to following table.
Embodiment 6
Take the Taxus mairei [Taxus chinensis (Pilger) Rehd] in a diameter of 1cm under autumn Mo pruning
Branch, the dry place's placement in cool place starts nature and comes off to blade, and 60 DEG C of dryings of Jing subsequently prescind in branch to can easily fracture
To the little bars of 3-5cm, crush, cross 60 mesh sieves, obtain taxus chinensis powder.Taxus chinensis powder with come off under blade mix, then with water with 1:6-
1:3 mass ratio mixing, preferably, in the present embodiment, with 1:5 mass ratio mixing, adds in object upon mixing
The phosphoric acid of 1.0wt%, standing is swelling to be existed without obvious liquid, homogenate.100 DEG C of steam distillation 240min of Jing after homogenate, collect
Distillation in condenser, by distillation stratification.By distillation point liquid, upper oil phase is taken, and volume is upper oil phase
The water phase of 30 times of lower floor, obtains basal liquid, in basal liquid add 2.5wt% carrageenans, 1.0wt% tweens, 1.0wt% formaldehyde,
The benzoic acid of 0.1wt% and the Ramulus et folium taxi cuspidatae essence of 0-1wt%（Ramulus et folium taxi cuspidatae essence can also be not added with）, it is mixed and heated to carrageenan complete
CL, be cooled to 50 DEG C, pours into and is cooled down in preprepared circle grinding tool, it is to be solidified after pour out, load bag air-vent
In packing box, Ramulus et folium taxi cuspidatae solid air freshening agent is obtained final product.The product has Ramulus et folium taxi cuspidatae natural flavor, and with tranquillizing and allaying excitement and drive
Worm effect.
Specific embodiment described herein is only explanation for example spiritual to the present invention.Technology neck belonging to of the invention
The technical staff in domain can be made various modifications to described specific embodiment or supplement or replaced using similar mode
Generation, but without departing from the spiritual of the present invention or surmount scope defined in appended claims.
Claims (6)
1. a kind of manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent, it is characterised in that this method is comprised the following steps：
A, prepare homogenate：The branch and leaf of Chinese yew genus plants are crushed after drying, branch and leaf ground product is obtained；By branch and leaf ground product with
Suitable quantity of water mixes, and adds appropriate non-volatile inorganic acid, is homogenized after swelling, obtains homogenate；
B, prepare basal liquid：Homogenate is passed through into steam distillation, condensation obtains distillation, then by distillation stratification, takes
The upper oil phase of distillation and part or all of lower floor's water phase, obtain basal liquid；
C, curing molding：Add gel and preservative in basal liquid, be mixed and heated to be completely dissolved, obtain liquid mixing
Thing；Pour above-mentioned liquefied mixture in mould cooling shaping, Ramulus et folium taxi cuspidatae solid air freshening agent obtained final product after the demoulding,
In stepb, distillation time is 30-240 minutes, condenses the distillation that obtains and reaches and stops after volume 1-5 times of homogenate
Only distill；Lower floor's water phase volume in described basal liquid is 20-50 times of upper oil phase volume,
In step C, described gel is any one or a few mixture of carrageenan, agar or alginate；Institute
The preservative stated is any one or a few mixture of tween, formaldehyde or benzoic acid,
In step C, the addition of described gel is the 1.5-3.5% of liquefied mixture gross weight；Described tween
Addition is the 0.5-2.0% of liquefied mixture gross weight；The addition of described formaldehyde is liquefied mixture gross weight
0.5-1.5%；The addition of described benzoic acid is the 0.1-1.5% of liquefied mixture gross weight；In described basal liquid
Also it is added with the Ramulus et folium taxi cuspidatae essence of the 0-1.0% that addition is liquefied mixture gross weight.
2. the manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 1, it is characterised in that in step,
Described branch and leaf ground product is 1 with the mass ratio of water:3-1:6；The addition of described non-volatile inorganic acid is that homogenate is total
The 0.01-1.0% of quality.
3. the manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 1, it is characterised in that in step,
The branch and leaf Jing 60-80 DEG C crushed after being dried of Chinese yew genus plants, crosses 50-80 mesh sieves, obtains branch and leaf ground product.
4. the manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 1, it is characterised in that in step C,
After being heated to being completely dissolved, liquefied mixture is cooled to into 50-70 DEG C, then above-mentioned liquefied mixture is poured in mould.
5. Semen Phaseoli obtained in the manufacture method of the Ramulus et folium taxi cuspidatae solid air freshening agent according to any one in claim 1-4
China fir solid air freshening agent.
6. a kind of Ramulus et folium taxi cuspidatae solid air freshening agent, it is characterised in that this air freshener includes the component of following mass fractions：
Gel 1.5-3.5%；Preservative 1.1-5.0%；Ramulus et folium taxi cuspidatae essence 0-1.0%, balance of basal liquid；Described basal liquid takes
From the distillation upper oil phase and part or all of lower floor's water phase of homogenate, described homogenate is by including Chinese yew genus plants branch
The branch and leaf ground product of leaf, water and non-volatile inorganic acid Jing homogenate is made,
Described branch and leaf ground product is 1 with the mass ratio of water:3-1:6, the addition of described non-volatile inorganic acid is homogenate
The 0.01-1.0% of liquid gross mass, condenses the rear stopping distillation of volume 1-5 times and basal liquid that the distillation for obtaining reaches homogenate
In lower floor water phase volume be 20-50 times of upper oil phase volume；Described gel is carrageenan, agar or alginate
Any one or a few mixture；Described preservative is the mixed of any one or a few of tween, formaldehyde or benzoic acid
Compound, and the addition of described gel accounts for the 1.5-3.5% of this total formula weight；The addition of described tween is accounted for originally matches somebody with somebody
The 0.5-2.0% of square gross weight；The addition of described formaldehyde accounts for the 0.5-1.5% of this total formula weight；Described Benzoinum
The addition of acid accounts for the 0.1-1.5% of this total formula weight；The addition of described Ramulus et folium taxi cuspidatae essence accounts for this total formula weight
0-1.0%.
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105087165A (en) * | 2015-09-18 | 2015-11-25 | 哈尔滨红豆杉科技开发有限责任公司 | Composite essential oil prepared from taxus cuspidata and coniferous plants and application of composite essential oil |
| CN107581568A (en) * | 2017-10-20 | 2018-01-16 | 天津商业大学 | One kind solidification paste essence |
| CN108379639A (en) * | 2018-05-02 | 2018-08-10 | 湖北祥瑞丰红豆杉科技股份有限公司 | A kind of air freshener and preparation method thereof |
| CN108524331B (en) * | 2018-05-02 | 2021-07-20 | 湖北祥瑞丰红豆杉科技股份有限公司 | Taxus chinensis solid perfume and preparation method thereof |
| CN112336901A (en) * | 2020-11-10 | 2021-02-09 | 湖北物莫生物科技有限公司 | Natural essential oil solid freshener and preparation process thereof |
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| CN102783589A (en) * | 2012-08-28 | 2012-11-21 | 青岛海之林生物科技开发有限公司 | Formulated gelatinizing powder and application thereof |
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| CN101138686A (en) * | 2007-07-23 | 2008-03-12 | 沈军 | Method for extracting active ingredient of natural product and uses thereof |
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| CN1097336A (en) * | 1993-07-10 | 1995-01-18 | 崔毅 | Solid-shaped air-clearing agent |
| CN102028965A (en) * | 2009-09-30 | 2011-04-27 | 湖北汇特生物医药技术有限公司 | Mugwort related extraction part medicinal property-based air freshener |
| CN101838588A (en) * | 2010-05-13 | 2010-09-22 | 合肥工业大学 | Method for extracting essential oil of taxus media |
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