CN103877602A - Taxus chinensis solid air freshener and preparation formula and preparation method thereof - Google Patents
Taxus chinensis solid air freshener and preparation formula and preparation method thereof Download PDFInfo
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Abstract
The invention provides a taxus chinensis solid air freshener and a preparation formula and a preparation method thereof and belongs to the technical field of daily-use chemical products. The preparation method comprises the following steps: preparing a homogenate; preparing a base solution; curing and forming and the like. The formula comprises the following components in parts by weight: 1.5-3.5% of a gel, 1.1-5.0% of a preservative, 0-1.0% of taxus chinensis essence and the balance of the base solution. The base solution is extracted from upper oil phase of a distillate or part of or all lower water phase of the distillate of the homogenate. The homogenate is prepared by homogenizing smashed branches and leaves of taxus chinensis plant branches and leaves, water and non-volatile inorganic acid. The taxus chinensis solid air freshener provided by the invention has the functions of strongly preventing insomnia, relieving nervousness, tranquilizing and allaying excitement and dispelling insects.
Description
Technical field
The present invention relates to a kind of Ramulus et folium taxi cuspidatae solid air freshening agent and manufacture formula and manufacture method, belong to daily chemical product technical field.
Background technology
At present the flavor type of air freshener series products is on the market taking the common fragrance of a flower, hay-scented and fruit perfume (or spice) as main, few using high megaphanerophyte branch and leaf abnormal smells from the patient as odor type separately, the not air freshener product using natural Ramulus et folium taxi cuspidatae fragrance as main body.The flavor component of air freshener series products, the simple chemical industry that relies on of great majority synthesizes, allocates, and does not contain natural extract active substance or content very low.The flavor component of air freshener mainly plays the effect of covering abnormal flavour in air, does not generally contain terpenes, alkaloids active skull cap components, does not have effects of tranquilizing and allaying excitement, does not have insect-expelling function.
People are through long-term exploration, various solutions have been proposed, Chinese patent [application number: 201310035244.9] discloses the health perfume product that a kind of taxus chinensis essential oil and Ramulus et folium taxi cuspidatae extract are raw material, the health perfume product of these perfume product taking taxus chinensis essential oil and Ramulus et folium taxi cuspidatae extract as raw material are by essence, spice, solvent and 1-30% taxus chinensis essential oil and Ramulus et folium taxi cuspidatae extract are made.This scheme can not cause side effect to human body, can be for a long time as daily perfume, and air freshener uses.
But such scheme does not clearly provide the leaching process of Ramulus et folium taxi cuspidatae extract, and taxus chinensis essential oil and Ramulus et folium taxi cuspidatae extract in this formula be liposoluble substance, and volatility is poor; Although contain the material such as ethanol, water in formula, do not provide and use which kind of surfactant to carry out solubilising, homogenizing, therefore, in the time that such scheme uses as air freshener, there is the shortcomings such as lack of homogeneity, volatility is poor, production cost is high.
Summary of the invention
The object of the invention is for the problems referred to above, provide a kind of easy to implement, the Ramulus et folium taxi cuspidatae solid air freshening agent manufacture method of superior product quality.
Another object of the present invention is to provide one and contains natural volatile ingredient, has the Ramulus et folium taxi cuspidatae solid air freshening agent of tranquillizing and allaying excitement and insect-expelling function.
It is reasonable that the present invention has an object to be to provide a kind of compatibility again, and cost is lower, the manufacture formula of the Ramulus et folium taxi cuspidatae solid air freshening agent of superior product quality.
For achieving the above object, the present invention adopts following technical proposals:
A manufacture method for Ramulus et folium taxi cuspidatae solid air freshening agent, this method comprises the following steps:
A, prepare homogenate: the branch and leaf of Chinese yew genus plants are pulverized after drying, obtained branch and leaf ground product; Branch and leaf ground product is mixed with suitable quantity of water, then add appropriate non-volatile mineral acid, homogenate after swelling, obtains homogenate;
B, prepare basal liquid: homogenate is passed into steam distillation, and condensation obtains distillation, then by distillation stratification, get the upper oil phase of distillation and part or all of lower floor's water, obtain basal liquid;
C, curing molding: in basal liquid, add gel and antiseptic, mix and be heated to and dissolve completely, obtain liquefied mixture; Pour above-mentioned liquefied mixture in mould cooling forming, after the demoulding, obtain Ramulus et folium taxi cuspidatae solid air freshening agent.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in steps A, described branch and leaf ground product and the mass ratio of water are 1:3-1:6; The addition of described non-volatile mineral acid is the 0.01-1.0% of homogenate gross mass.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in steps A, the branch and leaf of Chinese yew genus plants, through 60-80 DEG C of crushed after being dried, are crossed 50-80 mesh sieve, obtain branch and leaf ground product.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step B, distillation time is 30-240 minute, and the volume 1-5 that the distillation that condensation obtains reaches homogenate stops distillation after doubly; Lower layer of water phase volume in described basal liquid is 20-50 times of upper oil phase volume.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step C, described gel is any one or a few mixture of carrageenan, agar or alginate; Described antiseptic is any one or a few mixture of tween, formaldehyde or benzoic acid.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step C, the addition of described gel is the 1.5-3.5% of liquefied mixture gross weight; The addition of described tween is the 0.5-2.0% of liquefied mixture gross weight; The addition of described formaldehyde is the 0.5-1.5% of liquefied mixture gross weight; The addition of described benzoic acid is the 0.1-1.5% of liquefied mixture gross weight; In described basal liquid, being also added with addition is the Ramulus et folium taxi cuspidatae essence of the 0-1.0% of liquefied mixture gross weight.
In the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, in step C, after being heated to dissolve completely, liquefied mixture is cooled to 50-70 DEG C, more above-mentioned liquefied mixture is poured in mould.
A kind of Ramulus et folium taxi cuspidatae solid air freshening agent making according to the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent.
A manufacture formula for Ramulus et folium taxi cuspidatae solid air freshening agent, this formula comprises the component of following mass fraction: gel 1.5-3.5%; Antiseptic 1.1-5.0%; Ramulus et folium taxi cuspidatae essence 0-1.0%, surplus is basal liquid; Described basal liquid is taken from distillation upper oil phase and the part or all of lower floor water of homogenate, and described homogenate is made up through homogenate of the branch and leaf ground product, water and the non-volatile mineral acid that comprise Chinese yew genus plants branch and leaf.
In the manufacture formula of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent, described branch and leaf ground product and the mass ratio of water are 1:3-1:6, the addition of described non-volatile mineral acid is the 0.01-1.0% of homogenate gross mass, the volume 1-5 that the distillation that condensation obtains reaches homogenate stop after doubly lower layer of water phase volume in distillation and basal liquid be upper oil phase volume 20-50 doubly; Described gel is any one or a few mixture of carrageenan, agar or alginate; Described antiseptic is any one or a few mixture of tween, formaldehyde or benzoic acid, and the addition of described gel accounts for the 1.5-3.5% of this formula gross weight; The addition of described tween accounts for the 0.5-2.0% of this formula gross weight; The addition of described formaldehyde accounts for the 0.5-1.5% of this formula gross weight; The addition of described benzoic acid accounts for the 0.1-1.5% of this formula gross weight; The addition of described Ramulus et folium taxi cuspidatae essence accounts for the 0-1.0% of this formula gross weight.
Compared with prior art, the invention has the advantages that:
1, the present invention has filled up the blank in existing air freshener product type, for it provides extra functional characteristic.
2, utilize this method to produce and contain natural volatile ingredient, there is powerful anti-insomnia, keeping tensions down emotion, effect of tranquillizing and allaying excitement, and have the solid-state air freshener of certain insect-expelling function concurrently.
Detailed description of the invention
Embodiment 1
A manufacture method for Ramulus et folium taxi cuspidatae solid air freshening agent, this method comprises the following steps:
A, prepare homogenate: the branch and leaf of Chinese yew genus plants are pulverized after drying, obtained branch and leaf ground product; Branch and leaf ground product is mixed with suitable quantity of water, then add appropriate non-volatile mineral acid, homogenate after swelling, obtains homogenate;
B, prepare basal liquid: homogenate is passed into steam distillation, and condensation obtains distillation, then by distillation stratification, get the upper oil phase of distillation and part or all of lower floor's water, obtain basal liquid;
C, curing molding: in basal liquid, add gel and antiseptic, mix and be heated to and dissolve completely, obtain liquefied mixture; Pour above-mentioned liquefied mixture in mould cooling forming, after the demoulding, obtain Ramulus et folium taxi cuspidatae solid air freshening agent.
Preferably, in steps A, described branch and leaf ground product and the mass ratio of water are 1:3-1:6, are preferably 1:4, and the addition of described non-volatile mineral acid is the 0.01-1.0% of homogenate gross mass, is preferably 0.5%.
Preferably, in steps A, the branch and leaf of Chinese yew genus plants are through 60-80 DEG C of crushed after being dried, and logical being preferably between 65-70 DEG C is dried, and crosses 50-80 mesh sieve, obtains branch and leaf ground product.
Preferably, in step B, distillation time is 30-240 minute, and the volume 1-5 that the distillation that condensation obtains reaches homogenate stops distillation after doubly; Under normal circumstances, distillation time is determined according to the volume of distillation, in the present embodiment, in the time that distillation volume reaches 3-4 times of homogenate volume, can stop distillation, be considered as distillation complete, in the time that distillation time is 30-240 minute, the lower layer of water phase volume in basal liquid is 20-50 times of upper oil phase volume.
Preferably, in step C, described gel is any one or a few mixture of carrageenan, agar or alginate; Described antiseptic is any one or a few mixture of tween, formaldehyde or benzoic acid.
Tween both can be used as antiseptic, can be used as again surfactant, and profit is more easily mixed, and reached the effect of solubilising, thereby the effective ingredient of Chinese yew genus plants is evenly distributed in water.
Preferably, in step C, the addition of described gel is the 1.5-3.5% of liquefied mixture gross weight; The addition of described tween is the 0.5-2.0% of liquefied mixture gross weight; The addition of described formaldehyde is the 0.5-1.5% of liquefied mixture gross weight; The addition of described benzoic acid is the 0.1-1.5% of liquefied mixture gross weight; In described basal liquid, being also added with addition is the Ramulus et folium taxi cuspidatae essence of the 0-1.0% of liquefied mixture gross weight.
Preferably, in step C, after being heated to dissolve completely, liquefied mixture is cooled to 50-70 DEG C, preferred, be cooled to 60 DEG C, more above-mentioned liquefied mixture is poured in mould.
A kind of Ramulus et folium taxi cuspidatae solid air freshening agent making according to the manufacture method of above-mentioned Ramulus et folium taxi cuspidatae solid air freshening agent.
A manufacture formula for Ramulus et folium taxi cuspidatae solid air freshening agent, this formula comprises the component of following mass fraction: gel 1.5-3.5%; Antiseptic 1.1-5.0%; Ramulus et folium taxi cuspidatae essence 0-1.0%, surplus is basal liquid; Described basal liquid is taken from distillation upper oil phase and the part or all of lower floor water of homogenate, and described homogenate is made up through homogenate of the branch and leaf ground product, water and the non-volatile mineral acid that comprise Chinese yew genus plants branch and leaf.
Preferably, described branch and leaf ground product and the mass ratio of water are 1:3-1:6, preferred, mass ratio is 1:4, the addition of described non-volatile mineral acid is the 0.01-1.0% of homogenate gross mass, preferred, the addition of non-volatile mineral acid is 0.5% of homogenate gross mass, the volume 1-5 that the distillation that condensation obtains reaches homogenate be doubly preferably 3-4 stop after doubly lower layer of water phase volume in distillation and basal liquid be upper oil phase volume 20-50 doubly; Described gel is any one or a few mixture of carrageenan, agar or alginate; Described antiseptic is any one or a few mixture of tween, formaldehyde or benzoic acid, and the addition of described gel accounts for the 1.5-3.5% of this formula gross weight; The addition of described tween accounts for the 0.5-2.0% of this formula gross weight; The addition of described formaldehyde accounts for the 0.5-1.5% of this formula gross weight; The addition of described benzoic acid accounts for the 0.1-1.5% of this formula gross weight; The addition of described Ramulus et folium taxi cuspidatae essence accounts for the 0-1.0% of this formula gross weight.
Above-mentioned non-volatile mineral acid is any one or its mixture of sulphuric acid, phosphoric acid, and wherein sulphuric acid is selected commercially available 98% concentrated sulphuric acid conventionally, and phosphoric acid is selected commercially available 85% phosphoric acid, certainly, after non-volatile mineral acid dilution that also can be above-mentioned, uses.
Embodiment 2-5
The work process of embodiment herein and embodiment 1, operation principle is basic identical, and difference is, at step C, curing molding: the mass number of adding gel and antiseptic in basal liquid is different, refers to following table.
Embodiment 6
The diameter of getting under autumn Mo pruning is Taxus mairei [Taxus chinensis (Pilger) Rehd] branch in 1cm, shady and cool dry place is placed to blade and starts nature and come off, be dried to and can easily fracture through 60 DEG C, subsequently branch is prescinded to little of 3-5cm, pulverize, cross 60 mesh sieves, obtain taxus chinensis powder.Taxus chinensis powder mixes with the blade under coming off, then mixes with the mass ratio of 1:6-1:3 with water, as preferably, in the present embodiment, mixes with the mass ratio of 1:5, adds the phosphoric acid of 1.0wt% in mixed object, leaves standstill and is swelling to without obviously liquid existence, homogenate.After homogenate, through 100 DEG C of steam distillation 240min, collect the distillation in condenser, by distillation stratification.By distillation separatory, get upper oil phase, and volume is the water of the lower floor of 30 times of upper oil phase, obtain basal liquid, in basal liquid, add the benzoic acid of 2.5wt% carrageenan, 1.0wt% tween, 1.0wt% formaldehyde, 0.1wt% and the Ramulus et folium taxi cuspidatae essence of 0-1wt% (Ramulus et folium taxi cuspidatae essence also can not add), being mixed and heated to carrageenan dissolves completely, be cooled to 50 DEG C, pour in the circular grinding tool of preprepared cooling, after solidifying, pour out, pack in the packing box of bag air-vent, obtain Ramulus et folium taxi cuspidatae solid air freshening agent.This product has Ramulus et folium taxi cuspidatae natural flavor, and has tranquillizing and allaying excitement and insect-expelling function.
Specific embodiment described herein is only to the explanation for example of the present invention's spirit.Those skilled in the art can make various amendments or supplement or adopt similar mode to substitute described specific embodiment, but can't depart from spirit of the present invention or surmount the defined scope of appended claims.
Claims (10)
1. a manufacture method for Ramulus et folium taxi cuspidatae solid air freshening agent, is characterized in that, this method comprises the following steps:
A, prepare homogenate: the branch and leaf of Chinese yew genus plants are pulverized after drying, obtained branch and leaf ground product; Branch and leaf ground product is mixed with suitable quantity of water, then add appropriate non-volatile mineral acid, homogenate after swelling, obtains homogenate;
B, prepare basal liquid: homogenate is passed into steam distillation, and condensation obtains distillation, then by distillation stratification, get the upper oil phase of distillation and part or all of lower floor's water, obtain basal liquid;
C, curing molding: in basal liquid, add gel and antiseptic, mix and be heated to and dissolve completely, obtain liquefied mixture; Pour above-mentioned liquefied mixture in mould cooling forming, after the demoulding, obtain Ramulus et folium taxi cuspidatae solid air freshening agent.
2. the manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 1, is characterized in that, in steps A, described branch and leaf ground product and the mass ratio of water are 1:3-1:6; The addition of described non-volatile mineral acid is the 0.01-1.0% of homogenate gross mass.
3. the manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 1, is characterized in that, in steps A, the branch and leaf of Chinese yew genus plants, through 60-80 DEG C of crushed after being dried, are crossed 50-80 mesh sieve, obtain branch and leaf ground product.
4. according to the manufacture method of the Ramulus et folium taxi cuspidatae solid air freshening agent described in claim 1 or 2 or 3, it is characterized in that, in step B, distillation time is 30-240 minute, and the volume 1-5 that the distillation that condensation obtains reaches homogenate stops distillation after doubly; Lower layer of water phase volume in described basal liquid is 20-50 times of upper oil phase volume.
5. according to the manufacture method of the Ramulus et folium taxi cuspidatae solid air freshening agent described in claim 1 or 2 or 3, it is characterized in that, in step C, described gel is any one or a few mixture of carrageenan, agar or alginate; Described antiseptic is any one or a few mixture of tween, formaldehyde or benzoic acid.
6. the manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 5, is characterized in that, in step C, the addition of described gel is the 1.5-3.5% of liquefied mixture gross weight; The addition of described tween is the 0.5-2.0% of liquefied mixture gross weight; The addition of described formaldehyde is the 0.5-1.5% of liquefied mixture gross weight; The addition of described benzoic acid is the 0.1-1.5% of liquefied mixture gross weight; In described basal liquid, being also added with addition is the Ramulus et folium taxi cuspidatae essence of the 0-1.0% of liquefied mixture gross weight.
7. the manufacture method of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 5, is characterized in that, in step C, after being heated to dissolve completely, liquefied mixture is cooled to 50-70 DEG C, more above-mentioned liquefied mixture is poured in mould.
8. the Ramulus et folium taxi cuspidatae solid air freshening agent making according to the manufacture method of the Ramulus et folium taxi cuspidatae solid air freshening agent described in any one in claim 1-7.
9. a manufacture formula for Ramulus et folium taxi cuspidatae solid air freshening agent, is characterized in that, this formula comprises the component of following mass fraction: gel 1.5-3.5%; Antiseptic 1.1-5.0%; Ramulus et folium taxi cuspidatae essence 0-1.0%, surplus is basal liquid; Described basal liquid is taken from distillation upper oil phase and the part or all of lower floor water of homogenate, and described homogenate is made up through homogenate of the branch and leaf ground product, water and the non-volatile mineral acid that comprise Chinese yew genus plants branch and leaf.
10. the manufacture formula of Ramulus et folium taxi cuspidatae solid air freshening agent according to claim 9, it is characterized in that, described branch and leaf ground product and the mass ratio of water are 1:3-1:6, the addition of described non-volatile mineral acid is the 0.01-1.0% of homogenate gross mass, the volume 1-5 that the distillation that condensation obtains reaches homogenate stop after doubly lower layer of water phase volume in distillation and basal liquid be upper oil phase volume 20-50 doubly; Described gel is any one or a few mixture of carrageenan, agar or alginate; Described antiseptic is any one or a few mixture of tween, formaldehyde or benzoic acid, and the addition of described gel accounts for the 1.5-3.5% of this formula gross weight; The addition of described tween accounts for the 0.5-2.0% of this formula gross weight; The addition of described formaldehyde accounts for the 0.5-1.5% of this formula gross weight; The addition of described benzoic acid accounts for the 0.1-1.5% of this formula gross weight; The addition of described Ramulus et folium taxi cuspidatae essence accounts for the 0-1.0% of this formula gross weight.
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| CN105087165A (en) * | 2015-09-18 | 2015-11-25 | 哈尔滨红豆杉科技开发有限责任公司 | Composite essential oil prepared from taxus cuspidata and coniferous plants and application of composite essential oil |
| CN107581568A (en) * | 2017-10-20 | 2018-01-16 | 天津商业大学 | One kind solidification paste essence |
| CN108379639A (en) * | 2018-05-02 | 2018-08-10 | 湖北祥瑞丰红豆杉科技股份有限公司 | A kind of air freshener and preparation method thereof |
| CN108524331A (en) * | 2018-05-02 | 2018-09-14 | 湖北祥瑞丰红豆杉科技股份有限公司 | A kind of Chinese yew solid perfume and preparation method thereof |
| CN112336901A (en) * | 2020-11-10 | 2021-02-09 | 湖北物莫生物科技有限公司 | Natural essential oil solid freshener and preparation process thereof |
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| CN112336901A (en) * | 2020-11-10 | 2021-02-09 | 湖北物莫生物科技有限公司 | Natural essential oil solid freshener and preparation process thereof |
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| CN103877602B (en) | 2017-05-03 |
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