CN110029022A - Solid plant essential oil of sustained release and preparation method thereof - Google Patents
Solid plant essential oil of sustained release and preparation method thereof Download PDFInfo
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- CN110029022A CN110029022A CN201910336320.7A CN201910336320A CN110029022A CN 110029022 A CN110029022 A CN 110029022A CN 201910336320 A CN201910336320 A CN 201910336320A CN 110029022 A CN110029022 A CN 110029022A
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- essential oil
- oil
- plant essential
- sustained release
- cerul
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses solid plant essential oil of a kind of sustained release and preparation method thereof, the solid plant essential oil of the sustained release includes natural polymer resin, cerul, oil base, liquid plant essential oil and volatilization auxiliary agent.The preparation method prepares solid essential oil by hot thawing method, and a certain amount of corn alcohol is added during the preparation process to reach sustained release purpose.Character form is good after the solid essential oil agent solidification of sustained release prepared by the present invention, and it is slow that essential oil discharges more original liquid essential oil, and essential oil residual volume is high, is suitble to prepare slow release type essential oil.
Description
Technical field
The present invention relates to a kind of chemicals and preparation method thereof more particularly to the solid plant essential oils and its system of a kind of sustained release
Preparation Method.
Background technique
Common plants essential oil is a kind of pure natural botanical extract mixture, and ingredient is complex.It at normal temperature, is easy
Volatilization, mostly liquid condition, specific gravity are soluble in the lesser organic solvent of polarity in 0.85-1.065g/mL.
The manufacturing method of plants essential oil has very much, common are the way of distillation, rouge inhales method and compression method.Wherein the way of distillation is most
Ancient method and most widely used, it is in a reservoir to be heated plant with water, evaporates vapor, produces mixed
Close the concentrate of oil and water.Due to density difference, oil and water can be separated, therefore can prepare essential oil.It is in frame that rouge, which inhales method,
On put one block of glass, then apply one layer of fat, then spread the plant of picking, stand a whole day, then fat can absorb plant
Essential oil in object, then in turn by frame, plant another side is fallen on another side frame, continues to absorb essential oil, repeatedly,
Essential oil is created.Compression method is directly to squeeze mature plant to sponge, then carry out recycling manufacture.
Plants essential oil is widely used in fields such as medicine, food and daily use chemicals.In terms of medicine, the essence that is extracted from elscholtiza
Oil has antibiotic property, can be used for treating some diseases (such as dysentery, gastroenteritis and influenza)；Peppermint oil have analgesic, it is refrigerant, disappear
Scorching and antipruritic effect.It can be used as food additives in the food industry, for changing food odors, increase food flavors.
In addition, plants essential oil can also be used in the fresh-keeping of fruits and vegetables, as the bactericidal activity of rutaceae Chinese parasol leaf oil becomes fruit
The desirable feedstock of preservative.In addition, vetiver oil, caryophyllus oil, lavender oil and cinnamon leaves oil etc. also have to nectarine bud it is good
Fresh-keeping effect.For a long time, natural plant essential oils are one of raw materials of daily chemical products, in order to increase the glamour of chemical product, people
Natural plant essential oils ingredient is often added in formula, makes it have unique fragrance.Common vegetalitas essential oil in chemical product
Including fennel oil, eucalyptus oil, cassia oil, white orchid oil, refined jasmine oil and Rosa Damascana etc..
But the volatility of plants essential oil is very strong, once ingress of air will volatilize quickly, also based on this reason, plants
Object essential oil is commonly stored in the dark-colored bottle of sealing.In addition, plants essential oil is exposed to meeting under the air and sunlight of certain temperature
Occur rotten.Therefore, the limit value use scope of plants essential oil to a certain extent.
Summary of the invention
The purpose of the present invention is volatile to solve current plants essential oil, condition of storage is limited and exposure is variable in air
The technical issues of matter.
In order to solve the above-mentioned technical problem, in a first aspect, the present invention provides a kind of solid plant essential oil of sustained release, including day
Right macromolecule resin, cerul, oil base, liquid plant essential oil and volatilization auxiliary agent；Wherein, the natural polymer resin and described
The mass ratio of cerul is 1-5:4-1；The additive amount of the oil base is the 1/9 of the natural polymer resin and cerul gross mass；
The additive amount of the volatilization auxiliary agent is the 20%-40% of the natural polymer resin, cerul and oil base gross mass；The liquid
The additive amount of plants essential oil is the 10%-30% of the natural polymer resin, cerul, oil base and auxiliary agent gross mass of volatilizing.
Further, the mass ratio of the natural polymer resin and the cerul is 5:4, this is selected to consolidate than what column obtained
Loss amount is minimum in the curing process for body sample, and tiny holes existing for the surface after solidifying can make essential oil enduringly
It evaporates.
Further, the additive amount of the volatilization auxiliary agent is the natural polymer resin, cerul and oil base gross mass
30%, the solid product form obtained at this time is best, and face crack is less.
Further, the additive amount of the liquid plant essential oil is the natural polymer resin, cerul, oil base and volatilization
The 25% of auxiliary agent gross mass is higher than the content, volatilizees too fast, and higher cost, is lower than this content, and slow release effect is unobvious.
Further, the natural polymer resin is gum dammar.Gum dammar is cheap compared with other resin prices, and
The surface arrived is flawless.
Further, the cerul is cera alba.Cera alba is one kind of natural bee product, is that one kind can be widely applied to
The natural materials of medical field, it is non-hazardous to human body.
Further, the oil base is palm oil.Palm oil is a kind of tropical xylophyta oil, what more other chemical industry used
Oil source is more green.
Further, the volatilization auxiliary agent is corn alcohol.Corn alcohol is more extensive compared with grain alcohol raw material sources, price
Cheaply.
Further, the liquid plant essential oil is Rosa Damascana.Rosa Damascana is referred to as " after essential oil ", is pure natural
Plants essential oil, fragrant；Can anti-inflammation and sterilization, can anti-communicable disease, anti-inflammation, anti-spasm promotes cell metabolism and cell
Regeneration；It is adjustable endocrine organ, promotes hormone secretion, promotes the sexual maturity, mends body, allows the physiology of human body and psychological activity to obtain good
Development；It can be suitably used for various skins, the characteristic for playing consolidation, releiving, nourishes rough skin delays senescence.
Second aspect, the present invention provide a kind of preparation method of the solid plant essential oil of sustained release, comprising the following steps:
(1) the gum dammar powder that balance weighs a certain amount of crushing is placed on heated at constant temperature blender into culture dish,
Melt to gum dammar；
(2) a certain amount of cera alba is added in the gum dammar of the melting of above-mentioned steps (1), is stirred with glass bar to white
Beeswax melts completely；
(3) a certain amount of palm oil is continuously added in the mixture of above-mentioned steps (2) melting, be sufficiently stirred, to palm
Stop heating after oily thawing completely；
(4) a certain amount of corn alcohol is added in the mixture of above-mentioned steps (3), continues to stir；
(5) under agitation, a certain amount of liquid plant essential oil is added into above-mentioned steps (4) mixture, in room temperature
It is lower to stand the solid plant essential oil for being frozen into sustained release.
Further, further comprising the steps of:
(6) the solid plant essential oil by the standing solidification that step (5) obtains records data, Zong Gongji every weighing in three days
Record 15 days calculates weight-loss ratio.
The present invention prepares solid essential oil by hot thawing method, a certain amount of corn alcohol is added during the preparation process to reach
It is sustained purpose, character form is good after the solid essential oil agent solidification of the sustained release of preparation, and the more original liquid essential oil of essential oil release is slow,
And essential oil residual volume is high, is suitble to prepare slow release type essential oil.
Specific embodiment
Presently in connection with embodiment, the present invention is described in further detail, and application of the invention is not limited to following
Embodiment, the accommodation in any form done to the present invention fall within protection scope of the present invention.
Preparation method embodiment 1
The gum dammar powder 10g crushed in advance is weighed into culture dish, is placed on heating stirrer and heats, until reaching Ma tree
It after rouge melts, then weighs the addition of 8g cera alba and melts and have in gum dammar culture dish, stirred with glass bar to cera alba and melted completely,
Claim 2g palm oil to be added again, be sufficiently stirred again after palm oil melts completely, reaches mixture fusion uniformly, add 5g later
(the 25% of sample gross mass) Rosa Damascana, at room temperature cooling and standings, the essential oil after solidification are labeled as A.Every three days title samples
Quality, record data, continuous record 15 days, and calculate weight-loss ratio.
Quality × 100% of weight-loss ratio=(quality after quality-placement when just preparing)/just when preparing.
Preparation method embodiment 2
The gum dammar powder 10g crushed in advance is weighed into culture dish, is placed on heating stirrer and heats, until reaching Ma tree
It after rouge melts, then weighs the addition of 8g cera alba and melts and have in gum dammar culture dish, stirred with glass bar to cera alba and melted completely,
Claim 2g palm oil to be added again, be sufficiently stirred again after palm oil melts completely, reaches mixture fusion uniformly, mixture is placed in
Under room temperature, the corn alcohol of 6g is added, after being sufficiently stirred, 6.5g (the 25% of sample gross mass) Rosa Damascana is added, at room temperature
Cooling and standings, the essential oil after solidification are labeled as B.The quality for claiming sample every three days records data, continuous record 15 days, and counts
Calculate weight-loss ratio.
Add the degree of volatility of 25% content essential oil in 1 gum dammar of table+cera alba+palm oil combination
Add the degree of volatility of 25% content essential oil in 2 gum dammars of table+cera alba+palm oil+alcohol combination
The data of Tables 1 and 2 are analyzed it is found that first, Rosa Damascana is all smaller in 15 days volatile quantities, second, addition
15 days weight-loss ratios after corn alcohol are higher than the weight-loss ratio without adding corn alcohol, further illustrate that corn alcohol is certain
It can achieve the purpose for helping volatilizer.Specifically, the present invention it is to be prepared be a kind of slow release solid essential oil, and it is simple
Liquid essential oil is volatilized too fast in air；If corn alcohol is not added, although also there is weightlessness, effect is unobvious, has added jade
After rice wine essence, one side solid essential oil than it is simple be not added alcohol when rate of release it is fast, on the other hand, released than liquid essential oil
It is slow to put rate, reaches sustained release purpose.
Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.
Claims (10)
1. the solid plant essential oil of sustained release, which is characterized in that including natural polymer resin, cerul, oil base, liquid plant essential oil
And volatilization auxiliary agent；
Wherein, the mass ratio of the natural polymer resin and the cerul is 1-5:4-1；The additive amount of the oil base is described
The 1/9 of natural polymer resin and cerul gross mass；The additive amount of the volatilization auxiliary agent is the natural polymer resin, cerul
With the 20%-40% of oil base gross mass；The additive amount of the liquid plant essential oil is the natural polymer resin, cerul, oil
The 10%-30% of base and volatilization auxiliary agent gross mass.
2. the solid plant essential oil of sustained release according to claim 1, which is characterized in that the natural polymer resin and institute
The mass ratio for stating cerul is 5:4.
3. the solid plant essential oil of sustained release according to claim 1, which is characterized in that it is described volatilization auxiliary agent additive amount be
The 30% of the natural polymer resin, cerul and oil base gross mass.
4. the solid plant essential oil of sustained release according to claim 1, which is characterized in that the addition of the liquid plant essential oil
Amount is the 25% of the natural polymer resin, cerul, oil base and volatilization auxiliary agent gross mass.
5. the solid plant essential oil of sustained release according to claim 1, which is characterized in that the natural polymer resin be up to
Saqima resin；The volatilization auxiliary agent is corn alcohol.
6. the solid plant essential oil of sustained release according to claim 1, which is characterized in that the cerul is cera alba.
7. the solid plant essential oil of sustained release according to claim 1, which is characterized in that the oil base is palm oil.
8. the solid plant essential oil of sustained release according to claim 1, which is characterized in that the liquid plant essential oil is rose
Essential oil.
9. the preparation method of the solid plant essential oil of sustained release, which comprises the following steps:
(1) the gum dammar powder that balance weighs a certain amount of crushing is placed on heated at constant temperature blender into culture dish, until reaching
Saqima resin melts；
(2) a certain amount of cera alba is added in the gum dammar of the melting of above-mentioned steps (1), is stirred with glass bar to cera alba
Melt completely；
(3) a certain amount of palm oil is continuously added in the mixture of above-mentioned steps (2) melting, be sufficiently stirred, it is complete to palm oil
Stop heating after full thawing；
(4) a certain amount of corn alcohol is added in the mixture of above-mentioned steps (3), continues to stir；
(5) under agitation, a certain amount of liquid plant essential oil is added into above-mentioned steps (4) mixture, it is quiet at room temperature
Set the solid plant essential oil for being frozen into sustained release.
10. preparation method according to claim 9, which is characterized in that further comprising the steps of:
(6) the solid plant essential oil by the standing solidification that step (5) obtains records data every weighing in three days, records 15 in total
It, calculates weight-loss ratio.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910336320.7A CN110029022A (en) | 2019-04-24 | 2019-04-24 | Solid plant essential oil of sustained release and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910336320.7A CN110029022A (en) | 2019-04-24 | 2019-04-24 | Solid plant essential oil of sustained release and preparation method thereof |
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| CN110029022A true CN110029022A (en) | 2019-07-19 |
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| CN201910336320.7A Pending CN110029022A (en) | 2019-04-24 | 2019-04-24 | Solid plant essential oil of sustained release and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113041283A (en) * | 2019-12-27 | 2021-06-29 | 宁波芬缘香薰制品有限公司 | External solid essential oil for skin for refreshing and restoring consciousness and preparation method thereof |
| CN113041297A (en) * | 2019-12-27 | 2021-06-29 | 宁波芬缘香薰制品有限公司 | Digestion-promoting solid essential oil for external use on skin and preparation method thereof |
| CN116270906A (en) * | 2023-01-06 | 2023-06-23 | 山东益得来生物科技有限公司 | Jerusalem artichoke flower compound solid essential oil for assisting in improving memory and preparation method thereof |
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Patent Citations (5)
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113041283A (en) * | 2019-12-27 | 2021-06-29 | 宁波芬缘香薰制品有限公司 | External solid essential oil for skin for refreshing and restoring consciousness and preparation method thereof |
| CN113041297A (en) * | 2019-12-27 | 2021-06-29 | 宁波芬缘香薰制品有限公司 | Digestion-promoting solid essential oil for external use on skin and preparation method thereof |
| CN116270906A (en) * | 2023-01-06 | 2023-06-23 | 山东益得来生物科技有限公司 | Jerusalem artichoke flower compound solid essential oil for assisting in improving memory and preparation method thereof |
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Application publication date: 20190719 |