CN106823678A - A kind of attapulgite sterilization deodorant and preparation method - Google Patents
A kind of attapulgite sterilization deodorant and preparation method Download PDFInfo
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Abstract
The invention discloses a kind of attapulgite sterilization deodorant and preparation method, belong to attapulgite technical field.The deodorant includes following component：Concave-convex clay rod, shale diatom ooze, folium artemisiae argyi, rhizoma atractylodis, Dalmatian chrysanthemum, Radix Glycyrrhizae, Kadsura Root-bark, crotons, calamus, the root bark of tree peony, frutus cnidii, sweet wormwood, caryophyllus oil, tea tree ethereal oil, Peppermint essential oil.Preparation method includes：Take herbal component broken and mix, obtain Traditional Chinese drug mixture；It is placed in apparatus,Soxhlet's, is extracted in the mixed solvent of second alcohol and water, obtains extract solution；Then heat modification Concave-convex clay rod is prepared；The Concave-convex clay rod after heat modification is placed in extract solution again, adds caryophyllus oil, tea tree ethereal oil and Peppermint essential oil, soaked under stirring condition, added shale diatom ooze and be well mixed, dried, grind, you can.Deodorant of the present invention not only has dynamical sterilized, deodorization, but with long service life, and preparation method is simple and easy to apply, with preferable application value.
Description
Technical field
The present invention relates to attapulgite technical field, and in particular to a kind of attapulgite sterilization deodorant and preparation method.
Background technology
With the continuous improvement of people's living standard, requirement of the people to living environment also more and more higher, and surrounding enviroment
Inevitably there is some bacteriums, the hyperplasia of mould, or even have foul odour, such as in automobile, hospital, kitchen, hotel,
The special occasions such as sewage treatment plant, slaughterhouse, penkeeping field, pharmaceutical factory, and it is adapted to both Nantural non-toxics of these special occasions
The preparation of energy deodorization and sterilization is seldom shown in again.The function of the air freshener that in the market is sold also is only capable of temporarily covering stink.Additionally,
Can also be disturbed by bacterium, mould constantly in the living environment of people itself, such as food, seafood, the fish deposited in refrigerator
Meat products overlong time, due to the effect of bacterium, can decompose protein denaturization, fat rancidity, amino acid, produce methylamine, three
Methylamine, first sulphur ferment, histamine, two dislike the foul smell such as pharynx, hydrogen sulfide.Deal with improperly and have a large amount of moulds tastes in the humidity place such as toilet
It is raw.Although eliminating foul smell, smelly source existing many preparations and bactericide being controlled, because its main component is all synthetics
Product, harmful, what is had is also poisonous.So, it is impossible in the occasion to having environmental sanitation and non-toxicity requirements, food and human body
A little the sterilized and deodorant of position are promoted the use of.It is the deodorant with suction-operated to also have a kind of deodorant on the market, is mostly
Activated carbon, but treatment effect is not obvious, and service life is shorter, does not also have bactericidal action, it is narrower using scope.
Therefore, researching and developing one kind had both had preferably sterilized, deodorization, and with long service life, and will not
The reagent damaged to human body is significant, it may have preferable application prospect and use value.
The content of the invention
For defect of the prior art, it is an object of the invention to provide a kind of attapulgite sterilization deodorant and preparation side
Method, the attapulgite sterilization deodorant not only has dynamical sterilized, deodorization, and with long service life, and
Raw material of the present invention uses natural material, also with green non-pollution the characteristics of, human body will not be damaged, be people's
Healthy living is provided and ensured.Additionally, the preparation method is simple and easy to apply, with preferable application value.
The present invention solves technical problem and adopts the following technical scheme that：
The present invention relates to a kind of attapulgite sterilization deodorant, including following parts by weight each component：Concave-convex clay rod 70 ~
90 parts, 5 ~ 15 parts of shale diatom ooze, 10 ~ 20 parts of folium artemisiae argyi, 5 ~ 10 parts of rhizoma atractylodis, 5 ~ 10 parts of Dalmatian chrysanthemum, 5 ~ 15 parts of Radix Glycyrrhizae, Kadsura Root-bark 5 ~
10 parts, 5 ~ 10 parts of crotons, 10 ~ 20 parts of calamus, 10 ~ 30 parts of the root bark of tree peony, 5 ~ 10 parts of frutus cnidii, 5 ~ 15 parts of sweet wormwood, 3 ~ 8 parts of caryophyllus oil,
3 ~ 8 parts of tea tree ethereal oil, 3 ~ 5 parts of Peppermint essential oil, also including appropriate solvent.
Preferably, 80 parts of the Concave-convex clay rod, 10 parts of shale diatom ooze, 15 parts of folium artemisiae argyi, 8 parts of rhizoma atractylodis, Dalmatian chrysanthemum 8
Part, 10 parts of Radix Glycyrrhizae, 8 parts of Kadsura Root-bark, 8 parts of crotons, 15 parts of calamus, 20 parts of the root bark of tree peony, 8 parts of frutus cnidii, 10 parts of sweet wormwood, 5 parts of caryophyllus oil,
5 parts of tea tree ethereal oil, 3 parts of Peppermint essential oil.
Preferably, the Concave-convex clay rod is the Concave-convex clay rod after heat modification.
Preferably, the solvent includes second alcohol and water.
The invention further relates to a kind of method for preparing attapulgite sterilization deodorant, comprise the following steps：
（1）Folium artemisiae argyi, rhizoma atractylodis, Dalmatian chrysanthemum, Radix Glycyrrhizae, Kadsura Root-bark, crotons, calamus, the root bark of tree peony, frutus cnidii, green grass or young crops are weighed respectively according to proportioning
Wormwood artemisia, crushes and mixes, and obtains Traditional Chinese drug mixture；
（2）Traditional Chinese drug mixture is placed in apparatus,Soxhlet's, 3 ~ 5h of extraction is carried out in the mixed solvent of second alcohol and water, extract knot
Shu Hou, obtains extract solution, standby；
（3）Natural attapulgite clay is carried out to be crushed to 100 ~ 200 mesh, is added water, stirring forms mud in suspension, then by ultrasound
After fully dispersed, upper suspension 5 ~ 10min of centrifugal treating in the centrifuge of 3000 turns/min, vacuum filtration after standing are taken；
Filter cake is placed in beaker, ethanol is added, in 10 ~ 20min of ultrasound, vacuum filtration after standing under Ultrasonic Conditions, is dried to obtain
Concave-convex clay rod pretreatment product；
（4）500 DEG C ~ 800 DEG C of Muffle 1 ~ 2h of kiln roasting is placed in after Concave-convex clay rod pretreatment product is dried, after cooling
Particle diameter is ground to for 100 ~ 200 mesh, the Concave-convex clay rod after heat modification is obtained final product；
（5）Concave-convex clay rod after heat modification is placed in extract solution, then according to proportioning add caryophyllus oil, tea tree ethereal oil and
Peppermint essential oil, soaks 10 ~ 12h under stirring condition, after terminating, add shale diatom ooze to be well mixed, and dries, then by solids
Matter is ground to 100 ~ 200 mesh, obtains final product the attapulgite sterilization deodorant.
Preferably, the step（1）In be crushed to particle diameter for 100 ~ 200 mesh.
Preferably, the step（2）The volume of middle addition mixed solvent is 5 ~ 10 times of each traditional Chinese medicinal components quality, wherein
Ethanol is 1 with the volume ratio of water:0.5~2：1 so that the traditional Chinese medicine ingredients that Concave-convex clay rod can be in quick adsorption extract solution, keep away
Exempt from, due to the insufficient phenomenon generation of the too dilute caused absorption of concentration, to cause its bactericidal effect to weaken.
Preferably, the step（2）In extract solution be Concave-convex clay rod mixing before need first concentration, be concentrated into
The volume of extract solution is 3 ~ 5 times of Concave-convex clay rod quality.
Preferably, the step（5）In drying steps include：Mixture is first placed in rotary evaporation in Rotary Evaporators
Solvent is removed, solid matter is placed in vacuum drying chamber again then and is dried, you can.
Compared with prior art, the present invention has following beneficial effect：
（1）Attapulgite sterilization deodorant of the present invention not only has dynamical sterilized, deodorization, and makes with more long
With the life-span, and raw material of the present invention uses natural material, also with green non-pollution the characteristics of, wound will not be caused to human body
Evil, for the healthy living of people provides guarantee.Additionally, the preparation method is simple and easy to apply, with preferable application value.
（2）Attapulgite sterilization deodorant of the present invention uses Concave-convex clay rod as base material, due to concave convex rod
Stone clay has layer chain structure, and viscosity is shown when moist, there is plasticity, and it is few to dry after-contraction, and cracking is not produced.Water imbibition is strong,
Chemical property is sufficiently stable, also has functions that sterilizing, deodorant, desinsection, detoxification, is the deodorization and sterilization of bactericidal deodorant of the present invention
Effect is provided and ensured, additionally, Concave-convex clay rod has superpower adsorption capacity, can effectively absorb the evil in surrounding environment
Odour, plays efficient deodorizing effect.
（3）The present invention is ensured using several kinds of Chinese medicinal materials combination Concave-convex clay rod double sterilization so that what is prepared kills
Bacterium deodorant has excellent bactericidal action, along with the presence of shale diatom ooze causes that preparation has preferable mould-proof bacteria-removing
Effect.
Specific embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1：
A kind of attapulgite sterilization deodorant and preparation method of the preferred embodiment of the present invention；
The attapulgite sterilization deodorant, is prepared from by each component of following parts by weight：Concave-convex clay rod 80 part, page
10 parts of rock diatom ooze, 15 parts of folium artemisiae argyi, 8 parts of rhizoma atractylodis, 8 parts of Dalmatian chrysanthemum, 10 parts of Radix Glycyrrhizae, 8 parts of Kadsura Root-bark, 8 parts of crotons, 15 parts of calamus,
20 parts of the root bark of tree peony, 8 parts of frutus cnidii, 10 parts of sweet wormwood, 5 parts of caryophyllus oil, 5 parts of tea tree ethereal oil, 3 parts of Peppermint essential oil.
Wherein, the Concave-convex clay rod is the Concave-convex clay rod after heat modification, and the solvent includes second alcohol and water.
The preparation method of the attapulgite sterilization deodorant, comprises the following steps：
（1）Folium artemisiae argyi, rhizoma atractylodis, Dalmatian chrysanthemum, Radix Glycyrrhizae, Kadsura Root-bark, crotons, calamus, the root bark of tree peony, frutus cnidii, green grass or young crops are weighed respectively according to proportioning
Wormwood artemisia, is crushed to particle diameter for 200 mesh and mixes, and obtains Traditional Chinese drug mixture；
（2）Traditional Chinese drug mixture is placed in apparatus,Soxhlet's, 3 ~ 5h of extraction is carried out in the mixed solvent of second alcohol and water, extract knot
Shu Hou, obtains extract solution, standby, wherein, the volume for adding mixed solvent is 5 ~ 10 times of each traditional Chinese medicinal components quality, wherein ethanol
It is 1 with the volume ratio of water:0.5；
（3）Natural attapulgite clay is carried out to be crushed to 200 mesh, is added water, stirring forms mud in suspension, then by ultrasonic abundant
After dispersion, upper suspension centrifugal treating 8min in the centrifuge of 3000 turns/min, vacuum filtration after standing are taken；Filter cake is put
In beaker, ethanol is added, in ultrasonic 15 min, vacuum filtration after standing under Ultrasonic Conditions, be dried to obtain attapulgite and glue
Native pretreatment product；
（4）600 DEG C of the h of Muffle kiln roasting 2 is placed in after Concave-convex clay rod pretreatment product is dried, is ground to after cooling
Particle diameter is 200 mesh, obtains final product the Concave-convex clay rod after heat modification；
（5）Concave-convex clay rod after heat modification is placed in extract solution, then according to proportioning add caryophyllus oil, tea tree ethereal oil and
10 h are soaked under Peppermint essential oil, stirring condition, after terminating, adds shale diatom ooze to be well mixed, dried, then by solid matter
200 mesh are ground to, the attapulgite sterilization deodorant is obtained final product.
Step（2）In extract solution be Concave-convex clay rod mixing before need first concentration, be concentrated into the body of extract solution
Product is 5 times of Concave-convex clay rod quality so that the traditional Chinese medicine ingredients that Concave-convex clay rod can be in quick adsorption extract solution, it is to avoid
Because the insufficient phenomenon of the too dilute caused absorption of concentration occurs, its bactericidal effect is caused to weaken.
Step（5）In drying steps include：Mixture is first placed in rotary evaporation in Rotary Evaporators and removes solvent, so
Solid matter is placed in vacuum drying chamber again afterwards and is dried, you can.
Embodiment 2：
A kind of attapulgite sterilization deodorant and preparation method of the preferred embodiment of the present invention；
Attapulgite sterilization deodorant, is prepared from by each component of following parts by weight：70 parts of Concave-convex clay rod, shale silicon
5 parts of algae mud, 10 parts of folium artemisiae argyi, 5 parts of rhizoma atractylodis, 5 parts of Dalmatian chrysanthemum, 5 parts of Radix Glycyrrhizae, 5 parts of Kadsura Root-bark, 5 parts of crotons, 10 parts of calamus, the root bark of tree peony 10
Part, 5 parts of frutus cnidii, 5 parts of sweet wormwood, 3 parts of caryophyllus oil, 3 parts of tea tree ethereal oil, 3 parts of Peppermint essential oil, also including appropriate solvent.
Wherein, the Concave-convex clay rod is the Concave-convex clay rod after heat modification, and the solvent includes second alcohol and water.
The preparation method of attapulgite sterilization deodorant, comprises the following steps：
（1）Folium artemisiae argyi, rhizoma atractylodis, Dalmatian chrysanthemum, Radix Glycyrrhizae, Kadsura Root-bark, crotons, calamus, the root bark of tree peony, frutus cnidii, green grass or young crops are weighed respectively according to proportioning
Wormwood artemisia, is crushed to particle diameter for 100 mesh and mixes, and obtains Traditional Chinese drug mixture；
（2）Traditional Chinese drug mixture is placed in apparatus,Soxhlet's, carries out extracting 3 h in the mixed solvent of second alcohol and water, extract knot
Shu Hou, obtains extract solution, standby, wherein, the volume for adding mixed solvent is 5 times of each traditional Chinese medicinal components quality, wherein ethanol with
The volume ratio of water is 1: 1；
（3）Natural attapulgite clay is carried out to be crushed to 100 mesh, is added water, stirring forms mud in suspension, then by ultrasonic abundant
After dispersion, upper suspension min of centrifugal treating 5 in the centrifuge of 3000 turns/min, vacuum filtration after standing are taken；By filter cake
It is placed in beaker, adds ethanol, in ultrasonic 10 min, vacuum filtration after standing under Ultrasonic Conditions, is dried to obtain attapulgite
Clay pretreatment product；
（4）500 DEG C of Muffle kiln roasting 2h is placed in after Concave-convex clay rod pretreatment product is dried, grain is ground to after cooling
Footpath is 100 mesh, obtains final product the Concave-convex clay rod after heat modification；
（5）Concave-convex clay rod after heat modification is placed in extract solution, then according to proportioning add caryophyllus oil, tea tree ethereal oil and
10 h are soaked under Peppermint essential oil, stirring condition, after terminating, adds shale diatom ooze to be well mixed, dried, then by solid matter
100 mesh are ground to, the attapulgite sterilization deodorant is obtained final product.
Step（2）In extract solution be Concave-convex clay rod mixing before need first concentration, be concentrated into the body of extract solution
Product is 3 times of Concave-convex clay rod quality.Enable the traditional Chinese medicine ingredients in Concave-convex clay rod quick adsorption extract solution, it is to avoid
Because the insufficient phenomenon of the too dilute caused absorption of concentration occurs, its bactericidal effect is caused to weaken.
Step（5）In drying steps include：Mixture is first placed in rotary evaporation in Rotary Evaporators and removes solvent, so
Solid matter is placed in vacuum drying chamber again afterwards and is dried, you can.
Embodiment 3：
A kind of attapulgite sterilization deodorant and preparation method of the preferred embodiment of the present invention；
Attapulgite sterilization deodorant, is prepared from by each component of following parts by weight：90 parts of Concave-convex clay rod, shale silicon
15 parts of algae mud, 20 parts of folium artemisiae argyi, 10 parts of rhizoma atractylodis, 10 parts of Dalmatian chrysanthemum, 15 parts of Radix Glycyrrhizae, 10 parts of Kadsura Root-bark, 10 parts of crotons, 20 parts of calamus,
30 parts of the root bark of tree peony, 10 parts of frutus cnidii, 15 parts of sweet wormwood, 8 parts of caryophyllus oil, 8 parts of tea tree ethereal oil, 5 parts of Peppermint essential oil, also including appropriate molten
Agent.
Wherein, the Concave-convex clay rod is the Concave-convex clay rod after heat modification, and the solvent includes second alcohol and water.
The preparation method of attapulgite sterilization deodorant, comprises the following steps：
（1）Folium artemisiae argyi, rhizoma atractylodis, Dalmatian chrysanthemum, Radix Glycyrrhizae, Kadsura Root-bark, crotons, calamus, the root bark of tree peony, frutus cnidii, green grass or young crops are weighed respectively according to proportioning
Wormwood artemisia, is crushed to particle diameter for 200 mesh and mixes, and obtains Traditional Chinese drug mixture；
（2）Traditional Chinese drug mixture is placed in apparatus,Soxhlet's, extraction 5h is carried out in the mixed solvent of second alcohol and water, extraction terminates
Afterwards, extract solution is obtained, it is standby, wherein, the volume for adding mixed solvent is 10 times of each traditional Chinese medicinal components quality, wherein ethanol and water
Volume ratio be 2：1；
（3）Natural attapulgite clay is carried out to be crushed to 200 mesh, is added water, stirring forms mud in suspension, then by ultrasonic abundant
After dispersion, upper suspension centrifugal treating 10min in the centrifuge of 3000 turns/min, vacuum filtration after standing are taken；By filter cake
It is placed in beaker, adds ethanol, in ultrasound 20min, vacuum filtration after standing under Ultrasonic Conditions, is dried to obtain attapulgite and glues
Native pretreatment product；
（4）800 DEG C of Muffle kiln roasting 1h is placed in after Concave-convex clay rod pretreatment product is dried, grain is ground to after cooling
Footpath is 200 mesh, obtains final product the Concave-convex clay rod after heat modification；
（5）Concave-convex clay rod after heat modification is placed in extract solution, then according to proportioning add caryophyllus oil, tea tree ethereal oil and
12h is soaked under Peppermint essential oil, stirring condition, after terminating, adds shale diatom ooze to be well mixed, dried, then by solid matter
200 mesh are ground to, the attapulgite sterilization deodorant is obtained final product.
Step（2）In extract solution be Concave-convex clay rod mixing before need first concentration, be concentrated into the body of extract solution
Product is 5 times of Concave-convex clay rod quality.Enable the traditional Chinese medicine ingredients in Concave-convex clay rod quick adsorption extract solution, it is to avoid
Because the insufficient phenomenon of the too dilute caused absorption of concentration occurs, its bactericidal effect is caused to weaken.
Step（5）In drying steps include：Mixture is first placed in rotary evaporation in Rotary Evaporators and removes solvent, so
Solid matter is placed in vacuum drying chamber again afterwards and is dried, you can.
In sum, the prepared attapulgite sterilization deodorant of the present invention not only has dynamical sterilized, deodorization,
There is long service life again, and raw material of the present invention uses natural material, also with green non-pollution the characteristics of, will not be right
Human body is damaged, for the healthy living of people provides guarantee.Additionally, the preparation method is simple and easy to apply, with preferable
Application value.
Specific embodiment of the invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can within the scope of the claims make various deformations or amendments, this not shadow
Sound substance of the invention.
Claims (9)
1. a kind of attapulgite sterilization deodorant, it is characterised in that：Each component including following parts by weight：Concave-convex clay rod
70 ~ 90 parts, 5 ~ 15 parts of shale diatom ooze, 10 ~ 20 parts of folium artemisiae argyi, 5 ~ 10 parts of rhizoma atractylodis, 5 ~ 10 parts of Dalmatian chrysanthemum, 5 ~ 15 parts of Radix Glycyrrhizae, cercis
5 ~ 10 parts of skin, 5 ~ 10 parts of crotons, 10 ~ 20 parts of calamus, 10 ~ 30 parts of the root bark of tree peony, 5 ~ 10 parts of frutus cnidii, 5 ~ 15 parts of sweet wormwood, caryophyllus oil 3 ~ 8
Part, 3 ~ 8 parts of tea tree ethereal oil, 3 ~ 5 parts of Peppermint essential oil, also including appropriate solvent.
2. attapulgite sterilization deodorant according to claim 1, it is characterised in that：80 parts of the Concave-convex clay rod,
10 parts of shale diatom ooze, 15 parts of folium artemisiae argyi, 8 parts of rhizoma atractylodis, 8 parts of Dalmatian chrysanthemum, 10 parts of Radix Glycyrrhizae, 8 parts of Kadsura Root-bark, 8 parts of crotons, calamus 15
Part, 20 parts of the root bark of tree peony, 8 parts of frutus cnidii, 10 parts of sweet wormwood, 5 parts of caryophyllus oil, 5 parts of tea tree ethereal oil, 3 parts of Peppermint essential oil.
3. attapulgite sterilization deodorant according to claim 1, it is characterised in that：The Concave-convex clay rod changes for heat
Concave-convex clay rod after property.
4. attapulgite sterilization deodorant according to claim 1, it is characterised in that：The solvent includes second alcohol and water.
5. the method that one kind prepares the attapulgite sterilization deodorant as described in any one of claim 1 ~ 4, it is characterised in that：Bag
Include following steps：
（1）Folium artemisiae argyi, rhizoma atractylodis, Dalmatian chrysanthemum, Radix Glycyrrhizae, Kadsura Root-bark, crotons, calamus, the root bark of tree peony, frutus cnidii, green grass or young crops are weighed respectively according to proportioning
Wormwood artemisia, crushes and mixes, and obtains Traditional Chinese drug mixture；
（2）Traditional Chinese drug mixture is placed in apparatus,Soxhlet's, 3 ~ 5h of extraction is carried out in the mixed solvent of second alcohol and water, extract knot
Shu Hou, obtains extract solution, standby；
（3）Natural attapulgite clay is carried out to be crushed to 100 ~ 200 mesh, is added water, stirring forms mud in suspension, then by ultrasound
After fully dispersed, upper suspension 5 ~ 10min of centrifugal treating in the centrifuge of 3000 turns/min, vacuum filtration after standing are taken；
Filter cake is placed in beaker, ethanol is added, in 10 ~ 20min of ultrasound, vacuum filtration after standing under Ultrasonic Conditions, is dried to obtain
Concave-convex clay rod pretreatment product；
（4）500 DEG C ~ 800 DEG C of Muffle 1 ~ 2h of kiln roasting is placed in after Concave-convex clay rod pretreatment product is dried, after cooling
Particle diameter is ground to for 100 ~ 200 mesh, the Concave-convex clay rod after heat modification is obtained final product；
（5）Concave-convex clay rod after heat modification is placed in extract solution, then according to proportioning add caryophyllus oil, tea tree ethereal oil and
Peppermint essential oil, soaks 10 ~ 12h under stirring condition, after terminating, add shale diatom ooze to be well mixed, and dries, then by solids
Matter is ground to 100 ~ 200 mesh, obtains final product the attapulgite sterilization deodorant.
6. the preparation method of attapulgite sterilization deodorant according to claim 5, it is characterised in that：The step（1）
In be crushed to particle diameter for 100 ~ 200 mesh.
7. the preparation method of attapulgite sterilization deodorant according to claim 5, it is characterised in that：The step（2）
The volume of middle addition mixed solvent is that 5 ~ 10 times of each traditional Chinese medicinal components quality, wherein ethanol and the volume ratio of water are 1:0.5~2：
1。
8. the preparation method of attapulgite sterilization deodorant according to claim 5, it is characterised in that：The step（2）
In extract solution first concentration is needed before mixing with Concave-convex clay rod, be concentrated into extract solution volume be Concave-convex clay rod
3 ~ 5 times of quality.
9. the preparation method of attapulgite sterilization deodorant according to claim 5, it is characterised in that：The step（5）
In drying steps include：Mixture is first placed in rotary evaporation in Rotary Evaporators and removes solvent, then again by solid matter
It is placed in vacuum drying chamber and dries, you can.
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| CN111317000A (en) * | 2020-04-03 | 2020-06-23 | 河南城建学院 | Chinese herbal medicine disinfectant and preparation method and application thereof |
| CN114950377A (en) * | 2022-06-14 | 2022-08-30 | 南京信息工程大学 | Attapulgite air adsorbent and preparation method thereof |
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Application publication date: 20170613 |