CN104069526A - Attapulgite particle air purification agent and preparation method thereof - Google Patents
Attapulgite particle air purification agent and preparation method thereof Download PDFInfo
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- CN104069526A CN104069526A CN201410324874.2A CN201410324874A CN104069526A CN 104069526 A CN104069526 A CN 104069526A CN 201410324874 A CN201410324874 A CN 201410324874A CN 104069526 A CN104069526 A CN 104069526A
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Abstract
The invention provides an attapulgite particle air purification agent which is prepared from the following raw materials in parts by weight: 40-50 parts of modified attapulgite, 4-6 parts of chamomile essential oil, 2-3 parts of ylang essential oil, 1-2 parts of eucalyptus essential oil, 1-2 parts of essential oil of jasminum, 1-2 parts of mastix essential oil, 6-8 parts of glycerol, 8-10 parts of ethyl alcohol, 1-2 parts of chitosan, 6-8 parts of sodium fluoride, 4-5 parts of tartaric acid and 8-10 parts of sodium dodecyl benzene sulfonate. A preparation method of the attapulgite particle air purification agent comprises the following steps: mixing modified attapulgite with chitosan, sodium fluoride, tartaric acid and sodium dodecyl benzene sulfonate for pelleting, then uniformly mixing with essential oils such as chamomile essential oil and the like and subsequently packing to prepare the attapulgite particle air purification agent. The air purification agent has the functions of purifying air, sterilizing, relaxing mind, deeply relaxing, relieving worries, calm heart, calming nerves and promoting sleep; the air purification agent is long in fragrance releasing time and has a long-term effect.
Description
technical field
the present invention relates to a kind of air purifying preparation, be specifically related to a kind of attapulgite granule air purifying preparation and preparation method thereof.
Background technology
Existing air purifying preparation mainly contains two types, one is covering type air purifying preparation, this air purifying preparation is actually has covered abnormal flavour, can not fundamentally eliminate abnormal flavour, so be discharged in air, it itself is exactly a kind of polluter, and it self decompose after, produce again hazardous substance, and in the air freshener having, also have some impurity, also be the material of contaminated environment, even have carcinogenic hidden danger, another kind is absorbent-type air purifying preparation, the kind of this air purifying preparation is single, and has potential safety hazard.Also do not possess on the market at present absorption and covering, many effects that sterilizes air purifying preparation simultaneously.
Summary of the invention
The invention provides a kind of attapulgite granule air purifying preparation and preparation method thereof.Of the present invention have the effect that purifies air and sterilize, and plays to loosen mood, further depressurized, alleviate worry simultaneously, allows soul calmness, calm the nerves, effect of hypnotic, and long-acting.
The technical solution used in the present invention is for achieving the above object:
A kind of attapulgite granule air purifying preparation, it is characterized in that, component raw material by following weight portion is made: attapulgite modified 40-50, Flos Matricariae chamomillae quintessence oil 4-6, Cananga odorata quintessence oil 2-3, eucalyptus quintessence oil 1-2 jasmin quintessence oil 1-2, Olibanum quintessence oil 1-2, glycerol 6-8, ethanol 8-10, chitin 1-2, sodium fluoride 6-8, tartaric acid 4-5, dodecylbenzene sodium sulfonate 8-10
Described attapulgite modified preparation method: a, take following component raw material by weight: attapulgite 100-150, Vermiculitum 10-12, nano-sized carbon 1-2, aluminium oxide 2-3, Essential Oil From Pine Needles 2-3, citric acid 1-2, sodium alginate 1-1.5, silane coupler 4-5, tea polyphenols 3-4;
B, attapulgite, Vermiculitum are calcined to 4-5h under 200 ~ 400 ° of C roastings, after rear taking-up is cooling, decoct with water 1-2 hour with together with the Chinese herbal medicine of attapulgite weight 8-10% again, filter, filtrate spraying is dry, obtain Chinese herbal medicine extract powders A, filtering residue adds in the vinegar liquid of 10-15% again and soaks and grind 1-2 hour, then takes out to dry to obtain powder B, then A and B are mixed to get to mixed material C;
C, above-mentioned gained mixed material C is mixed with nano-sized carbon, aluminium oxide, carboxymethyl cellulose, Essential Oil From Pine Needles and other residual components, and even with the high speed dispersion of 8000-10000 rev/min, obtain attapulgite modified,
Described Chinese herbal medicine comprises the crude drug of following weight portion: mentha leave 3-4, Folium Nelumbinis 3-4, Ramulus Cinnamomi 4-5, Radix Stemonae 2-4, Radix rhamni crenatae 3-5, Radix Isatidis 4-6, Radix Salviae Miltiorrhizae 4-6, Radix Clematidis 4-6, Radix Stemonae 4-6, Herba Violae 2-4, Cortex Fraxini 2-4,
Described Chinese herbal medicine comprises the crude drug of following weight portion: mentha leave 3-4, Folium Nelumbinis 3-4, Ramulus Cinnamomi 4-5, Radix Stemonae 2-4, Radix rhamni crenatae 3-5, Radix Isatidis 4-6, Radix Salviae Miltiorrhizae 4-6, Radix Clematidis 4-6, Radix Stemonae 4-6, Herba Violae 2-4, Cortex Fraxini 2-4.
The preparation method of described attapulgite granule air purifying preparation, is characterized in that, comprises the following steps:
(1), by chitin, sodium fluoride, tartaric acid and appropriate water, at 50-60 DEG C, fully stir 20-30 minute, and then add dodecylbenzene sodium sulfonate fully to stir after 5-10 minute, then add attapulgite modified high-speed stirred 10-20 minute, pelletize;
(2) Flos Matricariae chamomillae quintessence oil, Cananga odorata quintessence oil, eucalyptus quintessence oil, jasmin quintessence oil, Olibanum quintessence oil, glycerol, ethanol are mixed in proportion, obtain mixed essential oil;
(3) pellet that mixed essential oil step (2) being obtained and step (1) make fully mixes, packaging on request.
beneficial effect
Air freshener of the present invention has the effect that purifies air and sterilize, play simultaneously and loosen mood, further depressurized, alleviate worry, allow soul calmness, calm the nerves, effect of hypnotic, and attapulgite modified adds, effectively extend the release time of air freshener, had long-lastingly, reached the object of the air of the long-acting pure and fresh confined space.
Detailed description of the invention
A kind of attapulgite granule air purifying preparation, component raw material by following weight (kg) is made: attapulgite modified 45, Flos Matricariae chamomillae quintessence oil 5, Cananga odorata quintessence oil 2.5, eucalyptus quintessence oil 1.5, jasmin quintessence oil 1.5, Olibanum quintessence oil 1.5, glycerol 7, ethanol 9, chitin 1.5, sodium fluoride 7, tartaric acid 4.5, dodecylbenzene sodium sulfonate 9
Wherein attapulgite modified preparation method: a, by weight (kg) take following component raw material: attapulgite 120, Vermiculitum 11, nano-sized carbon 2, aluminium oxide 2.5, Essential Oil From Pine Needles 2.5, citric acid 1.5, sodium alginate 1, silane coupler 4.5, tea polyphenols 3.4;
B, attapulgite, Vermiculitum are calcined to 4-5h under 200 ~ 400 ° of C roastings, after rear taking-up is cooling, decoct with water 1-2 hour with together with the Chinese herbal medicine of attapulgite weight 8-10% again, filter, filtrate spraying is dry, obtain Chinese herbal medicine extract powders A, filtering residue adds in the vinegar liquid of 10-15% again and soaks and grind 1-2 hour, then takes out to dry to obtain powder B, then A and B are mixed to get to mixed material C;
C, above-mentioned gained mixed material C is mixed with nano-sized carbon, aluminium oxide, carboxymethyl cellulose, Essential Oil From Pine Needles and other residual components, and even with the high speed dispersion of 8000-10000 rev/min, obtain attapulgite modified,
Wherein, Chinese herbal medicine comprises the crude drug of following weight (kg): mentha leave 3, Folium Nelumbinis 4, Ramulus Cinnamomi 4, the Radix Stemonae 3, Radix rhamni crenatae 4, Radix Isatidis 5, Radix Salviae Miltiorrhizae 5, Radix Clematidis 5, the Radix Stemonae 5, Herba Violae 3, Cortex Fraxini 3.
The preparation method of attapulgite granule air purifying preparation, comprises the following steps:
(1), by chitin, sodium fluoride, tartaric acid and appropriate water, at 55 DEG C, fully stir 25 minutes, and then add dodecylbenzene sodium sulfonate fully to stir after 8 minutes, then add attapulgite modified high-speed stirred 15 minutes, pelletize;
(2) Flos Matricariae chamomillae quintessence oil, Cananga odorata quintessence oil, eucalyptus quintessence oil, jasmin quintessence oil, Olibanum quintessence oil, glycerol, ethanol are mixed in proportion, obtain mixed essential oil;
(3) pellet that mixed essential oil step (2) being obtained and step (1) make fully mixes, packaging on request.
Claims (2)
1. an attapulgite granule air purifying preparation, it is characterized in that, component raw material by following weight portion is made: attapulgite modified 40-50, Flos Matricariae chamomillae quintessence oil 4-6, Cananga odorata quintessence oil 2-3, eucalyptus quintessence oil 1-2 jasmin quintessence oil 1-2, Olibanum quintessence oil 1-2, glycerol 6-8, ethanol 8-10, chitin 1-2, sodium fluoride 6-8, tartaric acid 4-5, dodecylbenzene sodium sulfonate 8-10
Described attapulgite modified preparation method: a, take following component raw material by weight: attapulgite 100-150, Vermiculitum 10-12, nano-sized carbon 1-2, aluminium oxide 2-3, Essential Oil From Pine Needles 2-3, citric acid 1-2, sodium alginate 1-1.5, silane coupler 4-5, tea polyphenols 3-4;
B, attapulgite, Vermiculitum are calcined to 4-5h under 200 ~ 400 ° of C roastings, after rear taking-up is cooling, decoct with water 1-2 hour with together with the Chinese herbal medicine of attapulgite weight 8-10% again, filter, filtrate spraying is dry, obtain Chinese herbal medicine extract powders A, filtering residue adds in the vinegar liquid of 10-15% again and soaks and grind 1-2 hour, then takes out to dry to obtain powder B, then A and B are mixed to get to mixed material C;
C, above-mentioned gained mixed material C is mixed with nano-sized carbon, aluminium oxide, carboxymethyl cellulose, Essential Oil From Pine Needles and other residual components, and even with the high speed dispersion of 8000-10000 rev/min, obtain attapulgite modified,
Described Chinese herbal medicine comprises the crude drug of following weight portion: mentha leave 3-4, Folium Nelumbinis 3-4, Ramulus Cinnamomi 4-5, Radix Stemonae 2-4, Radix rhamni crenatae 3-5, Radix Isatidis 4-6, Radix Salviae Miltiorrhizae 4-6, Radix Clematidis 4-6, Radix Stemonae 4-6, Herba Violae 2-4, Cortex Fraxini 2-4.
2. the preparation method of attapulgite granule air purifying preparation as claimed in claim 1, is characterized in that, comprises the following steps:
(1) by chitin, sodium fluoride, tartaric acid and appropriate water, at 50-60 DEG C, fully stir 20-30 minute, and then add dodecylbenzene sodium sulfonate fully to stir after 5-10 minute, then add attapulgite modified high-speed stirred 10-20 minute, pelletize,
(2) Flos Matricariae chamomillae quintessence oil, Cananga odorata quintessence oil, eucalyptus quintessence oil, jasmin quintessence oil, Olibanum quintessence oil, glycerol, ethanol are mixed in proportion, obtain mixed essential oil;
(3) pellet that mixed essential oil step (2) being obtained and step (1) make fully mixes, packaging on request.
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Cited By (12)
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CN105435277A (en) * | 2015-12-15 | 2016-03-30 | 天津一橙泽恒环保科技发展有限公司 | Air refreshing and dedusting agent |
CN106139817A (en) * | 2016-07-29 | 2016-11-23 | 无锡信大气象传感网科技有限公司 | A kind of air purifying preparation and preparation method thereof |
CN106823678A (en) * | 2017-04-14 | 2017-06-13 | 明光市安盛非金属材料厂 | A kind of attapulgite sterilization deodorant and preparation method |
CN107050496A (en) * | 2017-04-11 | 2017-08-18 | 明光市安盛非金属材料厂 | A kind of concave-convex stick air purification agent and preparation method thereof |
CN107252613A (en) * | 2017-07-27 | 2017-10-17 | 嘉兴市九分钟生物科技有限公司 | It is a kind of to remove ammonia and the material for air purification of deodorization and preparation method thereof |
CN107362680A (en) * | 2017-08-02 | 2017-11-21 | 合肥东恒锐电子科技有限公司 | A kind of cleanser for air purifier and preparation method thereof |
CN107376641A (en) * | 2017-09-22 | 2017-11-24 | 太仓弘杉环保科技有限公司 | A kind of environment-friendly filter element material for air purifier |
CN108017421A (en) * | 2017-11-07 | 2018-05-11 | 安徽同济生生物科技有限公司 | A kind of seedbed of stem of noble dendrobium polyploid and preparation method thereof |
CN108031272A (en) * | 2017-11-02 | 2018-05-15 | 肇庆市高新区伟瑞生物科技有限公司 | A kind of dedicated Chinese medicine cleanser of air purifier |
CN111358719A (en) * | 2020-03-18 | 2020-07-03 | 西北师范大学白银师科创新研究院 | Chinese herbal medicine lipstick with cheilitis preventing function and preparation method thereof |
CN112263703A (en) * | 2020-10-26 | 2021-01-26 | 北京硅宝纳米活性硅材料有限公司 | Adsorption bag with antibacterial, nerve-calming and sleep-aiding functions |
CN113318259A (en) * | 2021-05-28 | 2021-08-31 | 明光市铭垚凹凸棒产业科技有限公司 | Attapulgite-based slow-release solid aromatic and preparation method thereof |
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Cited By (13)
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---|---|---|---|---|
CN105435277A (en) * | 2015-12-15 | 2016-03-30 | 天津一橙泽恒环保科技发展有限公司 | Air refreshing and dedusting agent |
CN106139817A (en) * | 2016-07-29 | 2016-11-23 | 无锡信大气象传感网科技有限公司 | A kind of air purifying preparation and preparation method thereof |
CN106139817B (en) * | 2016-07-29 | 2019-01-01 | 广东得天生物科技有限公司 | A kind of air purifying preparation and preparation method thereof |
CN107050496A (en) * | 2017-04-11 | 2017-08-18 | 明光市安盛非金属材料厂 | A kind of concave-convex stick air purification agent and preparation method thereof |
CN106823678A (en) * | 2017-04-14 | 2017-06-13 | 明光市安盛非金属材料厂 | A kind of attapulgite sterilization deodorant and preparation method |
CN107252613A (en) * | 2017-07-27 | 2017-10-17 | 嘉兴市九分钟生物科技有限公司 | It is a kind of to remove ammonia and the material for air purification of deodorization and preparation method thereof |
CN107362680A (en) * | 2017-08-02 | 2017-11-21 | 合肥东恒锐电子科技有限公司 | A kind of cleanser for air purifier and preparation method thereof |
CN107376641A (en) * | 2017-09-22 | 2017-11-24 | 太仓弘杉环保科技有限公司 | A kind of environment-friendly filter element material for air purifier |
CN108031272A (en) * | 2017-11-02 | 2018-05-15 | 肇庆市高新区伟瑞生物科技有限公司 | A kind of dedicated Chinese medicine cleanser of air purifier |
CN108017421A (en) * | 2017-11-07 | 2018-05-11 | 安徽同济生生物科技有限公司 | A kind of seedbed of stem of noble dendrobium polyploid and preparation method thereof |
CN111358719A (en) * | 2020-03-18 | 2020-07-03 | 西北师范大学白银师科创新研究院 | Chinese herbal medicine lipstick with cheilitis preventing function and preparation method thereof |
CN112263703A (en) * | 2020-10-26 | 2021-01-26 | 北京硅宝纳米活性硅材料有限公司 | Adsorption bag with antibacterial, nerve-calming and sleep-aiding functions |
CN113318259A (en) * | 2021-05-28 | 2021-08-31 | 明光市铭垚凹凸棒产业科技有限公司 | Attapulgite-based slow-release solid aromatic and preparation method thereof |
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