CN107118536A - A kind of mouse material and preparation method - Google Patents
A kind of mouse material and preparation method Download PDFInfo
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- CN107118536A CN107118536A CN201710479549.7A CN201710479549A CN107118536A CN 107118536 A CN107118536 A CN 107118536A CN 201710479549 A CN201710479549 A CN 201710479549A CN 107118536 A CN107118536 A CN 107118536A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L69/00—Compositions of polycarbonates; Compositions of derivatives of polycarbonates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/20—Applications use in electrical or conductive gadgets
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Abstract
The invention discloses a kind of mouse material and preparation method, the material includes following component：Makrolon, polyphenylene sulfide, graphene, nano titanium oxide, nano silicon, modified attapulgite clay, shale diatom ooze, bacteria remover, filler, age resistor, coupling agent.Preparation method includes：Bacteria remover is prepared first, processing then is modified to makrolon and polyphenylene sulfide with graphene, and modified attapulgite clay, shale diatom ooze and filler are added into modified mixture, after being well mixed, the scattered 10 ~ 30min of shearing；Bacteria remover is added into mixture again, 20 ~ 30min of ultrasound is stirred, then the double screw extruder extrusion that screw speed is 330 turns/min is being added mixture to, pelletizing obtains the mouse material.Materials application of the present invention not only has preferable waterproof and mechanical property in mouse, also with certain antibacterial and radiation protection, with preferable application value.
Description
Technical field
The present invention relates to computer articles for use field, and in particular to a kind of mouse material and preparation method.
Background technology
Since human society was stepped into the information age, computer is just into our indispensable favorites, nothing at one's side
By from each faces of panoramic each side such as office life ＆ amusements, we will come into contacts with computer everywhere.And we beat therewith
The approach at dealings is following most common two kinds nothing but, keyboard and mouse.Keyboard and mouse be the mankind using computer the most often in contact with
Peripheral product, while being also time of contact most long product certainly.We are daily in use, unavoidable can speckle with hand
Keyboard and mouse is used when grease or moisture content, at the same time, our palm finger can also secrete sweat and excreta, these
So-called " dirt " can all stick to the surface of mouse-keyboard.
People can directly contact the bacterium leaving or grow using keyboard and mouse, can usually will suffer from unknown cause
Various skin diseases, illness in eye and enterogastric diseases, constitute a threat to health.So, realize the subjective antisepsis of keyboard and mouse and dredge
Water oleophobic function, just naturally becomes the urgent demand of people.
At this stage, definitely keyboard and mouse uses the mode of coating to realize special functional effect, such as antibacterial waterproof mostly.
This process had both added process and operation difficulty, and the possibility for the products appearance breaking-up that coating shedding is caused is added again
Property, while coating covering may do not reached at some seams and hole, and antibacterial waterproof and other effects can not be realized, influence product
Whole structure.And existing mouse does not have radiation protection mostly, the Radiation On Human body production that mouse is produced is used for a long time in people
Raw certain injury.
Therefore, researching and developing one kind both has preferable performance, by the key with preferable antibacterial, radiation protection
Disk film is significant, also complies with the demand of existing market, with preferable application prospect.
The content of the invention
It is described it is an object of the invention to provide a kind of mouse material and preparation method for defect of the prior art
Materials application not only has preferable waterproof and mechanical property in mouse, also with certain antibacterial action, greatly reduces mouse
The bacteria breed on surface is marked, while having certain shielding action to electromagnetic radiation, mouse, which is used for a long time, for people provides peace
All risk insurance hinders, with preferable application value.
The present invention solves technical problem and adopted the following technical scheme that：
The present invention relates to a kind of mouse material, include each component of following parts by weight：40 ~ 60 parts of makrolon, polyphenylene sulfide
20 ~ 50 parts, 0.6 ~ 1.3 part of graphene, 8 ~ 15 parts of nano titanium oxide, 10 ~ 17 parts of nano silicon, modified attapulgite glue
9 ~ 16 parts of soil, 5 ~ 10 parts of shale diatom ooze, 10 ~ 15 parts of bacteria remover, 15 ~ 20 parts of filler, 3 ~ 9 parts of age resistor, coupling agent 2 ~ 5
Part；
The bacteria remover includes each component of following parts by weight：10 ~ 20 parts of folium artemisiae argyi, 15 ~ 25 parts of the root bark of tree peony, 10 ~ 20 parts, five times of calamus
10 ~ 15 parts of son, 5 ~ 12 parts of folium isatidis, 15 ~ 22 parts of radix glycyrrhizae, 10 ~ 15 parts of the root of Dahurain angelica, 5 ~ 12 parts of the root of langdu, 6 ~ 10 parts of cloves, Salvia japonica
5 ~ 10 parts.
Preferably, the mouse includes each component of following parts by weight with material：55 parts of makrolon, polyphenylene sulfide 40
Part, 1.1 parts of graphene, 12 parts of nano titanium oxide, 15 parts of nano silicon, 14 parts of modified attapulgite clay, shale silicon
8 parts of algal gel, 13 parts of bacteria remover, 18 parts of filler, 6 parts of age resistor, 3 parts of coupling agent.
Preferably, the bacteria remover includes each component of following parts by weight：16 parts of folium artemisiae argyi, 20 parts of the root bark of tree peony, 15 parts of calamus, five
13 parts of gall nut, 10 parts of folium isatidis, 20 parts of radix glycyrrhizae, 12 parts of the root of Dahurain angelica, 7 parts of the root of langdu, cloves sub 8 parts, 7 parts of Salvia japonica.
Preferably, the modified attapulgite clay is purified natural attapulgite clay, acidifying, after heat modification
Product.
Preferably, the filler is nanometer porous calcium carbonate, superfine talcum powder, superfine white carbon black, ultrafine mica powder
In one or more kinds of mixing.
The invention further relates to a kind of method for preparing mouse material, comprise the following steps：
（1）Bacteria remover each component is weighed respectively according to proportioning, is crushed to particle diameter less than 300 nanometers, is well mixed, then will mixing
Powder is added in apparatus,Soxhlet's, in 78 ~ 80 DEG C, is extracted 3 ~ 5h in the in the mixed solvent of second alcohol and water, is obtained extract solution, then
Extract solution is concentrated, solvent is freezed away, bacteria remover freeze-dried powder is obtained, it is standby；
（2）Makrolon is weighed respectively according to proportioning and polyphenylene sulfide is added in reactor, molten condition is warming up to, to mixing
Graphene and coupling agent, 1 ~ 2h of stirring reaction are added in thing, age resistor is then added into reactant mixture, stirring 10 ~
30min, obtains mixture a1；
（3）Modified attapulgite clay, shale diatom ooze and filler are added into mixture a1, after being well mixed, will be mixed
The speed conditions down cut that thing is transferred in cutter in 500 ~ 700 turns/min disperses 10 ~ 30min, obtains mixture a2；
（4）Bacteria remover is added into mixture a2, after stirring, mixture 20 ~ 30min of ultrasound in ultrasonic wave is placed in, so
Afterwards in the double screw extruder that screw speed is 330 turns/min is added mixture to, melting extrusion, pelletizing obtains institute
State mouse material.
Preferably, the step（1）The addition of middle mixed solvent is 10 ~ 16 times of bacteria remover each component gross weight, its
The volume ratio of middle ethanol and water is 1：1~3.
Preferably, the step（2）The preparation method of middle modified attapulgite clay is：
Take natural attapulgite to be crushed and cross 200 mesh sieves, be placed in beaker, add the water of 10 ~ 20 times of attapulgite quality,
Stirring forms mud in suspension, takes upper suspension 5 ~ 10min of centrifugal treating, vacuum in 2000 ~ 3000 turns/min centrifuge
Suction filtration；Filter cake is placed in flask, 2mol/L watery hydrochloric acid is added, 20 ~ 30min is stirred at reflux in 60 ~ 80 DEG C, is filtered by vacuum,
And it is 6 ~ 7 to be cleaned with distilled water to PH, obtains filter cake, then filter cake is placed in into Muffle furnace Program and be warming up to 600 ~ 800 DEG C, Ran Houheng
Temperature 1 ~ 3h of roasting, is ground to particle diameter for 200 mesh after cooling.
Preferably, the volume that the watery hydrochloric acid is added is 1mL with Concave-convex clay rod mass ratio：5g~10g.
Preferably, the step（4）Water cooling step is first passed through after middle twin-screw extrusion and carries out pelletizing again.
Compared with prior art, the present invention has following beneficial effect：
（1）Mouse material of the present invention, not only with preferable waterproof and mechanical property, also makees with certain antibacterial
With, greatly reduce the bacteria breed of mouse surface, prevent bacteria breed produce cross-infection, be people health office carry
Condition has been supplied, while the mouse prepared using this material also has certain shielding action to electromagnetic radiation, it is that people make for a long time
Safety guarantee is provided with mouse, with preferable application value.
（2）Modified Concave-convex clay rod is added with mouse material of the present invention, due to its unique chain
Layer structure and larger specific surface area, make it have preferable sound insulation, adsorption effect, so that obtained using this material
Mouse has muting function, also has certain suction-operated to electromagnetic radiation and bad smell.
（3）Graphene is added with mouse material of the present invention, it is polymer-modified with graphene, due to graphene tool
There is lamella conjugated structure, be layering the waterproof to form densification, anticorrosive coat, can effectively suppress water to the infiltration of material with oozing
Thoroughly, so that graphene is polymer-modified to have preferable water-fast decay resistance；Further, since the excellent mechanics of graphene
Performance and chemical stability so that modified polymer has preferable wear-resisting, high tenacity mechanical property and chemically stable
Property, and then cause the mouse prepared that there is preferable wear-resisting, drop resistant performance and preferable chemical stability, substantially increase
The performance and service life of mouse.
（4）Added with crude drug component as bacteria remover in mouse material of the present invention, can effectively it kill except thin
Bacterium, and can effectively prevent bacteria breed；And bacteria remover is used in combination with shale diatom ooze, also with preferable anti-mold effect, have
Effect prevents the growth of mould in mouse surface and mouse, and guarantee is provided for people's safe handling mouse.
（5）The preparation technology of mouse material of the present invention is simple, mild condition, and preparation process thing pollutant is produced,
Safety and environmental protection, is adapted to industrialization promotion production.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.The experimental method of unreceipted actual conditions in the following example, generally according to normal condition, for example
Sambrook equimoleculars are cloned：Laboratory manual（New York:Cold Spring Harbor Laboratory Press,
1989）Described in condition, or according to the condition proposed by manufacturer.
Embodiment 1：
A kind of mouse material and preparation method of the preferred embodiment of the present invention；
The mouse material, is prepared from by each component of following parts by weight：
55 parts of makrolon, 40 parts of polyphenylene sulfide, 1.1 parts of graphene, 12 parts of nano titanium oxide, 15 parts of nano silicon,
14 parts of modified attapulgite clay, 8 parts of shale diatom ooze, 13 parts of bacteria remover, 18 parts of filler, 6 parts of age resistor, 3 parts of coupling agent；
The bacteria remover is prepared from by each component of following parts by weight：16 parts of folium artemisiae argyi, 20 parts of the root bark of tree peony, 15 parts of calamus, Chinese gall
13 parts, 10 parts of folium isatidis, 20 parts of radix glycyrrhizae, 12 parts of the root of Dahurain angelica, 7 parts of the root of langdu, cloves sub 8 parts, 7 parts of Salvia japonica.
The modified attapulgite clay is the product after purified natural attapulgite clay, acidifying, heat modification.Make
It is due to its unique chain layer structure and larger specific surface area with this material, makes it have preferable sound insulation, adsorption effect,
So that the mouse obtained using this material has muting function, also there is certain absorption to electromagnetic radiation and bad smell
Effect.
The filler is nanometer porous calcium carbonate, superfine white carbon black according to mass ratio 1:1 mixing.
The method of the present invention for preparing mouse material, comprises the following steps：
（1）Bacteria remover each component is weighed respectively according to proportioning, is crushed to particle diameter less than 300 nanometers, is well mixed, then will mixing
Powder is added in apparatus,Soxhlet's, in 78 ~ 80 DEG C, is extracted 4h in the in the mixed solvent of second alcohol and water, is obtained extract solution, then will
Extract solution is concentrated, freezes away solvent, obtains bacteria remover freeze-dried powder, standby；
（2）Makrolon is weighed respectively according to proportioning and polyphenylene sulfide is added in reactor, molten condition is warming up to, to mixing
Graphene and coupling agent, stirring reaction 2h are added in thing, age resistor is then added into reactant mixture, 20min is stirred, obtains
Mixture a1；
（3）Modified attapulgite clay, shale diatom ooze and filler are added into mixture a1, after being well mixed, will be mixed
The speed conditions down cut that thing is transferred in cutter in 600 turns/min disperses 20min, obtains mixture a2；
（4）Bacteria remover is added into mixture a2, after stirring, mixture is placed in ultrasound 20min, Ran Hou in ultrasonic wave
Add mixture in the double screw extruder that screw speed is 330 turns/min, melting extrusion, pelletizing after water cooling is produced
To the mouse material.
Step（1）The addition of middle mixed solvent is 15 times of bacteria remover each component gross weight, the wherein body of ethanol and water
Product is than being 1：2.
Step（2）The preparation method of middle modified attapulgite clay is：
Take natural attapulgite to be crushed and cross 200 mesh sieves, be placed in beaker, add the water of 16 times of attapulgite quality, stir
Mix to form mud in suspension, take upper suspension centrifugal treating 10min in 3000 turns/min centrifuge, be filtered by vacuum；Will filter
Cake is placed in flask, adds 2mol/L watery hydrochloric acid, wherein, the volume that watery hydrochloric acid is added and Concave-convex clay rod mass ratio
For 1mL：8g, is then stirred at reflux 20min in 80 DEG C, vacuum filtration, and it is 6 ~ 7 to be cleaned with distilled water to PH, obtains filter cake, then will
Filter cake is placed in Muffle furnace Program and is warming up to 700 DEG C, then constant temperature calcining 2h, and particle diameter is ground to after cooling for 200 mesh.
Embodiment 2：
A kind of mouse material and preparation method of the preferred embodiment of the present invention；
The mouse material, is prepared from by each component of following parts by weight：
40 parts of makrolon, 20 parts of polyphenylene sulfide, 0.6 part of graphene, 8 parts of nano titanium oxide, 10 parts of nano silicon, change
9 parts of Concave-convex clay rod of property, 5 parts of shale diatom ooze, 10 parts of bacteria remover, 15 parts of filler, 3 parts of age resistor, 2 parts of coupling agent；
The bacteria remover is prepared from by each component of following parts by weight：10 parts of folium artemisiae argyi, 15 parts of the root bark of tree peony, 10 parts of calamus, Chinese gall
10 parts, 5 parts of folium isatidis, 15 parts of radix glycyrrhizae, 10 parts of the root of Dahurain angelica, 5 parts of the root of langdu, cloves sub 6 parts, 5 parts of Salvia japonica.
The modified attapulgite clay is the product after purified natural attapulgite clay, acidifying, heat modification.
The filler is superfine talcum powder.
The method of the present invention for preparing mouse material, comprises the following steps：
（1）Bacteria remover each component is weighed respectively according to proportioning, is crushed to particle diameter less than 300 nanometers, is well mixed, then will mixing
Powder is added in apparatus,Soxhlet's, in 78 ~ 80 DEG C, is extracted 3h in the in the mixed solvent of second alcohol and water, is obtained extract solution, then will
Extract solution is concentrated, freezes away solvent, obtains bacteria remover freeze-dried powder, standby；
（2）Makrolon is weighed respectively according to proportioning and polyphenylene sulfide is added in reactor, molten condition is warming up to, to mixing
Graphene and coupling agent, stirring reaction 1h are added in thing, age resistor is then added into reactant mixture, 10min is stirred, obtains
Mixture a1；
（3）Modified attapulgite clay, shale diatom ooze and filler are added into mixture a1, after being well mixed, will be mixed
The speed conditions down cut that thing is transferred in cutter in 500 turns/min disperses 30min, obtains mixture a2；
（4）Bacteria remover is added into mixture a2, after stirring, mixture is placed in ultrasound 20min, Ran Hou in ultrasonic wave
Add mixture in the double screw extruder that screw speed is 330 turns/min, melting extrusion, pelletizing after water cooling is produced
To the mouse material.
Step（1）The addition of middle mixed solvent is 10 times of bacteria remover each component gross weight, the wherein body of ethanol and water
Product is than being 1：1.
Step（2）The preparation method of middle modified attapulgite clay is：
Take natural attapulgite to be crushed and cross 200 mesh sieves, be placed in beaker, add the water of 10 times of attapulgite quality, stir
Mix to form mud in suspension, take upper suspension centrifugal treating 10min in 2000 turns/min centrifuge, be filtered by vacuum；Will filter
Cake is placed in flask, adds 2mol/L watery hydrochloric acid, wherein, the volume that watery hydrochloric acid is added and Concave-convex clay rod mass ratio
For 1mL：5g, is then stirred at reflux 30min in 60 DEG C, vacuum filtration, and it is 6 ~ 7 to be cleaned with distilled water to PH, obtains filter cake, then will
Filter cake is placed in Muffle furnace Program and is warming up to 600 DEG C, then constant temperature calcining 3h, and particle diameter is ground to after cooling for 200 mesh.
Embodiment 3：
A kind of mouse material and preparation method of the preferred embodiment of the present invention；
The mouse material, is prepared from by each component of following parts by weight：
60 parts of makrolon, 50 parts of polyphenylene sulfide, 1.3 parts of graphene, 15 parts of nano titanium oxide, 17 parts of nano silicon,
16 parts of modified attapulgite clay, 10 parts of shale diatom ooze, 15 parts of bacteria remover, 20 parts of filler, 9 parts of age resistor, coupling agent 5
Part；
The bacteria remover is prepared from by each component of following parts by weight：20 parts of folium artemisiae argyi, 25 parts of the root bark of tree peony, 20 parts of calamus, Chinese gall
15 parts, 12 parts of folium isatidis, 22 parts of radix glycyrrhizae, 15 parts of the root of Dahurain angelica, 12 parts of the root of langdu, cloves sub 10 parts, 10 parts of Salvia japonica.
The modified attapulgite clay is the product after purified natural attapulgite clay, acidifying, heat modification.
The filler is ultrafine mica powder.
The method of the present invention for preparing mouse material, comprises the following steps：
（1）Bacteria remover each component is weighed respectively according to proportioning, is crushed to particle diameter less than 300 nanometers, is well mixed, then will mixing
Powder is added in apparatus,Soxhlet's, in 78 ~ 80 DEG C, is extracted 5h in the in the mixed solvent of second alcohol and water, is obtained extract solution, then will
Extract solution is concentrated, freezes away solvent, obtains bacteria remover freeze-dried powder, standby；
（2）Makrolon is weighed respectively according to proportioning and polyphenylene sulfide is added in reactor, molten condition is warming up to, to mixing
Graphene and coupling agent, stirring reaction 2h are added in thing, age resistor is then added into reactant mixture, 30min is stirred, obtains
Mixture a1；
（3）Modified attapulgite clay, shale diatom ooze and filler are added into mixture a1, after being well mixed, will be mixed
The speed conditions down cut that thing is transferred in cutter in 700 turns/min disperses 10min, obtains mixture a2；
（4）Bacteria remover is added into mixture a2, after stirring, mixture is placed in ultrasound 30min, Ran Hou in ultrasonic wave
Add mixture in the double screw extruder that screw speed is 330 turns/min, melting extrusion, pelletizing after water cooling is produced
To the mouse material.
Step（1）The addition of middle mixed solvent is 16 times of bacteria remover each component gross weight, the wherein body of ethanol and water
Product is than being 1：3.
Step（2）The preparation method of middle modified attapulgite clay is：
Take natural attapulgite to be crushed and cross 200 mesh sieves, be placed in beaker, add the water of 20 times of attapulgite quality, stir
Mix to form mud in suspension, take upper suspension centrifugal treating 5min in 3000 turns/min centrifuge, be filtered by vacuum；By filter cake
It is placed in flask, adds 2mol/L watery hydrochloric acid, wherein, the volume that watery hydrochloric acid is added is with Concave-convex clay rod mass ratio
1mL：10g, is then stirred at reflux 20min in 80 DEG C, vacuum filtration, and it is 6 ~ 7 to be cleaned with distilled water to PH, obtains filter cake, then will
Filter cake is placed in Muffle furnace Program and is warming up to 800 DEG C, then constant temperature calcining 1h, and particle diameter is ground to after cooling for 200 mesh.
In summary, mouse material of the present invention, not only with preferable waterproof and mechanical property, also with one
Fixed antibacterial action, greatly reduces the bacteria breed of mouse surface, and the cross-infection for preventing bacteria breed from producing, is people's
Health office provides condition, while the mouse prepared using this material also has certain shielding action to electromagnetic radiation, is
People are used for a long time mouse and provide safety guarantee, with preferable application value.The preparation of mouse material of the present invention
Technique is simple, mild condition, and preparation process thing pollutant is produced, safety and environmental protection, is adapted to industrialization promotion production.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (10)
1. a kind of mouse material, it is characterised in that：Include each component of following parts by weight：40 ~ 60 parts of makrolon, polyphenylene sulfide
20 ~ 50 parts of ether, 0.6 ~ 1.3 part of graphene, 8 ~ 15 parts of nano titanium oxide, 10 ~ 17 parts of nano silicon, modified attapulgite
9 ~ 16 parts of clay, 5 ~ 10 parts of shale diatom ooze, 10 ~ 15 parts of bacteria remover, 15 ~ 20 parts of filler, 3 ~ 9 parts of age resistor, coupling agent 2 ~ 5
Part；
The bacteria remover includes each component of following parts by weight：10 ~ 20 parts of folium artemisiae argyi, 15 ~ 25 parts of the root bark of tree peony, 10 ~ 20 parts, five times of calamus
10 ~ 15 parts of son, 5 ~ 12 parts of folium isatidis, 15 ~ 22 parts of radix glycyrrhizae, 10 ~ 15 parts of the root of Dahurain angelica, 5 ~ 12 parts of the root of langdu, 6 ~ 10 parts of cloves, Salvia japonica
5 ~ 10 parts.
2. mouse material according to claim 1, it is characterised in that：The mouse includes following parts by weight with material
Each component：55 parts of makrolon, 40 parts of polyphenylene sulfide, 1.1 parts of graphene, 12 parts of nano titanium oxide, nano silicon 15
Part, 14 parts of modified attapulgite clay, 8 parts of shale diatom ooze, 13 parts of bacteria remover, 18 parts of filler, 6 parts of age resistor, coupling agent 3
Part.
3. mouse material according to claim 1, it is characterised in that：The bacteria remover includes each group of following parts by weight
Point：16 parts of folium artemisiae argyi, 20 parts of the root bark of tree peony, 15 parts of calamus, 13 parts of Chinese gall, 10 parts of folium isatidis, 20 parts of radix glycyrrhizae, 12 parts of the root of Dahurain angelica, the root of langdu 7
Part, cloves sub 8 parts, 7 parts of Salvia japonica.
4. mouse material according to claim 1, it is characterised in that：The modified attapulgite clay is natural concavo-convex
Rod stone clay is purified, acidifying, the product after heat modification.
5. mouse material according to claim 1, it is characterised in that：The filler be nanometer porous calcium carbonate,
One or more kinds of mixing in superfine talcum powder, superfine white carbon black, ultrafine mica powder.
6. the method that one kind prepares the mouse material as described in any one of claim 1 ~ 5, it is characterised in that：Including following step
Suddenly：
（1）Bacteria remover each component is weighed respectively according to proportioning, is crushed to particle diameter less than 300 nanometers, is well mixed, then will mixing
Powder is added in apparatus,Soxhlet's, in 78 ~ 80 DEG C, is extracted 3 ~ 5h in the in the mixed solvent of second alcohol and water, is obtained extract solution, then
Extract solution is concentrated, solvent is freezed away, bacteria remover freeze-dried powder is obtained, it is standby；
（2）Makrolon is weighed respectively according to proportioning and polyphenylene sulfide is added in reactor, molten condition is warming up to, to mixing
Graphene and coupling agent, 1 ~ 2h of stirring reaction are added in thing, age resistor is then added into reactant mixture, stirring 10 ~
30min, obtains mixture a1；
（3）Modified attapulgite clay, shale diatom ooze and filler are added into mixture a1, after being well mixed, will be mixed
The speed conditions down cut that thing is transferred in cutter in 500 ~ 700 turns/min disperses 10 ~ 30min, obtains mixture a2；
（4）Bacteria remover is added into mixture a2, after stirring, mixture 20 ~ 30min of ultrasound in ultrasonic wave is placed in, so
Afterwards in the double screw extruder that screw speed is 330 turns/min is added mixture to, melting extrusion, pelletizing obtains institute
State mouse material.
7. the preparation method of mouse material according to claim 6, it is characterised in that：The step（1）Middle mixing is molten
The addition of agent is 10 ~ 16 times of bacteria remover each component gross weight, and wherein the volume ratio of ethanol and water is 1：1~3.
8. the preparation method of mouse material according to claim 6, it is characterised in that：The step（2）Middle modification is recessed
The preparation method of convex rod stone clay is：
Take natural attapulgite to be crushed and cross 200 mesh sieves, be placed in beaker, add the water of 10 ~ 20 times of attapulgite quality,
Stirring forms mud in suspension, takes upper suspension 5 ~ 10min of centrifugal treating, vacuum in 2000 ~ 3000 turns/min centrifuge
Suction filtration；Filter cake is placed in flask, 2mol/L watery hydrochloric acid is added, 20 ~ 30min is stirred at reflux in 60 ~ 80 DEG C, is filtered by vacuum,
And it is 6 ~ 7 to be cleaned with distilled water to PH, obtains filter cake, then filter cake is placed in into Muffle furnace Program and be warming up to 600 ~ 800 DEG C, Ran Houheng
Temperature 1 ~ 3h of roasting, is ground to particle diameter for 200 mesh after cooling.
9. the preparation method of mouse material according to claim 8, it is characterised in that：The volume that the watery hydrochloric acid is added
Amount is 1mL with Concave-convex clay rod mass ratio：5g~10g.
10. the preparation method of mouse material according to claim 6, it is characterised in that：The step（4）Middle twin-screw
Water cooling step is first passed through after extrusion and carries out pelletizing again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710479549.7A CN107118536A (en) | 2017-06-22 | 2017-06-22 | A kind of mouse material and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710479549.7A CN107118536A (en) | 2017-06-22 | 2017-06-22 | A kind of mouse material and preparation method |
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| Publication Number | Publication Date |
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| CN107118536A true CN107118536A (en) | 2017-09-01 |
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| CN201710479549.7A Withdrawn CN107118536A (en) | 2017-06-22 | 2017-06-22 | A kind of mouse material and preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107227013A (en) * | 2017-07-27 | 2017-10-03 | 合肥锦和信息技术有限公司 | A kind of mouse material and preparation method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104387757A (en) * | 2014-11-21 | 2015-03-04 | 厦门烯成科技有限公司 | Graphene composite thermal conductive plastic and preparation method thereof |
| CN106823678A (en) * | 2017-04-14 | 2017-06-13 | 明光市安盛非金属材料厂 | A kind of attapulgite sterilization deodorant and preparation method |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104387757A (en) * | 2014-11-21 | 2015-03-04 | 厦门烯成科技有限公司 | Graphene composite thermal conductive plastic and preparation method thereof |
| CN106823678A (en) * | 2017-04-14 | 2017-06-13 | 明光市安盛非金属材料厂 | A kind of attapulgite sterilization deodorant and preparation method |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107227013A (en) * | 2017-07-27 | 2017-10-03 | 合肥锦和信息技术有限公司 | A kind of mouse material and preparation method |
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