CN1038580C - 对苯二酸的制备方法 - Google Patents

对苯二酸的制备方法 Download PDF

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Publication number
CN1038580C
CN1038580C CN92101420A CN92101420A CN1038580C CN 1038580 C CN1038580 C CN 1038580C CN 92101420 A CN92101420 A CN 92101420A CN 92101420 A CN92101420 A CN 92101420A CN 1038580 C CN1038580 C CN 1038580C
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CN
China
Prior art keywords
mother liquor
terephthalic acid
water
solution
separation column
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
CN92101420A
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English (en)
Chinese (zh)
Other versions
CN1064675A (zh
Inventor
E·欣德马什
J·A·特纳
D·帕克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Invista Technologies Sarl
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=10689524&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN1038580(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Publication of CN1064675A publication Critical patent/CN1064675A/zh
Application granted granted Critical
Publication of CN1038580C publication Critical patent/CN1038580C/zh
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14—Monocyclic dicarboxylic acids
    • C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/26—1,4 - Benzenedicarboxylic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)
  • Treatment Of Water By Oxidation Or Reduction (AREA)
CN92101420A 1991-02-05 1992-02-03 对苯二酸的制备方法 Ceased CN1038580C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB919102393A GB9102393D0 (en) 1991-02-05 1991-02-05 Production of terephthalic acid
GB9102393.7 1991-02-05

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN96109973A Division CN1130328C (zh) 1991-02-05 1996-08-15 对苯二酸的制备方法

Publications (2)

Publication Number Publication Date
CN1064675A CN1064675A (zh) 1992-09-23
CN1038580C true CN1038580C (zh) 1998-06-03

Family

ID=10689524

Family Applications (2)

Application Number Title Priority Date Filing Date
CN92101420A Ceased CN1038580C (zh) 1991-02-05 1992-02-03 对苯二酸的制备方法
CN96109973A Expired - Fee Related CN1130328C (zh) 1991-02-05 1996-08-15 对苯二酸的制备方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN96109973A Expired - Fee Related CN1130328C (zh) 1991-02-05 1996-08-15 对苯二酸的制备方法

Country Status (12)

Country Link
US (2) US5304676A (OSRAM)
EP (1) EP0498591B2 (OSRAM)
JP (1) JPH0558948A (OSRAM)
KR (1) KR100214397B1 (OSRAM)
CN (2) CN1038580C (OSRAM)
CA (1) CA2059719C (OSRAM)
DE (1) DE69201978T3 (OSRAM)
ES (1) ES2070586T5 (OSRAM)
GB (2) GB9102393D0 (OSRAM)
IN (1) IN185008B (OSRAM)
MX (1) MX9200478A (OSRAM)
TW (1) TW326037B (OSRAM)

Families Citing this family (67)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9104776D0 (en) * 1991-03-07 1991-04-17 Ici Plc Process for the production of terephthalic acid
GB9310070D0 (en) * 1992-05-29 1993-06-30 Ici Plc Process for the production of purified terephthalic acid
GB9303191D0 (en) * 1993-02-17 1993-03-31 Ici Plc Separation process
EG20284A (en) * 1993-02-17 1998-07-30 Ici Plc Separation process
US5612007A (en) * 1994-10-14 1997-03-18 Amoco Corporation Apparatus for preparing aromatic carboxylic acids with efficient energy recovery
US5961942A (en) * 1995-06-05 1999-10-05 E. I. Du Pont De Nemours And Company Effluent gas treatment
KR100431684B1 (ko) * 1995-06-05 2004-08-16 이.아이,듀우판드네모아앤드캄파니 유출가스처리방법
US6013835A (en) 1995-06-07 2000-01-11 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid
US5767311A (en) * 1995-06-07 1998-06-16 Glitsch International, Inc. Method and apparatus for preparing purified terephtalic acid
US5929274A (en) 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
US6054610A (en) 1995-06-07 2000-04-25 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid and isophthalic acid from mixed xylenes
DE69522590T2 (de) * 1995-12-30 2002-07-11 Sunkyong Industries Co. Ltd., Suwon Verfahren zur herstellung von terephthalsäure
CA2280503C (en) * 1997-03-14 2008-01-29 E.I. Du Pont De Nemours And Company Treatment of effluent streams containing organic acids
GB9705349D0 (en) 1997-03-14 1997-04-30 Ici Plc Treatment of effluent streams
US6137001A (en) * 1998-02-11 2000-10-24 Bp Amoco Corporation Process for preparing aromatic carboxylic acids with efficient treatments of gaseous effluent
US6765113B2 (en) 2000-07-19 2004-07-20 E.I. Du Pont De Nemours And Company Production of aromatic carboxylic acids
ATE458714T1 (de) * 2001-05-15 2010-03-15 Mitsubishi Chem Corp Verfahren zur herstellung einer verbindung
US7196215B2 (en) * 2001-06-04 2007-03-27 Eastman Chemical Company Process for the production of purified terephthalic acid
US7485747B2 (en) * 2001-06-04 2009-02-03 Eastman Chemical Company Two stage oxidation process for the production of aromatic dicarboxylic acids
ITMI20021423A1 (it) * 2002-06-27 2003-12-29 Eurotecnica Dev & Licensing S Processo per la separazione dell'acqua prodotta nella ossidazione catalitica di idrocarburi aromatici ad acidi aromatici policarbossilici
MXPA05000341A (es) * 2002-07-09 2005-08-19 Invista Tech Sarl Proceso para producir acidos dicarboxilicos aromaticos bajo condiciones supercriticas.
WO2004060847A1 (ja) * 2003-01-07 2004-07-22 Mitsubishi Chemical Corporation 高純度テレフタル酸の製造方法
CN100453517C (zh) * 2003-01-10 2009-01-21 三菱化学株式会社 芳香羧酸的制备方法和对苯二甲酸的制备方法
US20050256335A1 (en) * 2004-05-12 2005-11-17 Ovidiu Marin Providing gases to aromatic carboxylic acid manufacturing processes
CN1960961B (zh) * 2004-05-28 2011-06-22 三菱化学株式会社 高纯度对苯二甲酸的制造方法
CN100551894C (zh) * 2004-06-28 2009-10-21 三菱化学株式会社 对苯二甲酸的制造方法
US7381836B2 (en) * 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7563926B2 (en) 2004-09-02 2009-07-21 Eastman Chemical Company Optimized liquid-phase oxidation
US20060047153A1 (en) * 2004-09-02 2006-03-02 Wonders Alan G Optimized liquid-phase oxidation
US7482482B2 (en) * 2004-09-02 2009-01-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7390921B2 (en) * 2004-09-02 2008-06-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7582793B2 (en) 2004-09-02 2009-09-01 Eastman Chemical Company Optimized liquid-phase oxidation
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7608733B2 (en) * 2004-09-02 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7507857B2 (en) * 2004-09-02 2009-03-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7615663B2 (en) * 2004-09-02 2009-11-10 Eastman Chemical Company Optimized production of aromatic dicarboxylic acids
US7608732B2 (en) * 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) * 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) * 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7361784B2 (en) * 2004-09-02 2008-04-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7399882B2 (en) * 2004-09-02 2008-07-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7692037B2 (en) 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7586000B2 (en) * 2004-09-02 2009-09-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) * 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7495125B2 (en) * 2004-09-02 2009-02-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7371894B2 (en) * 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation
US7589231B2 (en) * 2004-09-02 2009-09-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7572936B2 (en) 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7572932B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
RU2435754C2 (ru) 2005-03-21 2011-12-10 Бп Корпорейшн Норт Америка Инк. Способ возврата энергии в процессе производства ароматических карбоновых кислот
RU2394017C2 (ru) * 2005-03-22 2010-07-10 Мицубиси Кемикал Корпорейшн Способ получения высокочистой терефталевой кислоты
US7884232B2 (en) * 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7402694B2 (en) * 2005-08-11 2008-07-22 Eastman Chemical Company Process for removal of benzoic acid from an oxidizer purge stream
US7358389B2 (en) * 2006-01-04 2008-04-15 Eastman Chemical Company Oxidation system employing internal structure for enhanced hydrodynamics
US7355068B2 (en) 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
CN100368370C (zh) * 2006-03-29 2008-02-13 中国石化仪征化纤股份有限公司 对二甲苯氧化母液中悬浮物的回收系统装置
CN101152969B (zh) * 2006-09-29 2011-01-19 中国石油化工股份有限公司石油化工科学研究院 对苯二甲酸生产废水的处理方法
WO2009141968A1 (ja) * 2008-05-20 2009-11-26 株式会社日立プラントテクノロジー 精製テレフタル酸分離母液の処理方法
WO2010122304A1 (en) 2009-04-24 2010-10-28 Invista Technologies S.A.R.L. Methods, processes, and systems for treating and purifying crude terephthalic acid and associated process streams
US9376364B2 (en) 2011-08-16 2016-06-28 Purac Biochem B.V. Acid/salt separation
EP2744747B1 (en) 2011-08-16 2020-11-18 Purac Biochem B.V. Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up
CN102798679B (zh) * 2012-09-03 2014-01-15 绍兴汉青环保科技有限公司 一种pta 生产装置气体中有机物的气相色谱分析方法
MX375895B (es) 2013-12-18 2025-03-07 Bp Corp North America Inc Proceso mejorado para fabricar acidos carboxilicos aromaticos.
ES2861055T3 (es) 2015-11-13 2021-10-05 Sabic Global Technologies Bv Proceso que utiliza resinas de intercambio iónico para el tratamiento de aguas residuales que derivan de la producción de ácido tereftálico purificado
CN113318471B (zh) * 2021-07-08 2024-05-31 山东友道化学有限公司 二甲苯氧化反应液的处理方法及系统

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GB970492A (en) * 1960-10-18 1964-09-23 Standard Oil Co Production of aromatic carboxylic acids
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US4933492A (en) * 1988-10-13 1990-06-12 Amoco Corporation Purification of crude isophthalic acid

Also Published As

Publication number Publication date
DE69201978T2 (de) 1995-08-24
DE69201978D1 (de) 1995-05-18
USRE36008E (en) 1998-12-22
KR920016399A (ko) 1992-09-24
EP0498591A2 (en) 1992-08-12
CA2059719A1 (en) 1992-08-06
DE69201978T3 (de) 2005-03-10
EP0498591A3 (en) 1993-01-27
GB9202241D0 (en) 1992-03-18
CN1130328C (zh) 2003-12-10
CN1150944A (zh) 1997-06-04
GB9102393D0 (en) 1991-03-20
CN1064675A (zh) 1992-09-23
ES2070586T5 (es) 2005-05-01
JPH0558948A (ja) 1993-03-09
KR100214397B1 (ko) 1999-08-02
MX9200478A (es) 1992-08-01
CA2059719C (en) 2002-10-08
ES2070586T3 (es) 1995-06-01
EP0498591B1 (en) 1995-04-12
EP0498591B2 (en) 2004-10-13
IN185008B (OSRAM) 2000-10-21
US5304676A (en) 1994-04-19
TW326037B (en) 1998-02-01

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Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C15 Extension of patent right duration from 15 to 20 years for appl. with date before 31.12.1992 and still valid on 11.12.2001 (patent law change 1993)
OR01 Other related matters
ASS Succession or assignment of patent right

Owner name: E. I. DU PONT DE NEMOURS AND CO.

Free format text: FORMER OWNER: IMPERIAL CHEMICAL CORPORATION

Effective date: 20040107

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20040107

Address after: Delaware, USA

Patentee after: E. I. du Pont de Nemours and Co.

Address before: London, England, United Kingdom

Patentee before: Imperial Chemical Industries PLC

EE01 Entry into force of recordation of patent licensing contract

Assignee: Oriental Petrochemical (Shanghai) Corporation

Assignor: E. I. du Pont de Nemours and Co.

Contract fulfillment period: Contract performance deadline July 8, 2013

Contract record no.: Contract filing No. 031000030258

Denomination of invention: Process for the preparation of terephthalic acid by the name of the invention

Granted publication date: 19980603

License type: Common License

Record date: 20031021

LIC Patent licence contract for exploitation submitted for record

Free format text: COMMON LICENCE; TIME LIMIT OF IMPLEMENTING CONTACT: 2013.7.8

Name of requester: ORIENTAL PETROCHEMICAL (SHANGHAI) CO., LTD.

Effective date: 20031021

ASS Succession or assignment of patent right

Owner name: INVISTA TECH SARL

Free format text: FORMER OWNER: E. I. DU PONT DE NEMOURS AND CO.

Effective date: 20060721

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20060721

Address after: Zurich Switzerland

Patentee after: INVISTA TECHNOLOGIES S.A.R.L.

Address before: Delaware, USA

Patentee before: E. I. du Pont de Nemours and Co.

C35 Partial or whole invalidation of patent or utility model
IW01 Full invalidation of patent right

Decision date of declaring invalidation: 20040303

Decision number of declaring invalidation: 4286