CN103829242A - Health-care food containing fruit of nitraria red pigment - Google Patents
Health-care food containing fruit of nitraria red pigment Download PDFInfo
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- CN103829242A CN103829242A CN201410080286.9A CN201410080286A CN103829242A CN 103829242 A CN103829242 A CN 103829242A CN 201410080286 A CN201410080286 A CN 201410080286A CN 103829242 A CN103829242 A CN 103829242A
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- 235000013305 food Nutrition 0.000 title claims abstract description 12
- 241000159206 Nitraria Species 0.000 title abstract description 7
- 239000001054 red pigment Substances 0.000 title abstract 4
- 150000004676 glycans Chemical class 0.000 claims abstract description 31
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 31
- 239000005017 polysaccharide Substances 0.000 claims abstract description 31
- 241000196324 Embryophyta Species 0.000 claims abstract description 15
- GUBGYTABKSRVRQ-ASMJPISFSA-N alpha-maltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-ASMJPISFSA-N 0.000 claims abstract description 12
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- OAIJSZIZWZSQBC-GYZMGTAESA-N lycopene Chemical compound CC(C)=CCC\C(C)=C\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C=C(/C)CCC=C(C)C OAIJSZIZWZSQBC-GYZMGTAESA-N 0.000 claims description 13
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- ZCIHMQAPACOQHT-ZGMPDRQDSA-N trans-isorenieratene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/c1c(C)ccc(C)c1C)C=CC=C(/C)C=Cc2c(C)ccc(C)c2C ZCIHMQAPACOQHT-ZGMPDRQDSA-N 0.000 claims description 13
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- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 10
- 239000012141 concentrate Substances 0.000 claims description 10
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to a health-care food containing fruit of nitraria red pigment. The food is prepared from the following components in parts by weight: 10-100 parts of fruit of nitraria red pigment, 10-100 parts of tomato red pigment, 10-100 parts of lycium ruthenicum anthocyanin, 10-100 of wall-broken pollen, 5-50 parts of polysaccharides of four fungi and 5-50 parts of source algae by add plant polysaccharides or amylodextrin by a conventional method, and then tabletting into chewable tablets under the condition of 80-100 kilonewton by sequentially granulating, drying at the temperature of 40-50 DEG C, and straightening, wherein the addition amount of plant polysaccharides or amylodextrin is less than or equal to 5 percent. The raw materials of the health-care food are easily obtained, and the health-care food is easily implemented industrially, has the auxiliary efficacy of improving prostatic hypertrophy, hyperplasia and dropsy of men, and has no harmful effect.
Description
Technical field
The present invention relates to a kind of health food, relate in particular to a kind of health food that contains white bur haematochrome.
Background technology
Bai Cishi China medicinal and edible plant.Be used for for a long time the complementary food materials of stomach invigorating, reducing blood sugar and blood fat by Mongolian medicine always.In " national Chinese herbal medicine compilation ", the function of organization of white thorn introduces and is: function cures mainly] strengthening the spleen and stomach, aid digestion, calm the nerves, induce sweat, lactogenesis.For treatments such as weakness of the spleen and the stomach, indigestion, neurasthenia, flu, agalactias.
The Gu Tebaici of Tang (
nitrariatangutorumBobr) be one of traditional genuine traditional Chinese medicinal materials assortment in Qinghai-Tibet Platean, Nitraria (
nitraria) be zygophyllaceae (
zygophyllceae) a little genus, for machaka, Nitraria has 12 kinds in the whole world, and there are 8 kinds in Asia, the lake basin area and the dust storm that are mainly grown in Gansu, Qinghai, Xinjiang, Eastern Tibet the north, West Inner Mongolia, western part, Ningxia, North Shaanxi are along the line, resource area approximately 66.67 ten thousand hm
2, be a kind of Major Sand-fixing vegetation of Desert Area, drought-resistant especially and saline and alkaline, be mainly self-sow and distribution for a long time.Because plateau climate condition is special, particularly solar radiation is strong, temperature on average is lower, arid etc., and climate characteristic causes this plant to have on physiology and modal specificity and irreplaceability.The well developed root system of the Gu Tebaici of Tang, blade plumpness, its fruit is for resisting ultraviolet radiation, and pigment content is high.
The wild resource amount of Nitraria At The Qaidam Basin is very abundant, and the white thorn of natural distributed has 3 kinds: be respectively the Gu Tebaici of Tang (
n.tangutorumBobr.), Nitraria sibirica (
n.sibiricapall) and greatly fruit is white stings (
n.roborowskiikom.), be mainly distributed in the area such as Dulan, Ulan, Delingha of central basin.Caidamu Basin annual precipitation 17 ~ 350 mm, average annual temperature-1.1 ~ 5.3 ℃.On lake basin, alluvial fan, river alongshore, edge, aeolian accumulation sand dune and intermountain solonchak Plain, white thorn is concentrated growth, and natural habitat is harsh, and mixed raw area approximately has 250,000 hm
2.In western part, white thorn be with matrimony vine, sea-buckthorn is the same is medicinal with the edible traditional wild acinus of the ethnic groups such as illiteracy, Tibetan, Uygur, the Caidamu Basin is because there is very large difference in special habitat and other areas, northwest, especially give prominence in height above sea level, thereby its chemical composition, nutritional labeling, functional component have increase to a certain degree along with the difference in environment border.
But rarely have people to study for white thorn haematochrome to the action and function of human body at present.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of health food that is easy to white bur haematochrome of containing of suitability for industrialized production.
For addressing the above problem, a kind of health food that contains white bur haematochrome of the present invention, is characterized in that: this food by the component of following weight parts add according to a conventional method plant polyose or amylodextrin successively through granulating, 40 ~ 50 ℃ of oven dry, whole grain, being 80 ~ 100,000 Ns at pressure, condition lower sheeting is made chewable tablets: bur haematochrome 10 ~ 100, lycopene 10 ~ 100, black fruit lyceum anthocyanidin 10 ~ 100, broken pollen 10 ~ 100, four mushroom polysaccharide 5 ~ 50, the raw algae 5 ~ 50 in source in vain; Addition≤5% of described plant polyose or amylodextrin.
Described granulation refers to and adopts the ethanol that volumetric concentration is 75% to utilize wet granulator to granulate.
Described lycopene refers to the lycopene product of content 90%.
Described broken pollen refers to broken wall rape pollen.
Described four mushroom polysaccharide refer to four mushroom polyoses of content 20%.
The raw algae in described source refers to the blue-green alga extract of content 90%.
Described black fruit lyceum anthocyanidin refers to the black fruit lyceum anthocyanidin product of content 45 ~ 75%.
Described white bur haematochrome, lycopene, black fruit lyceum anthocyanidin, broken pollen all adopt 95% inulin extracting in jerusalem artichoke and witloof to carry out according to a conventional method encapsulation.
Described white bur haematochrome is to make as follows:
(1) the chlorine dioxide that is 1% by mass concentration after ancient the fresh Tang of plucking extra white bur removal impurity is carried out to sterilization, then utilize the white thorn of seed skin separation equipment separation seed, and this white seed that stings is sent into colloid mill grinding, obtain white thorn pulp;
(2) by described white thorn pulp in temperature be under the condition of 45 ~ 52 ℃ through reduced pressure concentration, obtain concentrated fruit pulp;
(3) the ethanolic solution that is 20% ~ 90% by described concentrated fruit pulp by mass concentration extracts at the temperature of 50 ~ 80 ℃ by the solid-liquid ratio of 1kg:30L ~ 50L, and extraction times is 2 ~ 3 times, and each 30 ~ 50 min, merge to obtain extract;
(4) described extract is crossed to filter cake through DB-80 macroreticular resin, then through flame filter press squeeze and filter, obtain filtrate;
(5) the impurity in separating filtrate:
1. separation resin: by described step (4) the filtrate of gained be to evaporate under the condition of 40 ~ 60 ℃ in temperature, remove ethanol and condensation is simultaneously reclaimed; Then in this filtrate, add the benzinum with weight such as filtrates, after stirring 1 ~ 2h, staticly settle 5 ~ 15min, draw resin and the film class material on filtrate upper strata, then be the benzinum of evaporative removal filtrate lower floor under the condition of 40 ~ 60 ℃ in temperature, must remove the pigment extract after resin;
2. separate pectin: the ethanolic solution that to add with the isopyknic mass concentration of extract in the described pigment extract of removing after resin be 55% ~ 66%, stirs and leaves standstill 12 ~ 24h after 5 ~ 15min pectin is precipitated out; Then the pectin being precipitated out is separated with the speed of 9000 ~ 11000r/min, obtain mother liquor, this mother liquor is the milipore filter of 0.01 ~ 10 μ m by aperture, must remove the macromolecular pigment extract of pectin;
3. separate sugar and polysaccharide: described in inciting somebody to action, remove the macromolecular pigment extract of pectin and at-15 ~-20 ℃ of temperature, leave standstill 20 ~ 40min, obtain respectively polysaccharide precipitation thing and clarified solution; Described clarified solution is with putting into settling tank after siphonage sucking-off, and the acetone that to add with the isopyknic mass concentration of described clarified solution be 100% stirs sedimentation 5 ~ 7h, obtains the pigment extract except desaccharification and polysaccharide, simultaneously Distillation recovery acetone;
4. isolated protein: in the described pigment extract except desaccharification and polysaccharide, the acetone soln that the ethanol that the NaCl solution that to add with the isopyknic mass concentration of extract be 1% ~ 5% or mass concentration are 55 ~ 66% or mass concentration are 100%, stir sedimentation, after 1 ~ 2h, obtain the pigment extract except deproteinize;
(6) by the described pigment extract except deproteinize in temperature be under the condition of 45 ~ 52 ℃ through reduced pressure concentration, obtain relative density and be 1.1 ~ 1.2 concentrate, this concentrate is spray-dried to constant weight, obtains Powdered haematochrome finished product.
Described step (6) in spray-dired condition refer to that inlet temperature is 120 ℃, outlet temperature is 80 ℃.
The present invention compared with prior art has the following advantages:
1, the present invention to medicine food dual purpose plant extract, separation and purification, obtain high-purity vegetable pigment, every phytochrome is equivalent to the former plant content of 15kg, recycling micro-capsule package technology wraps up, and carry out adding food-grade auxiliary material after prescription with other plant extracts, through batch mixing, granulation, compressing tablet, thereby human body is at utmost utilized and absorb plant extracts; Light sensitivity and the thermal sensitivity that can greatly reduce plant anthocyanin class material by micro-capsule package technology make shelf life of products bring up to 18 ~ 20 months simultaneously.
2, product of the present invention nontoxic (referring to Fig. 1, Fig. 2) after testing, has auxiliary effect of improving male prostate hyperplasia and oedema.
3, raw material of the present invention is easy to get, and can efficiently utilize the wild or tame white thorn resource in areas such as being grown in Qinghai, Inner Mongol, Gansu and Xinjiang; Be easy to industrializing implementation, to improving the added value of resource and driving local high-tech biological industry all to have important meaning simultaneously.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the specific embodiment of the present invention is described in further detail.
Fig. 1 is examining report first page of the present invention.
Fig. 2 is examining report second page of the present invention.
The specific embodiment
embodiment 1a health food that contains white bur haematochrome, this food by the component of following weight parts add according to a conventional method plant polyose or amylodextrin successively through granulating, 40 ℃ of oven dry, whole grain, being 80,000 Ns at pressure, condition lower sheeting is made chewable tablets: bur haematochrome 10mg, lycopene 10 mg, black fruit lyceum anthocyanidin 10 mg, broken pollen 10 mg, four mushroom polysaccharide 5 mg, raw algae 5 mg in source in vain; Addition≤5% of plant polyose or amylodextrin.
Wherein: white bur haematochrome is to make as follows:
(1) the chlorine dioxide that is 1% by mass concentration after ancient the fresh Tang of plucking extra white bur removal impurity is carried out to sterilization, then utilize the white thorn of seed skin separation equipment separation seed, and this white seed that stings is sent into colloid mill grinding, obtain white thorn pulp;
By sting in vain pulp in temperature be under the condition of 45 ℃ through reduced pressure concentration, obtain concentrated fruit pulp;
(3) the ethanolic solution that is 20% by concentrated fruit pulp by mass concentration extracts at the temperature of 50 ℃ by the solid-liquid ratio of 1kg:30L, and extraction times is 2 times, and each 30 min, merge to obtain extract;
(4) extract is crossed to filter cake through DB-80 macroreticular resin, then through flame filter press squeeze and filter, obtain filtrate;
(5) the impurity in separating filtrate:
1. separation resin: by step (4) the filtrate of gained be to evaporate under the condition of 40 ℃ in temperature, remove ethanol and condensation is simultaneously reclaimed; Then in this filtrate, add the benzinum with weight such as filtrates, after stirring 1h, staticly settle 5min, draw resin and the film class material on filtrate upper strata, then be the benzinum of evaporative removal filtrate lower floor under the condition of 40 ℃ in temperature, must remove the pigment extract after resin;
2. separate pectin: the ethanolic solution that to add with the isopyknic mass concentration of extract in the pigment extract of removing after resin be 55%, stirs and leaves standstill 12h after 5min pectin is precipitated out; Then the pectin being precipitated out is separated with the speed of 9000r/min, obtain mother liquor, this mother liquor is the milipore filter of 0.01 μ m by aperture, must remove the macromolecular pigment extract of pectin;
3. separate sugar and polysaccharide: will remove the macromolecular pigment extract of pectin and at-15 ℃ of temperature, leave standstill 20min, and obtain respectively polysaccharide precipitation thing and clarified solution; Clarified solution is with putting into settling tank after siphonage sucking-off, and the acetone that to add with the isopyknic mass concentration of clarified solution be 100% stirs sedimentation 5h, obtains the pigment extract except desaccharification and polysaccharide, simultaneously Distillation recovery acetone;
4. isolated protein: in the pigment extract except desaccharification and polysaccharide, the NaCl solution that to add with the isopyknic mass concentration of extract be 1% ~ 5%, stirs sedimentation, obtains the pigment extract except deproteinize after 1h;
(6) will be through reduced pressure concentration in temperature except the pigment extract of deproteinize under the condition of 45 ℃, obtain relative density and be 1.1 ~ 1.2 concentrate, this concentrate is that 120 ℃, outlet temperature are spray-dried to constant weight under the condition of 80 ℃ in inlet temperature, obtains Powdered haematochrome finished product.
embodiment 2a health food that contains white bur haematochrome, this food by the component of following weight parts add according to a conventional method plant polyose or amylodextrin successively through granulating, 50 ℃ of oven dry, whole grain, being 100,000 Ns at pressure, condition lower sheeting is made chewable tablets: bur haematochrome 100 mg, lycopene 100 mg, black fruit lyceum anthocyanidin 100 mg, broken pollen 100 mg, four mushroom polysaccharide 50 mg, raw algae 50 mg in source in vain; Addition≤5% of plant polyose or amylodextrin.
Wherein: white bur haematochrome is to make as follows:
(1) the chlorine dioxide that is 1% by mass concentration after ancient the fresh Tang of plucking extra white bur removal impurity is carried out to sterilization, then utilize the white thorn of seed skin separation equipment separation seed, and this white seed that stings is sent into colloid mill grinding, obtain white thorn pulp;
By sting in vain pulp in temperature be under the condition of 52 ℃ through reduced pressure concentration, obtain concentrated fruit pulp;
(3) the ethanolic solution that is 90% by concentrated fruit pulp by mass concentration extracts at the temperature of 80 ℃ by the solid-liquid ratio of 1kg:50L, and extraction times is 3 times, and each 50 min, merge to obtain extract;
(4) extract is crossed to filter cake through DB-80 macroreticular resin, then through flame filter press squeeze and filter, obtain filtrate;
(5) the impurity in separating filtrate:
1. separation resin: by step (4) the filtrate of gained be to evaporate under the condition of 60 ℃ in temperature, remove ethanol and condensation is simultaneously reclaimed; Then in this filtrate, add the benzinum with weight such as filtrates, after stirring 2h, staticly settle 15min, draw resin and the film class material on filtrate upper strata, then be the benzinum of evaporative removal filtrate lower floor under the condition of 60 ℃ in temperature, must remove the pigment extract after resin;
2. separate pectin: the ethanolic solution that to add with the isopyknic mass concentration of extract in the pigment extract of removing after resin be 66%, stirs and leaves standstill 24h after 15min pectin is precipitated out; Then the pectin being precipitated out is separated with the speed of 11000r/min, obtain mother liquor, this mother liquor is the milipore filter of 10 μ m by aperture, must remove the macromolecular pigment extract of pectin;
3. separate sugar and polysaccharide: will remove the macromolecular pigment extract of pectin and at-20 ℃ of temperature, leave standstill 40min, and obtain respectively polysaccharide precipitation thing and clarified solution; Clarified solution is with putting into settling tank after siphonage sucking-off, and the acetone that to add with the isopyknic mass concentration of clarified solution be 100% stirs sedimentation 7h, obtains the pigment extract except desaccharification and polysaccharide, simultaneously Distillation recovery acetone;
4. isolated protein: in the pigment extract except desaccharification and polysaccharide, the ethanolic solution that to add with the isopyknic mass concentration of extract be 55 ~ 66%, stirs sedimentation, obtains the pigment extract except deproteinize after 2h;
(6) will be through reduced pressure concentration in temperature except the pigment extract of deproteinize under the condition of 52 ℃, obtain relative density and be 1.1 ~ 1.2 concentrate, this concentrate is that 120 ℃, outlet temperature are spray-dried to constant weight under the condition of 80 ℃ in inlet temperature, obtains Powdered haematochrome finished product.
embodiment 3a health food that contains white bur haematochrome, this food by the component of following weight parts add according to a conventional method plant polyose or amylodextrin successively through granulating, 45 ℃ of oven dry, whole grain, being 90,000 Ns at pressure, condition lower sheeting is made chewable tablets: bur haematochrome 50 mg, lycopene 50mg, black fruit lyceum anthocyanidin 50 mg, broken pollen 50 mg, four mushroom polysaccharide 25 mg, raw algae 25 mg in source in vain; Addition≤5% of plant polyose or amylodextrin.
Wherein: white bur haematochrome is to make as follows:
(1) the chlorine dioxide that is 1% by mass concentration after ancient the fresh Tang of plucking extra white bur removal impurity is carried out to sterilization, then utilize the white thorn of seed skin separation equipment separation seed, and this white seed that stings is sent into colloid mill grinding, obtain white thorn pulp;
By sting in vain pulp in temperature be under the condition of 48 ℃ through reduced pressure concentration, obtain concentrated fruit pulp;
(3) the ethanolic solution that is 55% by concentrated fruit pulp by mass concentration extracts at the temperature of 65 ℃ by the solid-liquid ratio of 1kg:40L, and extraction times is 2 times, and each 40 min, merge to obtain extract;
(4) extract is crossed to filter cake through DB-80 macroreticular resin, then through flame filter press squeeze and filter, obtain filtrate;
(5) the impurity in separating filtrate:
1. separation resin: by step (4) the filtrate of gained be to evaporate under the condition of 50 ℃ in temperature, remove ethanol and condensation is simultaneously reclaimed; Then in this filtrate, add the benzinum with weight such as filtrates, after stirring 1.5h, staticly settle 10min, draw resin and the film class material on filtrate upper strata, then be the benzinum of evaporative removal filtrate lower floor under the condition of 50 ℃ in temperature, must remove the pigment extract after resin;
2. separate pectin: the ethanolic solution that to add with the isopyknic mass concentration of extract in the pigment extract of removing after resin be 60%, stirs and leaves standstill 18h after 10min pectin is precipitated out; Then the pectin being precipitated out is separated with the speed of 10000r/min, obtain mother liquor, this mother liquor is the milipore filter of 5 μ m by aperture, must remove the macromolecular pigment extract of pectin;
3. separate sugar and polysaccharide: will remove the macromolecular pigment extract of pectin and at-18 ℃ of temperature, leave standstill 30min, and obtain respectively polysaccharide precipitation thing and clarified solution; Clarified solution is with putting into settling tank after siphonage sucking-off, and the acetone that to add with the isopyknic mass concentration of clarified solution be 100% stirs sedimentation 6h, obtains the pigment extract except desaccharification and polysaccharide, simultaneously Distillation recovery acetone;
4. isolated protein: in the pigment extract except desaccharification and polysaccharide, the acetone soln that to add with the isopyknic mass concentration of extract be 100%, stirs sedimentation, obtains the pigment extract except deproteinize after 1.5h;
(6) will be through reduced pressure concentration in temperature except the pigment extract of deproteinize under the condition of 48 ℃, obtain relative density and be 1.1 ~ 1.2 concentrate, this concentrate is that 120 ℃, outlet temperature are spray-dried to constant weight under the condition of 80 ℃ in inlet temperature, obtains Powdered haematochrome finished product.
Above-mentioned
embodiment 1 ~ 3in, granulate and refer to that the ethanol that employing volumetric concentration is 75% utilizes wet granulator to granulate.
Lycopene refers to the lycopene product of the content 90% of Shaanxi Sen Fu high-tech Industrial Co., Ltd. production.
Broken pollen refers to " tremnbling " broken wall rape pollen that Qinghai Kangpu Biological Science and Technology Co., Ltd. produces.
Four mushroom polysaccharide refer to four mushroom polyoses of the content 20% of Sen Yuan bio tech ltd, Xi'an or the production and sales of Xi'an Lv Ze biotech company.
The raw algae in source refers to the blue-green alga extract of the content 90% of Shaanxi Sen Fu high-tech Industrial Co., Ltd. production.
Black fruit lyceum anthocyanidin refers to the anthocyanin class material that utilizes alcohol extracting method to extract from black fruit lyceum, the black fruit lyceum anthocyanidin product by Shaanxi Sen Fu high-tech Industrial Co., Ltd. for the content 45 ~ 75% of processing.
White bur haematochrome, lycopene, black fruit lyceum anthocyanidin, broken pollen all adopt 95% inulin (Vad, Qinghai Bioisystech Co., Ltd produces) extracting in jerusalem artichoke and witloof to carry out according to a conventional method encapsulation.
Claims (10)
1. a health food that contains white bur haematochrome, is characterized in that: this food by the component of following weight parts add according to a conventional method plant polyose or amylodextrin successively through granulating, 40 ~ 50 ℃ of oven dry, whole grain, being 80 ~ 100,000 Ns at pressure, condition lower sheeting is made chewable tablets: bur haematochrome 10 ~ 100, lycopene 10 ~ 100, black fruit lyceum anthocyanidin 10 ~ 100, broken pollen 10 ~ 100, four mushroom polysaccharide 5 ~ 50, the raw algae 5 ~ 50 in source in vain; Addition≤5% of described plant polyose or amylodextrin.
2. a kind of health food that contains white bur haematochrome as claimed in claim 1, is characterized in that: described granulation refers to and adopts the ethanol that volumetric concentration is 75% to utilize wet granulator to granulate.
3. a kind of health food that contains white bur haematochrome as claimed in claim 1, is characterized in that: described lycopene refers to the lycopene product of content 90%.
4. a kind of health food that contains white bur haematochrome as claimed in claim 1, is characterized in that: described broken pollen refers to broken wall rape pollen.
5. a kind of health food that contains white bur haematochrome as claimed in claim 1, is characterized in that: described four mushroom polysaccharide refer to four mushroom polyoses of content 20%.
6. a kind of health food that contains white bur haematochrome as claimed in claim 1, is characterized in that: the raw algae in described source refers to the blue-green alga extract of content 90%.
7. a kind of health food that contains white bur haematochrome as claimed in claim 1, is characterized in that: described black fruit lyceum anthocyanidin refers to the black fruit lyceum anthocyanidin product of content 45 ~ 75%.
8. a kind of health food that contains white bur haematochrome as described in claim 1,3,4 or 7, is characterized in that: described white bur haematochrome, lycopene, black fruit lyceum anthocyanidin, broken pollen all adopt 95% inulin extracting in jerusalem artichoke and witloof to carry out according to a conventional method encapsulation.
9. a kind of health food that contains white bur haematochrome as claimed in claim 1, is characterized in that: described white bur haematochrome is to make as follows:
(1) the chlorine dioxide that is 1% by mass concentration after ancient the fresh Tang of plucking extra white bur removal impurity is carried out to sterilization, then utilize the white thorn of seed skin separation equipment separation seed, and this white seed that stings is sent into colloid mill grinding, obtain white thorn pulp;
(2) by described white thorn pulp in temperature be under the condition of 45 ~ 52 ℃ through reduced pressure concentration, obtain concentrated fruit pulp;
(3) the ethanolic solution that is 20% ~ 90% by described concentrated fruit pulp by mass concentration extracts at the temperature of 50 ~ 80 ℃ by the solid-liquid ratio of 1kg:30L ~ 50L, and extraction times is 2 ~ 3 times, and each 30 ~ 50 min, merge to obtain extract;
(4) described extract is crossed to filter cake through DB-80 macroreticular resin, then through flame filter press squeeze and filter, obtain filtrate;
(5) the impurity in separating filtrate:
1. separation resin: by described step (4) the filtrate of gained be to evaporate under the condition of 40 ~ 60 ℃ in temperature, remove ethanol and condensation is simultaneously reclaimed; Then in this filtrate, add the benzinum with weight such as filtrates, after stirring 1 ~ 2h, staticly settle 5 ~ 15min, draw resin and the film class material on filtrate upper strata, then be the benzinum of evaporative removal filtrate lower floor under the condition of 40 ~ 60 ℃ in temperature, must remove the pigment extract after resin;
2. separate pectin: the ethanolic solution that to add with the isopyknic mass concentration of extract in the described pigment extract of removing after resin be 55% ~ 66%, stirs and leaves standstill 12 ~ 24h after 5 ~ 15min pectin is precipitated out; Then the pectin being precipitated out is separated with the speed of 9000 ~ 11000r/min, obtain mother liquor, this mother liquor is the milipore filter of 0.01 ~ 10 μ m by aperture, must remove the macromolecular pigment extract of pectin;
3. separate sugar and polysaccharide: described in inciting somebody to action, remove the macromolecular pigment extract of pectin and at-15 ~-20 ℃ of temperature, leave standstill 20 ~ 40min, obtain respectively polysaccharide precipitation thing and clarified solution; Described clarified solution is with putting into settling tank after siphonage sucking-off, and the acetone that to add with the isopyknic mass concentration of described clarified solution be 100% stirs sedimentation 5 ~ 7h, obtains the pigment extract except desaccharification and polysaccharide, simultaneously Distillation recovery acetone;
4. isolated protein: in the described pigment extract except desaccharification and polysaccharide, the acetone soln that the ethanol that the NaCl solution that to add with the isopyknic mass concentration of extract be 1% ~ 5% or mass concentration are 55 ~ 66% or mass concentration are 100%, stir sedimentation, after 1 ~ 2h, obtain the pigment extract except deproteinize;
(6) by the described pigment extract except deproteinize in temperature be under the condition of 45 ~ 52 ℃ through reduced pressure concentration, obtain relative density and be 1.1 ~ 1.2 concentrate, this concentrate is spray-dried to constant weight, obtains Powdered haematochrome finished product.
10. a kind of health food that contains white bur haematochrome as claimed in claim 9, is characterized in that: described step (6) in spray-dired condition refer to that inlet temperature is 120 ℃, outlet temperature is 80 ℃.
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