CN103813977A - 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法 - Google Patents

可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法 Download PDF

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Publication number
CN103813977A
CN103813977A CN201280045958.1A CN201280045958A CN103813977A CN 103813977 A CN103813977 A CN 103813977A CN 201280045958 A CN201280045958 A CN 201280045958A CN 103813977 A CN103813977 A CN 103813977A
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CN
China
Prior art keywords
solution
mgcl
magnesium
succinic acid
hcl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201280045958.1A
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English (en)
Chinese (zh)
Inventor
A·B·德哈恩
J·范布鲁格尔
P·L·J·范德魏德
P·P·扬森
J·M·比达尔兰西斯
A·塞尔达巴罗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Purac Biochem BV
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Purac Biochem BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Purac Biochem BV filed Critical Purac Biochem BV
Priority to CN201811117286.6A priority Critical patent/CN109134239A/zh
Publication of CN103813977A publication Critical patent/CN103813977A/zh
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/02Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/01Chlorine; Hydrogen chloride
    • C01B7/03Preparation from chlorides
    • C01B7/035Preparation of hydrogen chloride from chlorides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00Compounds of magnesium
    • C01F5/02Magnesia
    • C01F5/06Magnesia by thermal decomposition of magnesium compounds
    • C01F5/10Magnesia by thermal decomposition of magnesium compounds by thermal decomposition of magnesium chloride with water vapour
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00Compounds of magnesium
    • C01F5/26Magnesium halides
    • C01F5/30Chlorides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
CN201280045958.1A 2011-08-16 2012-08-16 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法 Pending CN103813977A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811117286.6A CN109134239A (zh) 2011-08-16 2012-08-16 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP11177633.2 2011-08-16
EP11177633 2011-08-16
US201161524353P 2011-08-17 2011-08-17
US61/524,353 2011-08-17
PCT/NL2012/050572 WO2013025105A1 (en) 2011-08-16 2012-08-16 Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201811117286.6A Division CN109134239A (zh) 2011-08-16 2012-08-16 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法

Publications (1)

Publication Number Publication Date
CN103813977A true CN103813977A (zh) 2014-05-21

Family

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Family Applications (1)

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CN201280045958.1A Pending CN103813977A (zh) 2011-08-16 2012-08-16 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法

Country Status (14)

Country Link
US (1) US9376364B2 (enExample)
EP (1) EP2744745B1 (enExample)
JP (1) JP6146922B2 (enExample)
KR (1) KR101991705B1 (enExample)
CN (1) CN103813977A (enExample)
AU (1) AU2012295625B2 (enExample)
BR (1) BR112014003379A2 (enExample)
CA (1) CA2843696C (enExample)
EA (1) EA027269B1 (enExample)
IN (1) IN2014CN01924A (enExample)
PL (1) PL2744745T3 (enExample)
UA (1) UA112991C2 (enExample)
WO (1) WO2013025105A1 (enExample)
ZA (1) ZA201401748B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107922188A (zh) * 2015-07-31 2018-04-17 普拉克生化公司 提供琥珀酸溶液的方法

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2488918B (en) 2010-06-26 2014-03-05 Virdia Ltd Sugar mixtures and methods for production and use thereof
IL206678A0 (en) 2010-06-28 2010-12-30 Hcl Cleantech Ltd A method for the production of fermentable sugars
WO2012137201A1 (en) 2011-04-07 2012-10-11 Hcl Cleantech Ltd. Lignocellulose conversion processes and products
CA2844404C (en) 2011-08-16 2020-07-07 Purac Biochem B.V. Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up
CN111808053A (zh) * 2011-08-16 2020-10-23 普拉克生化公司 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法
JP6374861B2 (ja) 2012-05-03 2018-08-15 ヴァーディア, インコーポレイテッド リグノセルロース材料の処理のための方法
EP2821368A1 (en) * 2013-07-03 2015-01-07 PURAC Biochem BV Method for processing magnesium chloride solutions
US11078548B2 (en) 2015-01-07 2021-08-03 Virdia, Llc Method for producing xylitol by fermentation
CN107849620B (zh) * 2015-05-27 2022-01-11 威尔迪亚有限责任公司 用于处理木质纤维素材料的综合方法
EP3118185A1 (en) * 2015-07-14 2017-01-18 PURAC Biochem BV Method for manufacturing succinic acid
CN113003538B (zh) * 2016-01-19 2023-12-29 普拉克生化公司 处理氯化镁溶液的改进方法和制备羧酸的方法
EA201990054A1 (ru) 2016-06-29 2019-05-31 Велинге Инновейшн Аб Способ и устройство для вставки язычка
CN114906812B (zh) * 2022-06-01 2023-06-23 湖南吴赣药业有限公司 一种有机混酸分离纯化方法
WO2024097329A1 (en) 2022-11-02 2024-05-10 Amalgamated Research Llc Smb separator for organic acid purification using a strong acid cation resin

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000017378A2 (en) * 1998-09-17 2000-03-30 Imi (Tami) Process for preparing lactic acid
CN1427813A (zh) * 2000-03-07 2003-07-02 伊斯曼化学公司 从水溶液中回收有机酸的方法
US20060276674A1 (en) * 2003-09-30 2006-12-07 Ajinomoto Co., Inc. Method for purifying succinic acid from fermentation broth
CN101550079A (zh) * 2009-05-12 2009-10-07 安徽丰原发酵技术工程研究有限公司 一种连续制备丁二酸的方法
CN101748161A (zh) * 2010-01-19 2010-06-23 南京工业大学 一种厌氧发酵纯化丁二酸的工艺
KR20100122773A (ko) * 2009-05-13 2010-11-23 삼성석유화학(주) 발효액으로부터 숙신산을 분리 및 정제하는 방법

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT559538A (enExample) 1954-12-08
GB9102393D0 (en) 1991-02-05 1991-03-20 Ici Plc Production of terephthalic acid
AUPP437698A0 (en) * 1998-06-30 1998-07-23 Baumgart, Karl Methods for treatment of coronary, carotid and other vascular disease
US6660505B2 (en) 2000-06-22 2003-12-09 Cognis Corporation Isolation of carboxylic acids from fermentation broth
JP2009079057A (ja) 2005-04-22 2009-04-16 Mitsubishi Chemicals Corp ポリエステル及びその製造方法
US20080223519A1 (en) 2006-12-06 2008-09-18 Locko George A Polyamide polyols and polyurethanes, methods for making and using, and products made therefrom
FR2925068B1 (fr) * 2007-12-13 2010-01-08 Roquette Freres Procedes de production d'acide succinique
US8431372B2 (en) * 2009-06-19 2013-04-30 Mbi International Fermentation method using a magnesium compound containing oxygen
CA2844404C (en) 2011-08-16 2020-07-07 Purac Biochem B.V. Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000017378A2 (en) * 1998-09-17 2000-03-30 Imi (Tami) Process for preparing lactic acid
CN1427813A (zh) * 2000-03-07 2003-07-02 伊斯曼化学公司 从水溶液中回收有机酸的方法
US20060276674A1 (en) * 2003-09-30 2006-12-07 Ajinomoto Co., Inc. Method for purifying succinic acid from fermentation broth
CN101550079A (zh) * 2009-05-12 2009-10-07 安徽丰原发酵技术工程研究有限公司 一种连续制备丁二酸的方法
KR20100122773A (ko) * 2009-05-13 2010-11-23 삼성석유화학(주) 발효액으로부터 숙신산을 분리 및 정제하는 방법
CN101748161A (zh) * 2010-01-19 2010-06-23 南京工业大学 一种厌氧发酵纯化丁二酸的工艺

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107922188A (zh) * 2015-07-31 2018-04-17 普拉克生化公司 提供琥珀酸溶液的方法
CN107922188B (zh) * 2015-07-31 2021-12-03 普拉克生化公司 提供琥珀酸溶液的方法

Also Published As

Publication number Publication date
EA027269B1 (ru) 2017-07-31
AU2012295625B2 (en) 2016-05-12
CA2843696C (en) 2019-09-24
KR20140064870A (ko) 2014-05-28
EP2744745B1 (en) 2019-10-30
UA112991C2 (uk) 2016-11-25
US20140200365A1 (en) 2014-07-17
AU2012295625A1 (en) 2014-03-20
BR112014003379A2 (pt) 2017-03-01
JP2014524254A (ja) 2014-09-22
CA2843696A1 (en) 2013-02-21
WO2013025105A1 (en) 2013-02-21
ZA201401748B (en) 2015-01-28
US9376364B2 (en) 2016-06-28
IN2014CN01924A (enExample) 2015-05-29
JP6146922B2 (ja) 2017-06-14
KR101991705B1 (ko) 2019-06-21
PL2744745T3 (pl) 2020-05-18
EA201490408A1 (ru) 2014-07-30
EP2744745A1 (en) 2014-06-25
WO2013025105A8 (en) 2014-04-10

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Application publication date: 20140521