UA112991C2 - Відновлення карбонової кислоти з магнієвих солей шляхом осаджування з використанням хлористоводневої кислоти для створення ферментивного поживного середовища - Google Patents
Відновлення карбонової кислоти з магнієвих солей шляхом осаджування з використанням хлористоводневої кислоти для створення ферментивного поживного середовищаInfo
- Publication number
- UA112991C2 UA112991C2 UAA201402003A UAA201402003A UA112991C2 UA 112991 C2 UA112991 C2 UA 112991C2 UA A201402003 A UAA201402003 A UA A201402003A UA A201402003 A UAA201402003 A UA A201402003A UA 112991 C2 UA112991 C2 UA 112991C2
- Authority
- UA
- Ukraine
- Prior art keywords
- succinic acid
- mgcl
- solution
- acid
- magnesium
- Prior art date
Links
- 159000000003 magnesium salts Chemical class 0.000 title abstract 2
- 102000004190 Enzymes Human genes 0.000 title 1
- 108090000790 Enzymes Proteins 0.000 title 1
- 239000002253 acid Substances 0.000 title 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 title 1
- 230000008021 deposition Effects 0.000 title 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 abstract 15
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 abstract 12
- 239000001384 succinic acid Substances 0.000 abstract 7
- 229910001629 magnesium chloride Inorganic materials 0.000 abstract 6
- 239000000243 solution Substances 0.000 abstract 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 4
- OKUCEQDKBKYEJY-UHFFFAOYSA-N tert-butyl 3-(methylamino)pyrrolidine-1-carboxylate Chemical compound CNC1CCN(C(=O)OC(C)(C)C)C1 OKUCEQDKBKYEJY-UHFFFAOYSA-N 0.000 abstract 3
- 239000000395 magnesium oxide Substances 0.000 abstract 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 abstract 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000007900 aqueous suspension Substances 0.000 abstract 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 abstract 1
- 238000000354 decomposition reaction Methods 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hcl hcl Chemical compound Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 230000020477 pH reduction Effects 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 238000005979 thermal decomposition reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/03—Preparation from chlorides
- C01B7/035—Preparation of hydrogen chloride from chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/02—Magnesia
- C01F5/06—Magnesia by thermal decomposition of magnesium compounds
- C01F5/10—Magnesia by thermal decomposition of magnesium compounds by thermal decomposition of magnesium chloride with water vapour
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/26—Magnesium halides
- C01F5/30—Chlorides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11177633 | 2011-08-16 | ||
| PCT/NL2012/050572 WO2013025105A1 (en) | 2011-08-16 | 2012-08-16 | Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA112991C2 true UA112991C2 (uk) | 2016-11-25 |
Family
ID=50279087
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA201402003A UA112991C2 (uk) | 2011-08-16 | 2012-08-16 | Відновлення карбонової кислоти з магнієвих солей шляхом осаджування з використанням хлористоводневої кислоти для створення ферментивного поживного середовища |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9376364B2 (enExample) |
| EP (1) | EP2744745B1 (enExample) |
| JP (1) | JP6146922B2 (enExample) |
| KR (1) | KR101991705B1 (enExample) |
| CN (1) | CN103813977A (enExample) |
| AU (1) | AU2012295625B2 (enExample) |
| BR (1) | BR112014003379A2 (enExample) |
| CA (1) | CA2843696C (enExample) |
| EA (1) | EA027269B1 (enExample) |
| IN (1) | IN2014CN01924A (enExample) |
| PL (1) | PL2744745T3 (enExample) |
| UA (1) | UA112991C2 (enExample) |
| WO (1) | WO2013025105A1 (enExample) |
| ZA (1) | ZA201401748B (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2585606A4 (en) | 2010-06-26 | 2016-02-17 | Virdia Ltd | SUGAR MIXTURES, METHODS OF PRODUCTION AND USE THEREOF |
| IL206678A0 (en) | 2010-06-28 | 2010-12-30 | Hcl Cleantech Ltd | A method for the production of fermentable sugars |
| US9512495B2 (en) | 2011-04-07 | 2016-12-06 | Virdia, Inc. | Lignocellulose conversion processes and products |
| JP6275039B2 (ja) | 2011-08-16 | 2018-02-07 | ピュラック バイオケム ビー． ブイ． | 発酵ブロス処理にとって有用な、塩化水素酸を用いた沈殿によるカルボン酸のそれらのマグネシウム塩からの回収 |
| GB2518547B (en) | 2012-05-03 | 2015-10-07 | Virdia Ltd | Method for the preparation of high purity lignin |
| EP2821368A1 (en) * | 2013-07-03 | 2015-01-07 | PURAC Biochem BV | Method for processing magnesium chloride solutions |
| CN112226466A (zh) | 2015-01-07 | 2021-01-15 | 威尔迪亚公司 | 萃取和转化半纤维素糖的方法 |
| BR112017025322A8 (pt) * | 2015-05-27 | 2022-08-23 | Virdia Inc | Processos integrados para recuperação de hidrolisato celulósico após hidrólise de polpa de celulose |
| EP3118185A1 (en) | 2015-07-14 | 2017-01-18 | PURAC Biochem BV | Method for manufacturing succinic acid |
| EP3124434A1 (en) | 2015-07-31 | 2017-02-01 | PURAC Biochem BV | Method for providing a succinic acid solution |
| EP3405434A2 (en) * | 2016-01-19 | 2018-11-28 | Purac Biochem bv | Improved method for processing magnesium chloride solutions and method for manufacturing carboxylic acids |
| WO2018004439A1 (en) | 2016-06-29 | 2018-01-04 | Välinge Innovation AB | Method and device for inserting a tongue |
| CN114906812B (zh) * | 2022-06-01 | 2023-06-23 | 湖南吴赣药业有限公司 | 一种有机混酸分离纯化方法 |
| WO2024097329A1 (en) | 2022-11-02 | 2024-05-10 | Amalgamated Research Llc | Smb separator for organic acid purification using a strong acid cation resin |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE548967A (enExample) | 1954-12-08 | 1956-07-14 | ||
| GB9102393D0 (en) | 1991-02-05 | 1991-03-20 | Ici Plc | Production of terephthalic acid |
| AUPP437698A0 (en) * | 1998-06-30 | 1998-07-23 | Baumgart, Karl | Methods for treatment of coronary, carotid and other vascular disease |
| IL126264A0 (en) | 1998-09-17 | 1999-05-09 | Tami Inst For Research & Dev L | Process for preparing lactic acid |
| US6670505B1 (en) | 2000-03-07 | 2003-12-30 | Eastman Chemical Company | Process for the recovery of organic acids from aqueous solutions |
| US6660505B2 (en) | 2000-06-22 | 2003-12-09 | Cognis Corporation | Isolation of carboxylic acids from fermentation broth |
| CN100534972C (zh) * | 2003-09-30 | 2009-09-02 | 味之素株式会社 | 从发酵液中纯化琥珀酸的方法 |
| JP2009079057A (ja) * | 2005-04-22 | 2009-04-16 | Mitsubishi Chemicals Corp | ポリエステル及びその製造方法 |
| US20080223519A1 (en) | 2006-12-06 | 2008-09-18 | Locko George A | Polyamide polyols and polyurethanes, methods for making and using, and products made therefrom |
| FR2925068B1 (fr) * | 2007-12-13 | 2010-01-08 | Roquette Freres | Procedes de production d'acide succinique |
| CN101550079B (zh) * | 2009-05-12 | 2010-10-27 | 安徽丰原发酵技术工程研究有限公司 | 一种连续制备丁二酸的方法 |
| KR101051582B1 (ko) * | 2009-05-13 | 2011-07-22 | 삼성석유화학(주) | 발효액으로부터 숙신산을 분리 및 정제하는 방법 |
| US8431372B2 (en) * | 2009-06-19 | 2013-04-30 | Mbi International | Fermentation method using a magnesium compound containing oxygen |
| CN101748161B (zh) * | 2010-01-19 | 2012-06-06 | 南京工业大学 | 一种厌氧发酵纯化丁二酸的工艺 |
| JP6275039B2 (ja) | 2011-08-16 | 2018-02-07 | ピュラック バイオケム ビー． ブイ． | 発酵ブロス処理にとって有用な、塩化水素酸を用いた沈殿によるカルボン酸のそれらのマグネシウム塩からの回収 |
-
2012
- 2012-08-16 JP JP2014525958A patent/JP6146922B2/ja not_active Expired - Fee Related
- 2012-08-16 AU AU2012295625A patent/AU2012295625B2/en not_active Ceased
- 2012-08-16 US US14/238,666 patent/US9376364B2/en not_active Expired - Fee Related
- 2012-08-16 EA EA201490408A patent/EA027269B1/ru not_active IP Right Cessation
- 2012-08-16 PL PL12750876T patent/PL2744745T3/pl unknown
- 2012-08-16 EP EP12750876.0A patent/EP2744745B1/en active Active
- 2012-08-16 BR BR112014003379A patent/BR112014003379A2/pt not_active IP Right Cessation
- 2012-08-16 KR KR1020147006790A patent/KR101991705B1/ko not_active Expired - Fee Related
- 2012-08-16 UA UAA201402003A patent/UA112991C2/uk unknown
- 2012-08-16 IN IN1924CHN2014 patent/IN2014CN01924A/en unknown
- 2012-08-16 CN CN201280045958.1A patent/CN103813977A/zh active Pending
- 2012-08-16 WO PCT/NL2012/050572 patent/WO2013025105A1/en not_active Ceased
- 2012-08-16 CA CA2843696A patent/CA2843696C/en active Active
-
2014
- 2014-03-10 ZA ZA2014/01748A patent/ZA201401748B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| KR101991705B1 (ko) | 2019-06-21 |
| EP2744745B1 (en) | 2019-10-30 |
| EA027269B1 (ru) | 2017-07-31 |
| EP2744745A1 (en) | 2014-06-25 |
| JP2014524254A (ja) | 2014-09-22 |
| EA201490408A1 (ru) | 2014-07-30 |
| AU2012295625B2 (en) | 2016-05-12 |
| WO2013025105A8 (en) | 2014-04-10 |
| CA2843696A1 (en) | 2013-02-21 |
| BR112014003379A2 (pt) | 2017-03-01 |
| PL2744745T3 (pl) | 2020-05-18 |
| KR20140064870A (ko) | 2014-05-28 |
| IN2014CN01924A (enExample) | 2015-05-29 |
| JP6146922B2 (ja) | 2017-06-14 |
| AU2012295625A1 (en) | 2014-03-20 |
| US20140200365A1 (en) | 2014-07-17 |
| CA2843696C (en) | 2019-09-24 |
| WO2013025105A1 (en) | 2013-02-21 |
| ZA201401748B (en) | 2015-01-28 |
| CN103813977A (zh) | 2014-05-21 |
| US9376364B2 (en) | 2016-06-28 |
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