EA201790354A3 - Извлечение карбоновой кислоты из ее магниевых солей путем осаждения с применением хлористоводородной кислоты, пригодное для выделения продукта реакции из ферментативного бульона - Google Patents
Извлечение карбоновой кислоты из ее магниевых солей путем осаждения с применением хлористоводородной кислоты, пригодное для выделения продукта реакции из ферментативного бульонаInfo
- Publication number
- EA201790354A3 EA201790354A3 EA201790354A EA201790354A EA201790354A3 EA 201790354 A3 EA201790354 A3 EA 201790354A3 EA 201790354 A EA201790354 A EA 201790354A EA 201790354 A EA201790354 A EA 201790354A EA 201790354 A3 EA201790354 A3 EA 201790354A3
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- carboxylic acid
- enzymal
- bulon
- depositing
- extraction
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/03—Preparation from chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/03—Preparation from chlorides
- C01B7/035—Preparation of hydrogen chloride from chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/02—Magnesia
- C01F5/06—Magnesia by thermal decomposition of magnesium compounds
- C01F5/10—Magnesia by thermal decomposition of magnesium compounds by thermal decomposition of magnesium chloride with water vapour
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/26—Magnesium halides
- C01F5/30—Chlorides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
- C07C55/02—Dicarboxylic acids
- C07C55/10—Succinic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
- C07C55/02—Dicarboxylic acids
- C07C55/14—Adipic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
- C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
- C07C57/13—Dicarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
- C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
- C07C57/13—Dicarboxylic acids
- C07C57/15—Fumaric acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C59/235—Saturated compounds containing more than one carboxyl group
- C07C59/245—Saturated compounds containing more than one carboxyl group containing hydroxy or O-metal groups
- C07C59/265—Citric acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Geology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Furan Compounds (AREA)
Abstract
Данное изобретение обеспечивает способ получения карбоновой кислоты, который включает следующие стадии: обеспечение карбоксилата магния, где карбоновая кислота, соответствующая карбоксилату, имеет растворимость в воде при 20°С 80 г/100 г воды или менее; подкисление карбоксилата магния HCl с получением раствора, содержащего карбоновую кислоту и хлорид магния (MgCl); возможно, стадию концентрирования, где раствор, содержащий карбоновую кислоту и MgClконцентрируют; осаждение карбоновой кислоты из раствора, содержащего карбоновую кислоту и MgCl, с получением осадка карбоновой кислоты и раствора MgCl. Было обнаружено, что добавление HCl к магниевой соли карбоновой кислоты и последующее осаждение карбоновой кислоты из раствора приводит к очень эффективному отделению карбоновой кислоты от раствора карбоксилата магния.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP11177633 | 2011-08-16 | ||
US201161524353P | 2011-08-17 | 2011-08-17 | |
PCT/NL2012/050573 WO2013025106A1 (en) | 2011-08-16 | 2012-08-16 | Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up |
Publications (3)
Publication Number | Publication Date |
---|---|
EA201790354A2 EA201790354A2 (ru) | 2017-09-29 |
EA201790354A3 true EA201790354A3 (ru) | 2017-10-31 |
EA039483B1 EA039483B1 (ru) | 2022-02-01 |
Family
ID=50263170
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EA201790354A EA039483B1 (ru) | 2011-08-16 | 2012-08-16 | Извлечение карбоновой кислоты из ее магниевых солей путем осаждения с применением хлористоводородной кислоты, пригодное для выделения продукта реакции из ферментативного бульона |
EA201490410A EA027342B1 (ru) | 2011-08-16 | 2012-08-16 | Извлечение карбоновой кислоты из ее магниевых солей путем осаждения c применением хлористо-водородной кислоты, пригодное для выделения продукта реакции из ферментативного бульона |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
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EA201490410A EA027342B1 (ru) | 2011-08-16 | 2012-08-16 | Извлечение карбоновой кислоты из ее магниевых солей путем осаждения c применением хлористо-водородной кислоты, пригодное для выделения продукта реакции из ферментативного бульона |
Country Status (13)
Country | Link |
---|---|
US (1) | US9061986B2 (ru) |
EP (1) | EP2744746B1 (ru) |
JP (1) | JP6275038B2 (ru) |
KR (1) | KR101974904B1 (ru) |
CN (1) | CN103813978A (ru) |
AU (1) | AU2012295626B2 (ru) |
BR (1) | BR112014003067A2 (ru) |
CA (1) | CA2844204C (ru) |
EA (2) | EA039483B1 (ru) |
PL (1) | PL2744746T3 (ru) |
UA (1) | UA114484C2 (ru) |
WO (1) | WO2013025106A1 (ru) |
ZA (1) | ZA201401745B (ru) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2020045349A (ja) * | 2011-08-16 | 2020-03-26 | ピュラック バイオケム ビー. ブイ. | 発酵ブロス処理にとって有用な、塩化水素酸を用いた沈殿によるカルボン酸のそれらのマグネシウム塩からの回収 |
CN108148027A (zh) * | 2011-08-16 | 2018-06-12 | 普拉克生化公司 | 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法 |
EP3845487A1 (en) | 2011-08-16 | 2021-07-07 | Purac Biochem B.V. | Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up |
NL2011027C2 (en) | 2013-06-24 | 2014-12-29 | Univ Delft Tech | Process for the preparation of 2,5-furandicarboxylic acid. |
EP2821368A1 (en) | 2013-07-03 | 2015-01-07 | PURAC Biochem BV | Method for processing magnesium chloride solutions |
CN111960447A (zh) | 2014-04-01 | 2020-11-20 | 普拉克生化公司 | 氯化镁的热分解 |
DE102014015958A1 (de) | 2014-10-31 | 2016-05-04 | Sig Technology Ag | Vorrichtung, insbesondere zum Verschließen eines Kopfbereichs eines Nahrungsmittel-behälters, aus einem Laminat mit geschältem und umgeschlagenen Randbereich |
US10577339B2 (en) * | 2015-03-17 | 2020-03-03 | Purac Biochem Bv | Method for manufacturing furan-2,5-dicarboxylic acid (FDCA) from a salt solution |
CN108473331B (zh) | 2016-01-19 | 2021-03-12 | 普拉克生化公司 | 处理氯化镁溶液的改进方法和制备羧酸的方法 |
CA3180216A1 (en) | 2020-04-20 | 2021-10-28 | Purac Biochem B.V. | Process for manufacturing high-purity magnesium oxide |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE548967A (ru) * | 1954-12-08 | 1956-07-14 | ||
IL126264A0 (en) * | 1998-09-17 | 1999-05-09 | Tami Inst For Research & Dev L | Process for preparing lactic acid |
WO2001030699A1 (en) * | 1999-10-25 | 2001-05-03 | Nedmag Industries Mining & Manufacturing B.V. | Magnesium oxide, a mixture of metal oxides, methods for preparation thereof and the use of the materials as frac proppant |
US6670505B1 (en) * | 2000-03-07 | 2003-12-30 | Eastman Chemical Company | Process for the recovery of organic acids from aqueous solutions |
US6660505B2 (en) | 2000-06-22 | 2003-12-09 | Cognis Corporation | Isolation of carboxylic acids from fermentation broth |
CN100534972C (zh) | 2003-09-30 | 2009-09-02 | 味之素株式会社 | 从发酵液中纯化琥珀酸的方法 |
KR101051582B1 (ko) * | 2009-05-13 | 2011-07-22 | 삼성석유화학(주) | 발효액으로부터 숙신산을 분리 및 정제하는 방법 |
US8431372B2 (en) * | 2009-06-19 | 2013-04-30 | Mbi International | Fermentation method using a magnesium compound containing oxygen |
CN101748161B (zh) * | 2010-01-19 | 2012-06-06 | 南京工业大学 | 一种厌氧发酵纯化丁二酸的工艺 |
US8829237B2 (en) * | 2011-03-03 | 2014-09-09 | The Michigan Biotechnology Institute | Production of carboxylic acid and salt co-products |
CN108148027A (zh) * | 2011-08-16 | 2018-06-12 | 普拉克生化公司 | 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法 |
EP3845487A1 (en) * | 2011-08-16 | 2021-07-07 | Purac Biochem B.V. | Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up |
-
2012
- 2012-08-16 WO PCT/NL2012/050573 patent/WO2013025106A1/en active Application Filing
- 2012-08-16 UA UAA201402155A patent/UA114484C2/uk unknown
- 2012-08-16 JP JP2014525959A patent/JP6275038B2/ja active Active
- 2012-08-16 EA EA201790354A patent/EA039483B1/ru unknown
- 2012-08-16 AU AU2012295626A patent/AU2012295626B2/en not_active Ceased
- 2012-08-16 CA CA2844204A patent/CA2844204C/en active Active
- 2012-08-16 KR KR1020147006791A patent/KR101974904B1/ko active IP Right Grant
- 2012-08-16 EP EP12750877.8A patent/EP2744746B1/en active Active
- 2012-08-16 CN CN201280046341.1A patent/CN103813978A/zh active Pending
- 2012-08-16 US US14/238,633 patent/US9061986B2/en active Active
- 2012-08-16 EA EA201490410A patent/EA027342B1/ru not_active IP Right Cessation
- 2012-08-16 BR BR112014003067A patent/BR112014003067A2/pt not_active Application Discontinuation
- 2012-08-16 PL PL12750877T patent/PL2744746T3/pl unknown
-
2014
- 2014-03-10 ZA ZA2014/01745A patent/ZA201401745B/en unknown
Also Published As
Publication number | Publication date |
---|---|
JP2014531408A (ja) | 2014-11-27 |
EP2744746B1 (en) | 2020-12-02 |
EP2744746A1 (en) | 2014-06-25 |
CA2844204A1 (en) | 2013-02-21 |
WO2013025106A1 (en) | 2013-02-21 |
AU2012295626B2 (en) | 2016-05-12 |
EA027342B1 (ru) | 2017-07-31 |
CN103813978A (zh) | 2014-05-21 |
US20140357877A1 (en) | 2014-12-04 |
AU2012295626A1 (en) | 2014-03-20 |
BR112014003067A2 (pt) | 2017-02-21 |
US9061986B2 (en) | 2015-06-23 |
KR101974904B1 (ko) | 2019-05-07 |
JP6275038B2 (ja) | 2018-02-07 |
EA201790354A2 (ru) | 2017-09-29 |
PL2744746T3 (pl) | 2021-06-14 |
UA114484C2 (uk) | 2017-06-26 |
KR20140057607A (ko) | 2014-05-13 |
AU2012295626A8 (en) | 2014-10-23 |
EA201490410A1 (ru) | 2014-07-30 |
CA2844204C (en) | 2020-01-28 |
EA039483B1 (ru) | 2022-02-01 |
ZA201401745B (en) | 2015-09-30 |
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