BR112014003379A2 - recuperação de ácido carboxílico a partir dos seus sais de magnésio por precipitação utilizando ácido clorídrico, útil para o desenvolvimento de um meio de fermentação - Google Patents
recuperação de ácido carboxílico a partir dos seus sais de magnésio por precipitação utilizando ácido clorídrico, útil para o desenvolvimento de um meio de fermentaçãoInfo
- Publication number
- BR112014003379A2 BR112014003379A2 BR112014003379A BR112014003379A BR112014003379A2 BR 112014003379 A2 BR112014003379 A2 BR 112014003379A2 BR 112014003379 A BR112014003379 A BR 112014003379A BR 112014003379 A BR112014003379 A BR 112014003379A BR 112014003379 A2 BR112014003379 A2 BR 112014003379A2
- Authority
- BR
- Brazil
- Prior art keywords
- succinic acid
- solution
- precipitation
- acid
- magnesium
- Prior art date
Links
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 title abstract 7
- 159000000003 magnesium salts Chemical class 0.000 title abstract 3
- 238000001556 precipitation Methods 0.000 title abstract 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 title abstract 2
- 238000000855 fermentation Methods 0.000 title abstract 2
- 230000004151 fermentation Effects 0.000 title abstract 2
- 238000011084 recovery Methods 0.000 title abstract 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 abstract 15
- 239000001384 succinic acid Substances 0.000 abstract 7
- OKUCEQDKBKYEJY-UHFFFAOYSA-N tert-butyl 3-(methylamino)pyrrolidine-1-carboxylate Chemical compound CNC1CCN(C(=O)OC(C)(C)C)C1 OKUCEQDKBKYEJY-UHFFFAOYSA-N 0.000 abstract 3
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 abstract 1
- 238000003916 acid precipitation Methods 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/03—Preparation from chlorides
- C01B7/035—Preparation of hydrogen chloride from chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/02—Magnesia
- C01F5/06—Magnesia by thermal decomposition of magnesium compounds
- C01F5/10—Magnesia by thermal decomposition of magnesium compounds by thermal decomposition of magnesium chloride with water vapour
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/26—Magnesium halides
- C01F5/30—Chlorides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11177633 | 2011-08-16 | ||
| US201161524353P | 2011-08-17 | 2011-08-17 | |
| PCT/NL2012/050572 WO2013025105A1 (en) | 2011-08-16 | 2012-08-16 | Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR112014003379A2 true BR112014003379A2 (pt) | 2017-03-01 |
Family
ID=50279087
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112014003379A BR112014003379A2 (pt) | 2011-08-16 | 2012-08-16 | recuperação de ácido carboxílico a partir dos seus sais de magnésio por precipitação utilizando ácido clorídrico, útil para o desenvolvimento de um meio de fermentação |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9376364B2 (enExample) |
| EP (1) | EP2744745B1 (enExample) |
| JP (1) | JP6146922B2 (enExample) |
| KR (1) | KR101991705B1 (enExample) |
| CN (1) | CN103813977A (enExample) |
| AU (1) | AU2012295625B2 (enExample) |
| BR (1) | BR112014003379A2 (enExample) |
| CA (1) | CA2843696C (enExample) |
| EA (1) | EA027269B1 (enExample) |
| IN (1) | IN2014CN01924A (enExample) |
| PL (1) | PL2744745T3 (enExample) |
| UA (1) | UA112991C2 (enExample) |
| WO (1) | WO2013025105A1 (enExample) |
| ZA (1) | ZA201401748B (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3401410B1 (en) | 2010-06-26 | 2020-12-30 | Virdia, Inc. | Methods for production of sugar mixtures |
| IL206678A0 (en) | 2010-06-28 | 2010-12-30 | Hcl Cleantech Ltd | A method for the production of fermentable sugars |
| EP3401322B1 (en) | 2011-04-07 | 2022-06-08 | Virdia, LLC | Lignocellulose conversion processes and products |
| KR101975177B1 (ko) | 2011-08-16 | 2019-05-07 | 푸락 바이오켐 비.브이. | 발효 브로스 후처리에 유용한, 염산을 사용하는 침전에 의한 카복실산 마그네슘염으로부터의 카복실산의 회수 |
| EA035054B1 (ru) * | 2011-08-16 | 2020-04-22 | Пурак Биокем Б.В. | Извлечение карбоновой кислоты из ее магниевых солей путем осаждения с применением хлористоводородной кислоты, пригодное для выделения продукта реакции из ферментативного бульона |
| BR112014027474B1 (pt) | 2012-05-03 | 2020-03-17 | Virdia, Inc. | Métodos de processamento de materiais lingnocelulósicos |
| EP2821368A1 (en) * | 2013-07-03 | 2015-01-07 | PURAC Biochem BV | Method for processing magnesium chloride solutions |
| WO2016112134A1 (en) | 2015-01-07 | 2016-07-14 | Virdia, Inc. | Methods for extracting and converting hemicellulose sugars |
| BR112017025322A8 (pt) * | 2015-05-27 | 2022-08-23 | Virdia Inc | Processos integrados para recuperação de hidrolisato celulósico após hidrólise de polpa de celulose |
| EP3118185A1 (en) * | 2015-07-14 | 2017-01-18 | PURAC Biochem BV | Method for manufacturing succinic acid |
| EP3124434A1 (en) | 2015-07-31 | 2017-02-01 | PURAC Biochem BV | Method for providing a succinic acid solution |
| JP6667646B2 (ja) * | 2016-01-19 | 2020-03-18 | ピュラック バイオケム ビー． ブイ． | 塩化マグネシウム溶液の改良処理方法及びカルボン酸の製造方法 |
| US10933592B2 (en) | 2016-06-29 | 2021-03-02 | Valinge Innovation Ab | Method and device for inserting a tongue |
| CN114906812B (zh) * | 2022-06-01 | 2023-06-23 | 湖南吴赣药业有限公司 | 一种有机混酸分离纯化方法 |
| WO2024097329A1 (en) | 2022-11-02 | 2024-05-10 | Amalgamated Research Llc | Smb separator for organic acid purification using a strong acid cation resin |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE548967A (enExample) | 1954-12-08 | 1956-07-14 | ||
| GB9102393D0 (en) | 1991-02-05 | 1991-03-20 | Ici Plc | Production of terephthalic acid |
| AUPP437698A0 (en) * | 1998-06-30 | 1998-07-23 | Baumgart, Karl | Methods for treatment of coronary, carotid and other vascular disease |
| IL126264A0 (en) | 1998-09-17 | 1999-05-09 | Tami Inst For Research & Dev L | Process for preparing lactic acid |
| US6670505B1 (en) * | 2000-03-07 | 2003-12-30 | Eastman Chemical Company | Process for the recovery of organic acids from aqueous solutions |
| US6660505B2 (en) | 2000-06-22 | 2003-12-09 | Cognis Corporation | Isolation of carboxylic acids from fermentation broth |
| CN100534972C (zh) * | 2003-09-30 | 2009-09-02 | 味之素株式会社 | 从发酵液中纯化琥珀酸的方法 |
| JP2009079057A (ja) | 2005-04-22 | 2009-04-16 | Mitsubishi Chemicals Corp | ポリエステル及びその製造方法 |
| US20080223519A1 (en) | 2006-12-06 | 2008-09-18 | Locko George A | Polyamide polyols and polyurethanes, methods for making and using, and products made therefrom |
| FR2925068B1 (fr) * | 2007-12-13 | 2010-01-08 | Roquette Freres | Procedes de production d'acide succinique |
| CN101550079B (zh) * | 2009-05-12 | 2010-10-27 | 安徽丰原发酵技术工程研究有限公司 | 一种连续制备丁二酸的方法 |
| KR101051582B1 (ko) * | 2009-05-13 | 2011-07-22 | 삼성석유화학(주) | 발효액으로부터 숙신산을 분리 및 정제하는 방법 |
| US8431372B2 (en) * | 2009-06-19 | 2013-04-30 | Mbi International | Fermentation method using a magnesium compound containing oxygen |
| CN101748161B (zh) * | 2010-01-19 | 2012-06-06 | 南京工业大学 | 一种厌氧发酵纯化丁二酸的工艺 |
| KR101975177B1 (ko) | 2011-08-16 | 2019-05-07 | 푸락 바이오켐 비.브이. | 발효 브로스 후처리에 유용한, 염산을 사용하는 침전에 의한 카복실산 마그네슘염으로부터의 카복실산의 회수 |
-
2012
- 2012-08-16 CA CA2843696A patent/CA2843696C/en active Active
- 2012-08-16 JP JP2014525958A patent/JP6146922B2/ja not_active Expired - Fee Related
- 2012-08-16 WO PCT/NL2012/050572 patent/WO2013025105A1/en not_active Ceased
- 2012-08-16 KR KR1020147006790A patent/KR101991705B1/ko not_active Expired - Fee Related
- 2012-08-16 EP EP12750876.0A patent/EP2744745B1/en active Active
- 2012-08-16 US US14/238,666 patent/US9376364B2/en not_active Expired - Fee Related
- 2012-08-16 PL PL12750876T patent/PL2744745T3/pl unknown
- 2012-08-16 UA UAA201402003A patent/UA112991C2/uk unknown
- 2012-08-16 EA EA201490408A patent/EA027269B1/ru not_active IP Right Cessation
- 2012-08-16 AU AU2012295625A patent/AU2012295625B2/en not_active Ceased
- 2012-08-16 IN IN1924CHN2014 patent/IN2014CN01924A/en unknown
- 2012-08-16 CN CN201280045958.1A patent/CN103813977A/zh active Pending
- 2012-08-16 BR BR112014003379A patent/BR112014003379A2/pt not_active IP Right Cessation
-
2014
- 2014-03-10 ZA ZA2014/01748A patent/ZA201401748B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA2843696C (en) | 2019-09-24 |
| WO2013025105A8 (en) | 2014-04-10 |
| EA027269B1 (ru) | 2017-07-31 |
| EA201490408A1 (ru) | 2014-07-30 |
| UA112991C2 (uk) | 2016-11-25 |
| US20140200365A1 (en) | 2014-07-17 |
| JP2014524254A (ja) | 2014-09-22 |
| EP2744745B1 (en) | 2019-10-30 |
| CA2843696A1 (en) | 2013-02-21 |
| EP2744745A1 (en) | 2014-06-25 |
| JP6146922B2 (ja) | 2017-06-14 |
| CN103813977A (zh) | 2014-05-21 |
| KR20140064870A (ko) | 2014-05-28 |
| AU2012295625B2 (en) | 2016-05-12 |
| IN2014CN01924A (enExample) | 2015-05-29 |
| US9376364B2 (en) | 2016-06-28 |
| PL2744745T3 (pl) | 2020-05-18 |
| KR101991705B1 (ko) | 2019-06-21 |
| ZA201401748B (en) | 2015-01-28 |
| WO2013025105A1 (en) | 2013-02-21 |
| AU2012295625A1 (en) | 2014-03-20 |
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Legal Events
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| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09B | Patent application refused [chapter 9.2 patent gazette] | ||
| B12B | Appeal against refusal [chapter 12.2 patent gazette] | ||
| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 12A ANUIDADE. |
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| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2788 DE 11-06-2024 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |