CN1036990C - 沉淀二氧化硅 - Google Patents

沉淀二氧化硅 Download PDF

Info

Publication number
CN1036990C
CN1036990C CN94117058A CN94117058A CN1036990C CN 1036990 C CN1036990 C CN 1036990C CN 94117058 A CN94117058 A CN 94117058A CN 94117058 A CN94117058 A CN 94117058A CN 1036990 C CN1036990 C CN 1036990C
Authority
CN
China
Prior art keywords
surface area
ctab
pore volume
silica
bet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN94117058A
Other languages
English (en)
Chinese (zh)
Other versions
CN1109445A (zh
Inventor
H·埃施
U·戈尔
R·库尔曼
R·劳施
Original Assignee
Degussa GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25930239&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN1036990(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Degussa GmbH filed Critical Degussa GmbH
Publication of CN1109445A publication Critical patent/CN1109445A/zh
Application granted granted Critical
Publication of CN1036990C publication Critical patent/CN1036990C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C08K3/36—Silica
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/19—Oil-absorption capacity, e.g. DBP values

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Silicon Compounds (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
CN94117058A 1993-10-07 1994-10-05 沉淀二氧化硅 Expired - Fee Related CN1036990C (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DEP4334201.9 1993-10-07
DE4334201 1993-10-07
DEP4427137.9 1994-07-30
DE4427137A DE4427137B4 (de) 1993-10-07 1994-07-30 Fällungskieselsäure

Publications (2)

Publication Number Publication Date
CN1109445A CN1109445A (zh) 1995-10-04
CN1036990C true CN1036990C (zh) 1998-01-14

Family

ID=25930239

Family Applications (1)

Application Number Title Priority Date Filing Date
CN94117058A Expired - Fee Related CN1036990C (zh) 1993-10-07 1994-10-05 沉淀二氧化硅

Country Status (11)

Country Link
EP (1) EP0647591B1 (enExample)
JP (1) JP2556670B2 (enExample)
KR (1) KR0140827B1 (enExample)
CN (1) CN1036990C (enExample)
BR (1) BR9404019A (enExample)
DE (2) DE4427137B4 (enExample)
ES (1) ES2081223T3 (enExample)
FI (1) FI107143B (enExample)
RU (1) RU2076066C1 (enExample)
TR (1) TR28814A (enExample)
TW (1) TW288031B (enExample)

Families Citing this family (72)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6977065B1 (en) 1993-10-07 2005-12-20 Degussa Ag Precipitated silicas
DE19617039A1 (de) * 1995-06-01 1996-12-05 Degussa Fällungskieselsäuren, Verfahren zu ihrer Herstellung und Verwendung von vulkanisierbaren Kautschukmischungen
IN188702B (enExample) * 1995-06-01 2002-10-26 Degussa
DE19526476A1 (de) * 1995-07-20 1997-01-23 Degussa Fällungskieselsäure
DE19527278A1 (de) * 1995-07-26 1997-01-30 Degussa Fällungskieselsäure
DE19642448A1 (de) * 1996-03-27 1997-10-02 Degussa Fällungskieselsäure
CN1115295C (zh) * 1996-05-31 2003-07-23 Ppg工业俄亥俄公司 非晶形沉淀氧化硅
KR100342941B1 (ko) * 1996-05-31 2002-08-22 피피지 인더스트리즈 오하이오 인코포레이티드 무정형의침전된실리카
US5929156A (en) * 1997-05-02 1999-07-27 J.M. Huber Corporation Silica product for use in elastomers
US5891949A (en) * 1997-05-02 1999-04-06 J.M. Huber Corporation Natural rubber compound
DE19740440A1 (de) * 1997-09-15 1999-03-18 Degussa Leicht dispergierbare Fällungskieselsäure
IL122851A0 (en) * 1998-01-05 1998-08-16 Rotem Amfert Negev Ltd Optimally dispersible precipitated silica particulates process for their preparation and their use
JPH11236208A (ja) * 1998-02-25 1999-08-31 Nippon Silica Ind Co Ltd ゴム補強用含水ケイ酸
US6121346A (en) * 1998-03-02 2000-09-19 The Goodyear Tire & Rubber Company Rubber compositions containing fillers having aggregates containing different particle sizes
DE19840153A1 (de) 1998-09-03 2000-04-20 Degussa Fällungskieselsäure
JP2000319513A (ja) * 1999-05-12 2000-11-21 Nippon Silica Ind Co Ltd シリコーンゴム補強充填剤
US6624233B2 (en) 1999-05-31 2003-09-23 Pirelli Pneumatici S.P.A. Low rolling resistance tire for vehicles
EP1189767B1 (en) * 1999-05-31 2004-07-28 PIRELLI PNEUMATICI Società per Azioni Low rolling resistance tire for vehicles
HUP0204138A3 (en) * 1999-07-28 2004-08-30 Grace Gmbh & Co Kg Preciptated silica, a process to make it, and its use
DE10112652A1 (de) 2001-03-16 2002-09-19 Degussa Inhomogene Kieselsäuren für Elastomerenmischungen
DE10146325A1 (de) * 2001-09-20 2003-04-10 Degussa Fällungskieselsäure mit hohem BET/CTAB-Verhältnis
KR100560223B1 (ko) * 2002-06-05 2006-03-10 삼성코닝 주식회사 고정도 연마용 금속 산화물 분말 및 이의 제조방법
DE10330221A1 (de) * 2002-08-03 2004-02-12 Degussa Ag Hochdispersible Fällungskieselsäure
JP5144878B2 (ja) * 2002-08-03 2013-02-13 エボニック デグサ ゲーエムベーハー 高表面積沈降珪酸
DE10330118A1 (de) * 2002-08-03 2004-02-12 Degussa Ag Fällungskieselsäure mit hoher Oberfläche
DE50308181D1 (de) * 2002-08-03 2007-10-25 Degussa Hochdispersible fällungskieselsäure mit hoher oberfläche
BRPI0406904A (pt) 2003-01-22 2005-12-13 Degussa ácidos silìcicos especialmente precipitados para aplicações em borrachas
CN100572424C (zh) * 2003-08-19 2009-12-23 株式会社德山 二氧化硅填充橡胶颗粒体及其制造方法
DE102004005411A1 (de) * 2004-02-03 2005-08-18 Degussa Ag Hydrophobe Fällungskieselsäure für Entschäumerformulierungen
US10258576B2 (en) 2004-05-24 2019-04-16 Takeda As Particulate comprising a calcium-containing compound and a sugar alcohol
KR100893847B1 (ko) 2004-06-01 2009-04-17 니코메드 파마 에이에스 칼슘-함유 화합물을 활성 물질로서 함유하는 씹어먹거나흡입 및 삼킬 수 있는 태블릿
SE529160C2 (sv) * 2004-12-27 2007-05-15 Svenska Aerogel Ab En metod för framställning av agglomerat av utfällt silikamaterial, ett mikroporöst material innefattande sådana agglomerat och användning därav
JP4805584B2 (ja) 2005-01-21 2011-11-02 住友ゴム工業株式会社 トレッド用ゴム組成物およびそれからなるタイヤ
CN101128186B (zh) 2005-02-03 2013-07-03 奈科明制药有限公司 制备含钙组合物的快速湿聚结方法
JP5224820B2 (ja) 2005-02-03 2013-07-03 ニコメド ファーマ エイエス カルシウム含有化合物を含む組成物の溶融造粒
DE102005043201A1 (de) * 2005-09-09 2007-03-15 Degussa Ag Fällungskieselsäuren mit einer besonderen Porengrößenverteilung
UA95093C2 (uk) 2005-12-07 2011-07-11 Нікомед Фарма Ас Спосіб одержання кальцієвмісної сполуки
JP5420907B2 (ja) 2005-12-07 2014-02-19 タケダ ニコメド エイエス 予備圧縮されたカルシウム含有化合物
EP1803766B1 (en) 2005-12-28 2014-03-12 Sumitomo Rubber Industries, Ltd. Rubber composition for coating textile cord and tire using the same
DE102007004757A1 (de) * 2006-05-26 2007-11-29 Degussa Gmbh Fällungskieselsäuren mit speziellen Oberflächeneigenschaften
JP5108352B2 (ja) 2007-03-28 2012-12-26 東海ゴム工業株式会社 防振ゴム組成物
JP4896826B2 (ja) * 2007-06-21 2012-03-14 住友ゴム工業株式会社 トレッド用ゴム組成物およびこれを用いた空気入りタイヤ
DE102008017747A1 (de) * 2008-04-07 2009-10-08 Evonik Degussa Gmbh Gefällte Kieselsäuren als Verstärkerfüllstoff für Elastomermischungen
DE102008017731A1 (de) * 2008-04-07 2009-10-08 Continental Aktiengesellschaft Kautschukmischung
WO2010054845A1 (en) 2008-11-17 2010-05-20 Nycomed Pharma As Improved dissolution stability of calcium carbonate tablets
JP2012251134A (ja) * 2011-05-12 2012-12-20 Sumitomo Chemical Co Ltd 組成物
RU2502754C2 (ru) * 2011-07-20 2013-12-27 Общество с ограниченной ответственностью "Научно-технический центр "Кама" Резиновая смесь
CN103922346B (zh) * 2013-01-14 2016-05-18 上海华明高技术（集团）有限公司 高分散沉淀白炭黑的制备方法
CN106700147A (zh) * 2015-11-13 2017-05-24 中国石油化工股份有限公司 低滚动阻力的橡胶组合物和硫化橡胶及其制备方法和应用
EP3394161A4 (en) * 2015-12-23 2019-08-14 Tata Chemicals Limited PRECIPITATION SILICA
KR20210136160A (ko) * 2016-07-27 2021-11-16 와커 헤미 아게 개질된 침전 실리카의 제조 방법 및 이를 함유하는 조성물
CA3030383C (en) 2016-07-29 2023-02-21 Evonik Degussa Gmbh Method for producing hydrophobic heat insulation material
JP7050810B2 (ja) 2017-01-18 2022-04-08 エボニック オペレーションズ ゲーエムベーハー 造粒体状断熱材およびその製造方法
DE102017209782A1 (de) 2017-06-09 2018-12-13 Evonik Degussa Gmbh Verfahren zur Wärmedämmung eines evakuierbaren Behälters
KR102690236B1 (ko) 2017-12-27 2024-08-01 로디아 오퍼레이션스 실리카 현탁액
PL3746403T3 (pl) 2018-02-01 2024-09-30 Rhodia Operations Zawiesina krzemionki w rozpuszczalniku organicznym i sposób jej wytwarzania
CN108439414A (zh) * 2018-02-11 2018-08-24 确成硅化学股份有限公司 一种pH值摆动法制备高分散大孔容沉淀二氧化硅的方法
WO2019170264A1 (de) 2018-03-05 2019-09-12 Evonik Degussa Gmbh Verfahren zur herstellung eines aerogelmaterials
KR102756383B1 (ko) 2018-07-13 2025-01-21 로디아 오퍼레이션스 가공처리 성질이 개선된 침전 실리카
EP3597615A1 (en) 2018-07-17 2020-01-22 Evonik Operations GmbH Granular mixed oxide material and thermal insulating composition on its basis
US12030810B2 (en) 2018-07-17 2024-07-09 Evonik Operations Gmbh Thermal insulating composition based on fumed silica granulates, processes for its preparation and uses thereof
EP3823942A1 (en) 2018-07-18 2021-05-26 Evonik Operations GmbH Process for hydrophobizing shaped insulation-material bodies based on silica at ambient pressure
EP4045334A1 (en) 2019-10-15 2022-08-24 Rhodia Operations Process for the preparation of modified silica, modified silica and its uses
WO2021190979A1 (en) 2020-03-24 2021-09-30 Rhodia Operations Whitening oral care compositions
CN115485239B (zh) 2020-04-30 2024-08-30 赢创运营有限公司 具有增大的碱性稳定性的二氧化硅气凝胶
EP3992147A1 (de) * 2020-10-28 2022-05-04 Evonik Operations GmbH Gefällte kieselsäuren, verfahren zur deren herstellung und deren verwendung
WO2022101015A1 (en) * 2020-11-10 2022-05-19 Rhodia Operations Whitening oral care compositions
JP2024511855A (ja) 2021-04-02 2024-03-15 ローディア オペレーションズ 新規なシリカ、その調製のための方法、及びその使用
CN114132938B (zh) * 2021-12-08 2022-05-24 金三江(肇庆)硅材料股份有限公司 一种高吸油值低比表面积二氧化硅及其制备方法
US20240158615A1 (en) 2022-11-02 2024-05-16 The Goodyear Tire & Rubber Company Precipitated silica pretreated with a coupling agent and polyethylene glycol for a rubber composition
CN120513274A (zh) 2022-11-14 2025-08-19 罗地亚经营管理公司 改性沉淀二氧化硅、其制造和用途
US20240326361A1 (en) 2023-03-29 2024-10-03 The Goodyear Tire & Rubber Company Sealant composition for self-sealing pneumatic tire

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0031271A1 (fr) * 1979-12-20 1981-07-01 Rhone-Poulenc Chimie Silice de précipitation, notamment utilisable comme charge renforçante
EP0157703A1 (fr) * 1984-04-06 1985-10-09 Rhone-Poulenc Chimie Nouvelle silice précipitée à caractères morphologiques améliorés, procédé pour son obention et application, notamment comme charge
EP0308165A2 (en) * 1987-09-15 1989-03-22 Unilever Plc Silicas
EP0341383A2 (de) * 1988-05-07 1989-11-15 Degussa Aktiengesellschaft Feinteilige Fällungskieselsäure mit hoher Struktur, Verfahren zu seiner Herstellung und Verwendung
EP0407262A1 (fr) * 1989-07-03 1991-01-09 Rhone-Poulenc Chimie Silice à porosité controlée et son procédé d'obtention

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL289590A (enExample) * 1962-03-02
FR2208948B1 (enExample) * 1972-08-24 1977-02-25 Sifrance
FR2646673B1 (fr) * 1989-05-02 1991-09-06 Rhone Poulenc Chimie Silice sous forme de bille, procede de preparation et son utilisation au renforcement des elastomeres
FR2673187B1 (fr) * 1991-02-25 1994-07-01 Michelin & Cie Composition de caoutchouc et enveloppes de pneumatiques a base de ladite composition.
FR2678259B1 (fr) * 1991-06-26 1993-11-05 Rhone Poulenc Chimie Nouvelles silices precipitees sous forme de granules ou de poudres, procedes de synthese et utilisation au renforcement des elastomeres.

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0031271A1 (fr) * 1979-12-20 1981-07-01 Rhone-Poulenc Chimie Silice de précipitation, notamment utilisable comme charge renforçante
EP0157703A1 (fr) * 1984-04-06 1985-10-09 Rhone-Poulenc Chimie Nouvelle silice précipitée à caractères morphologiques améliorés, procédé pour son obention et application, notamment comme charge
EP0308165A2 (en) * 1987-09-15 1989-03-22 Unilever Plc Silicas
EP0341383A2 (de) * 1988-05-07 1989-11-15 Degussa Aktiengesellschaft Feinteilige Fällungskieselsäure mit hoher Struktur, Verfahren zu seiner Herstellung und Verwendung
EP0407262A1 (fr) * 1989-07-03 1991-01-09 Rhone-Poulenc Chimie Silice à porosité controlée et son procédé d'obtention

Also Published As

Publication number Publication date
RU94035656A (ru) 1997-04-20
JP2556670B2 (ja) 1996-11-20
RU2076066C1 (ru) 1997-03-27
EP0647591B1 (de) 1995-12-20
CN1109445A (zh) 1995-10-04
FI107143B (fi) 2001-06-15
KR0140827B1 (ko) 1998-06-01
DE4427137B4 (de) 2007-08-23
DE59400068D1 (de) 1996-02-01
KR950011329A (ko) 1995-05-15
TR28814A (tr) 1997-04-03
EP0647591A1 (de) 1995-04-12
BR9404019A (pt) 1995-06-27
DE4427137A1 (de) 1995-04-13
JPH07172815A (ja) 1995-07-11
TW288031B (enExample) 1996-10-11
ES2081223T3 (es) 1996-02-16
FI944679A0 (fi) 1994-10-06
FI944679L (fi) 1995-04-08

Similar Documents

Publication Publication Date Title
CN1036990C (zh) 沉淀二氧化硅
US5846506A (en) Precipitated silicas
CN1310835C (zh) 高bet/ctab比的沉淀二氧化硅
JP3795237B2 (ja) 易分散性沈降ケイ酸
CN1259364C (zh) 天然橡胶母体混合物及其制造方法和天然橡胶组成物
JP3958898B2 (ja) 沈降ケイ酸、その製法並びにそれを含有するゴム混合物及び加硫ゴム
CN1262591C (zh) 用于制造公路型轮胎的以二氧化硅为基础的橡胶组合物
CN1217859C (zh) 补强性铝填料和含有这种填料的橡胶组合物
CN1263109A (zh) 橡胶粉末及其制备方法
JP2009132615A (ja) 少なくとも二つの珪酸フラクシヨンを含有する珪酸、その製法、これを含有するエラストマー混合物及び充填剤としてのその使用
US6977065B1 (en) Precipitated silicas
CN1580106A (zh) 炭黑
CN103890105A (zh) 经处理的填料、含有其的组合物和由其制成的制品
JP2005533735A (ja) 調整可能なｂｅｔ／ｃｔａｂ‐比を有するアルミニウム含有の沈降珪酸
CN1262588C (zh) 包括改性填料的粉状橡胶粉、应用及其制备方法
CN1208375C (zh) 包含改性填料的粉状橡胶粉、其制备方法以及其应用
JP2000351847A (ja) ゴム粉末ならびに微粉状充填剤含有ゴムおよび加硫性ゴム混合物の製造法
US7071257B2 (en) Precipitated silicas
CN1189522C (zh) 用作聚合物组合物中的增强填料的组合物
CN1391595A (zh) 橡胶组合物及其生产方法
CN1323329A (zh) 碳酸羟铝、碳酸羟氧化铝或碳酸氧化铝作为填料在橡胶混合物中的应用
TW200400920A (en) Precipitated silica containing aluminum with adjustable BET/CTAB ratio
TW202110737A (zh) 二氧化矽-石墨烯碳複合粒子及包括此等粒子之彈性體材料
HK1194752A (en) Treated fillers, compositions containing same, and articles prepared therefrom

Legal Events

Date Code Title Description
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C06 Publication
PB01 Publication
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: DUESSELDORF, FEDERAL GERMANY

Free format text: FORMER NAME OR ADDRESS: HANAU, GERMANY

CP03 Change of name, title or address

Patentee address after: Dusseldorf, Federal Republic of Germany

Patentee address before: Federal Republic of Germany, Kazakhstan

C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee