CN103666078A - Ultraviolet light curing ink for ink jet printer and preparation method of ultraviolet light curing ink - Google Patents
Ultraviolet light curing ink for ink jet printer and preparation method of ultraviolet light curing ink Download PDFInfo
- Publication number
- CN103666078A CN103666078A CN201310619066.4A CN201310619066A CN103666078A CN 103666078 A CN103666078 A CN 103666078A CN 201310619066 A CN201310619066 A CN 201310619066A CN 103666078 A CN103666078 A CN 103666078A
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- ink
- ultraviolet light
- light curing
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- Granted
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- -1 polytetrafluoroethylene Polymers 0.000 claims abstract description 17
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims abstract description 8
- FDLQZKYLHJJBHD-UHFFFAOYSA-N [3-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=CC(CN)=C1 FDLQZKYLHJJBHD-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003822 epoxy resin Substances 0.000 claims abstract description 7
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 4
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229920000728 polyester Polymers 0.000 claims abstract description 4
- 229920000570 polyether Polymers 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000049 pigment Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 125000004423 acyloxy group Chemical group 0.000 claims description 3
- 150000004645 aluminates Chemical class 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- 229910052760 oxygen Inorganic materials 0.000 claims description 3
- 239000001301 oxygen Substances 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 239000002904 solvent Substances 0.000 abstract description 9
- 238000005265 energy consumption Methods 0.000 abstract description 2
- KUDUQBURMYMBIJ-UHFFFAOYSA-N 2-prop-2-enoyloxyethyl prop-2-enoate Chemical compound C=CC(=O)OCCOC(=O)C=C KUDUQBURMYMBIJ-UHFFFAOYSA-N 0.000 abstract 2
- SCNFOPZWAVWOEF-UHFFFAOYSA-N 1-(4,5-dihydroimidazol-1-yl)-N-ethylheptadec-1-en-2-amine Chemical compound C(C)NC(=CN1C=NCC1)CCCCCCCCCCCCCCC SCNFOPZWAVWOEF-UHFFFAOYSA-N 0.000 abstract 1
- ZDQNWDNMNKSMHI-UHFFFAOYSA-N 1-[2-(2-prop-2-enoyloxypropoxy)propoxy]propan-2-yl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COCC(C)OC(=O)C=C ZDQNWDNMNKSMHI-UHFFFAOYSA-N 0.000 abstract 1
- 239000005909 Kieselgur Substances 0.000 abstract 1
- 239000012860 organic pigment Substances 0.000 abstract 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 abstract 1
- 239000004810 polytetrafluoroethylene Substances 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- 239000000976 ink Substances 0.000 description 32
- 239000002932 luster Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000010422 painting Methods 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
- Ink Jet Recording Methods And Recording Media Thereof (AREA)
Abstract
The invention discloses ultraviolet light curing ink for an ink jet printer. The ultraviolet light curing ink is characterized by being made from raw materials in parts by weight as follows: 1-2 parts of organic pigments, 2-3 parts of polytetrafluoroethylene, 1-2 parts of diatomaceous earth, 1-2 parts of 2-ethylamino heptadecenyl imidazoline, 30-34 parts of E-12 epoxy resin, 7-10 parts of 1.6 ethylene glycol diacrylate, 4-6 parts of m-xylylenediamine, 12-16 parts of tripropylene glycol diacrylate, 8-10 parts of polyester acrylate, 12-15 parts of polyether acrylate, 1-2 parts of distearoyl isopropoxy aluminate, 8-10 parts of ethyl acrylate, 5-9 parts of a 2959 photoinitiator and 4-5 parts of an auxiliary. The auxiliary improves the toughness of the ink, so that the ink can be uniformly dispersed; and the ink doesn't contain a volatile solvent and has small pollution on the environment, the energy consumption is small, the printing smoothness is good, the curing speed is high, the color of a pattern is bright, a printing substrate is wide in application range, and the preparation process is simple.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of inkjet printer UV curable ink and preparation method thereof.
Background technology
Large inkjet printer ink, according to the difference of its main ingredient, can be divided into three major types: water color ink, solvent type ink and UV curable ink.Water color ink cost is low, not pollution, bright in luster, but because the picture of water color ink air brushing is difficult for being dried and easily by Absorption of Medium, it requires painting medium to have special coating, is mainly used on paper and various fiber-like (cloth) ground, cated painting medium.And solvent in solvent type ink generally can directly merge with ground, do not require that medium is covered with coating, and its evaporation rate is fast, meet the requirement of flying print.But the problem of solvent type ink maximum is exactly friendly not to environment, because volatilizable organic content is high in ink, is certain in the long run be subject to many limitations gradually.
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can produce different-energy, the monomer polymerization in different ink vehicles is become to polymkeric substance, so the look film of UV ink has good machinery and chemical property.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, resistance to solvent, wear resisting property is good.In UV ink, light trigger is a kind of light activated compound that is subject to, and after absorb light is shone, is excited into free radical, and energy is transferred to photosensitivity molecule or photocrosslinking agent, makes UV China ink that photocuring reaction occur.UV China ink has become a kind of more ripe ink technology at present, and its pollutant emission is almost nil.Except not containing solvent, UV China ink is also just like being difficult for scumming, and site is clear, the bright-coloured light of mass colour, the advantage such as chemical resistance is excellent, low-consuming.
Summary of the invention
The object of this invention is to provide a kind of inkjet printer UV curable ink and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
An inkjet printer UV curable ink, is made by the raw material of following weight part: pigment dyestuff 1-2, tetrafluoroethylene 2-3, diatomite 1-2,2-ethylamino 17 alkenyl imidazoline 1-2, E-12 epoxy resin 30-34,1.6 glycol diacrylate 7-10, m-xylene diamine 4-6, tri (propylene glycol) diacrylate 12-16, polyester acrylate 8-10, polyether acrylate 12-15, sec.-propyl distearyl acyl-oxygen base Aluminate 1-2, ethyl propenoate 8-10,2959 light trigger 5-9, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 1-2, linking agent TAC2-3, polyisobutene 2-3, sec.-propyl three (dioctylphyrophosphoric acid acyloxy) titanic acid ester 2-3, phenylformic acid amine 1-2, Viscoat 295 10-12, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Inkjet printer UV curable ink of the present invention, by following concrete steps, made: first add pigment dyestuff, tetrafluoroethylene, diatomite, 2-ethylamino 17 alkenyl imidazolines, E-12 epoxy resin, 1.6 glycol diacrylates, m-xylene diamine, tri (propylene glycol) diacrylate stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 2959 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 2959 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The invention has the beneficial effects as follows: auxiliary agent of the present invention has improved the toughness of ink, make distributes ink even; Ink non-volatility solvent of the present invention, environmental pollution is little, energy consumption is few, print that fluency is good, solidification rate fast, pattern color and luster is beautiful, it is wide to print ground range of applicability, and preparation technology is simple.
Specific embodiments
Below by specific examples, the present invention is described in detail.
An inkjet printer UV curable ink, by following weight part (kilogram) raw material make: pigment dyestuff 1, tetrafluoroethylene 2, diatomite 1,2-ethylamino 17 alkenyl imidazolines 1, E-12 epoxy resin 30,1.6 glycol diacrylates 7, m-xylene diamine 4, tri (propylene glycol) diacrylate 12, polyester acrylate 8, polyether acrylate 12, sec.-propyl distearyl acyl-oxygen base Aluminate 1, ethyl propenoate 8,2959 light triggers 5, auxiliary agent 4;
Described auxiliary agent by following weight part (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, Silane coupling agent KH550 1, linking agent TAC2, polyisobutene 2, sec.-propyl three (dioctylphyrophosphoric acid acyloxy) titanic acid ester 2, phenylformic acid amine 1, Viscoat 295 10, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Inkjet printer UV curable ink of the present invention, by following concrete steps, made: first add pigment dyestuff, tetrafluoroethylene, diatomite, 2-ethylamino 17 alkenyl imidazolines, E-12 epoxy resin, 1.6 glycol diacrylates, m-xylene diamine, tri (propylene glycol) diacrylate stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 2959 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 2959 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The ink of gained, is used cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. an inkjet printer UV curable ink, it is characterized in that, by the raw material of following weight part, made: pigment dyestuff 1-2, tetrafluoroethylene 2-3, diatomite 1-2,2-ethylamino 17 alkenyl imidazoline 1-2, E-12 epoxy resin 30-34,1.6 glycol diacrylate 7-10, m-xylene diamine 4-6, tri (propylene glycol) diacrylate 12-16, polyester acrylate 8-10, polyether acrylate 12-15, sec.-propyl distearyl acyl-oxygen base Aluminate 1-2, ethyl propenoate 8-10,2959 light trigger 5-9, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 1-2, linking agent TAC2-3, polyisobutene 2-3, sec.-propyl three (dioctylphyrophosphoric acid acyloxy) titanic acid ester 2-3, phenylformic acid amine 1-2, Viscoat 295 10-12, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
2. inkjet printer UV curable ink according to claim 1, it is characterized in that, by following concrete steps, made: first add pigment dyestuff, tetrafluoroethylene, diatomite, 2-ethylamino 17 alkenyl imidazolines, E-12 epoxy resin, 1.6 glycol diacrylates, m-xylene diamine, tri (propylene glycol) diacrylate stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 2959 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 2959 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310619066.4A CN103666078B (en) | 2013-11-29 | 2013-11-29 | A kind of inkjet printer UV curable ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310619066.4A CN103666078B (en) | 2013-11-29 | 2013-11-29 | A kind of inkjet printer UV curable ink and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666078A true CN103666078A (en) | 2014-03-26 |
| CN103666078B CN103666078B (en) | 2016-04-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310619066.4A Active CN103666078B (en) | 2013-11-29 | 2013-11-29 | A kind of inkjet printer UV curable ink and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1415679A (en) * | 2001-11-02 | 2003-05-07 | 北京英力科技发展有限公司 | Visible light solidified compsn. |
| CN101560348A (en) * | 2009-05-25 | 2009-10-21 | 王景泉 | Ultraviolet light curing offset printing ink and preparation method thereof |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
-
2013
- 2013-11-29 CN CN201310619066.4A patent/CN103666078B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1415679A (en) * | 2001-11-02 | 2003-05-07 | 北京英力科技发展有限公司 | Visible light solidified compsn. |
| CN101560348A (en) * | 2009-05-25 | 2009-10-21 | 王景泉 | Ultraviolet light curing offset printing ink and preparation method thereof |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
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| Publication number | Publication date |
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| CN103666078B (en) | 2016-04-27 |
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| PB01 | Publication | ||
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB02 | Change of applicant information |
Inventor after: Wei Renshan Inventor after: Yi Bin Inventor before: Dong Liangqing |
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| COR | Change of bibliographic data | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20161215 Address after: Baoan District Shiyan street of Shenzhen city in Guangdong Province on the 518000 Avenue house Tian Industrial Zone tenth Patentee after: Shenzhen Haizhonghui Ink Products Co.,Ltd. Address before: South Taibai town 243161 Anhui city of Ma'anshan province Dangtu County Xintai white road Patentee before: DANGTU KEHUI TRADE Co.,Ltd. |
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| CP03 | Change of name, title or address |
Address after: 518000 Hangwei Avenue, Shangwu Community, Shiyan Street, Baoan District, Shenzhen City, Guangdong Province Patentee after: Shenzhen Haizhonghui New Material Technology Co.,Ltd. Address before: 518000 Tianxin Industrial Zone, Shangwu Avenue, Shiyan Street, Baoan District, Shenzhen City, Guangdong Province Patentee before: Shenzhen Haizhonghui Ink Products Co.,Ltd. |
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Effective date of registration: 20230518 Address after: 511500 No. 15 Xiongxing Industrial Avenue, Yinzhan Community, Longtang Town, Qingcheng District, Qingyuan City, Guangdong Province Patentee after: Guangdong Haihui New Material Technology Co.,Ltd. Address before: 518000 Hangwei Avenue, Shangwu Community, Shiyan Street, Baoan District, Shenzhen City, Guangdong Province Patentee before: Shenzhen Haizhonghui New Material Technology Co.,Ltd. |
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