CN103666073A - Novel ultraviolet-curable silk-screen pearlescent ink and preparation method thereof - Google Patents
Novel ultraviolet-curable silk-screen pearlescent ink and preparation method thereof Download PDFInfo
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- CN103666073A CN103666073A CN201310618215.5A CN201310618215A CN103666073A CN 103666073 A CN103666073 A CN 103666073A CN 201310618215 A CN201310618215 A CN 201310618215A CN 103666073 A CN103666073 A CN 103666073A
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Abstract
The invention discloses novel ultraviolet-curable silk-screen pearlescent ink. The ink is characterized in that the ink is made from raw materials in parts by weight as follows: 1-3 parts of organic pigment, 20-24 parts of urethane acrylate, 1-2 parts of expanded graphite, 1-3 parts of expanded perlite powder, 1-2 parts of selenium acetylacetonate, 5-8 parts of 2,4,6-trimethylbenzoyldiphenyl phosphine oxide, 3-4 parts of linseed oil, 12-14 parts of organic silicone resin, 2-3 parts of polytetrafluoroethene, 10-12 parts of trimethylolpropane triacrylate, 4-8 parts of a 1173 photoinitiator, 2-4 parts of zinc naphthenate, 1-2 parts of diethylamine and 4-5 parts of an assistant. The assistant can improve the toughness of the ink, so that the ink is even in dispersion, and the stability of the ink is maintained; the ink has good adhesive force to printing stocks and has good flexibility, abrasive resistance, scratch resistance and resistance to various solvents, and silk-screen printing requirements can be met.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of new ultra-violet photocuring silk screen pearl ink and preparation method thereof.
Background technology
Silk screen printing is that silk fabrics, synthetic fabrics or wire cloth are stretched tight on screen frame, adopts manual method of carving paint film or photochemistry plate-making to make screen printing forme.Modern screen printing technique, to utilize sensitive materials by photomechanical method, to make the flat carriers such as screen printing forme (making the silk screen hole of picture and text part on screen printing forme is through hole, and the silk screen hole of non-graphic part is plugged) oil painting, etching, pictorial poster, business card, binding and layout front cover, commodity packaging, product tag, dyeing textile product, glass and metal etc.
Pearly pigment is as a kind of mode of printing of special-effect, rely on its unique pearliness, make printed matter surface produce graceful unique, the soft pleasing reward effect of looking, the characteristic simultaneously with anti-duplicating, there is certain antifalse effect, in numerous mode of printings, take the course of its own, become popular a kind of false proof and decorating printing technology.The application of pearly-lustre silk-screen ink can well embody the distinctive effect of pearly-lustre, in fields such as banknote, security, Package and labels, is widely applied.
Summary of the invention
The object of this invention is to provide a kind of new ultra-violet photocuring silk screen pearl ink and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
A kind of new ultra-violet photocuring silk screen pearl ink, raw material by following weight part is made: pigment dyestuff 1-3, urethane acrylate 20-24, expanded graphite 1-2, swelling perlite powder 1-3, methyl ethyl diketone selenium 1-2,2,4,6-trimethylbenzoyl diphenyl phosphine oxide 5-8, oleum lini 3-4, silicone resin 12-14, tetrafluoroethylene 2-3, Viscoat 295 10-12,1173 light trigger 4-8, zinc naphthenate 2-4, diethylamine 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 1-2, linking agent TAC2-3, polyisobutene 2-3, sec.-propyl three (dioctylphyrophosphoric acid acyloxy) titanic acid ester 2-3, phenylformic acid amine 1-2, Viscoat 295 10-12, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
New ultra-violet photocuring silk screen pearl ink of the present invention, by following concrete steps, made: first add pigment dyestuff, urethane acrylate, expanded graphite, swelling perlite powder, methyl ethyl diketone selenium stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1173 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1173 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The invention has the beneficial effects as follows: auxiliary agent of the present invention has improved the toughness of ink, make distributes ink even, and maintained the stability of ink; Between ink of the present invention and each stock, all there is good sticking power, snappiness, wear-resisting scratch resistance intensity, resistance to all kinds of solvent natures, can meet the requirement of silk screen printing.
Specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of new ultra-violet photocuring silk screen pearl ink, by following weight part (kilogram) raw material make: pigment dyestuff 1, urethane acrylate 20, expanded graphite 1, swelling perlite powder 1, methyl ethyl diketone selenium 1,2,4,6-trimethylbenzoyl diphenyl phosphine oxide 5, oleum lini 3, silicone resin 12, tetrafluoroethylene 2, Viscoat 295 10,1173 light triggers 4, zinc naphthenate 2, diethylamine 1, auxiliary agent 4;
Described auxiliary agent by following weight part (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, Silane coupling agent KH550 1, linking agent TAC2, polyisobutene 2, sec.-propyl three (dioctylphyrophosphoric acid acyloxy) titanic acid ester 2, phenylformic acid amine 1, Viscoat 295 10, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
New ultra-violet photocuring silk screen pearl ink of the present invention, by following concrete steps, made: first add pigment dyestuff, urethane acrylate, expanded graphite, swelling perlite powder, methyl ethyl diketone selenium stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1173 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1173 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The ink of gained, is used cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. a new ultra-violet photocuring silk screen pearl ink, it is characterized in that, raw material by following weight part is made: pigment dyestuff 1-3, urethane acrylate 20-24, expanded graphite 1-2, swelling perlite powder 1-3, methyl ethyl diketone selenium 1-2,2,4,6-trimethylbenzoyl diphenyl phosphine oxide 5-8, oleum lini 3-4, silicone resin 12-14, tetrafluoroethylene 2-3, Viscoat 295 10-12,1173 light trigger 4-8, zinc naphthenate 2-4, diethylamine 1-2, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, Silane coupling agent KH550 1-2, linking agent TAC2-3, polyisobutene 2-3, sec.-propyl three (dioctylphyrophosphoric acid acyloxy) titanic acid ester 2-3, phenylformic acid amine 1-2, Viscoat 295 10-12, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
2. new ultra-violet photocuring silk screen pearl ink according to claim 1, it is characterized in that, by following concrete steps, made: first add pigment dyestuff, urethane acrylate, expanded graphite, swelling perlite powder, methyl ethyl diketone selenium stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1173 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1173 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310618215.5A CN103666073B (en) | 2013-11-29 | 2013-11-29 | A kind of Novel ultraviolet-curable silk-screen pearlescent ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310618215.5A CN103666073B (en) | 2013-11-29 | 2013-11-29 | A kind of Novel ultraviolet-curable silk-screen pearlescent ink and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103666073A true CN103666073A (en) | 2014-03-26 |
| CN103666073B CN103666073B (en) | 2016-04-27 |
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| CN201310618215.5A Expired - Fee Related CN103666073B (en) | 2013-11-29 | 2013-11-29 | A kind of Novel ultraviolet-curable silk-screen pearlescent ink and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104194478A (en) * | 2014-07-28 | 2014-12-10 | 蚌埠首创滤清器有限公司 | Organic silicon resin printing ink dyed by soy sauce |
| CN106398387A (en) * | 2016-10-07 | 2017-02-15 | 苏州高精特专信息科技有限公司 | Optical fiber coloring ink capable of being solidified by LED and preparing method thereof |
| CN110437676A (en) * | 2019-09-16 | 2019-11-12 | 杭州科望特种油墨有限公司 | One kind is with scape color shifting ink |
| CN115433515A (en) * | 2022-09-19 | 2022-12-06 | 广东希贵光固化材料有限公司 | High-hardness and super-wear-resistant UV transfer adhesive and preparation method thereof |
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| CN1415679A (en) * | 2001-11-02 | 2003-05-07 | 北京英力科技发展有限公司 | Visible light solidified compsn. |
| CN101560348A (en) * | 2009-05-25 | 2009-10-21 | 王景泉 | Ultraviolet light curing offset printing ink and preparation method thereof |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
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2013
- 2013-11-29 CN CN201310618215.5A patent/CN103666073B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1415679A (en) * | 2001-11-02 | 2003-05-07 | 北京英力科技发展有限公司 | Visible light solidified compsn. |
| CN101560348A (en) * | 2009-05-25 | 2009-10-21 | 王景泉 | Ultraviolet light curing offset printing ink and preparation method thereof |
| CN101974267A (en) * | 2010-11-04 | 2011-02-16 | 中钞油墨有限公司 | Aqueous ultraviolet light curing pearlescent silk screen ink and preparation method thereof |
| CN102634251A (en) * | 2012-04-10 | 2012-08-15 | 中钞油墨有限公司 | Photo-curing silk screen pearly-luster ink applicable to different printing substrates and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104194478A (en) * | 2014-07-28 | 2014-12-10 | 蚌埠首创滤清器有限公司 | Organic silicon resin printing ink dyed by soy sauce |
| CN106398387A (en) * | 2016-10-07 | 2017-02-15 | 苏州高精特专信息科技有限公司 | Optical fiber coloring ink capable of being solidified by LED and preparing method thereof |
| CN106398387B (en) * | 2016-10-07 | 2020-11-13 | 广东昊辉新材料有限公司 | Optical fiber coloring ink capable of being cured by LED lamp and manufacturing method thereof |
| CN110437676A (en) * | 2019-09-16 | 2019-11-12 | 杭州科望特种油墨有限公司 | One kind is with scape color shifting ink |
| CN115433515A (en) * | 2022-09-19 | 2022-12-06 | 广东希贵光固化材料有限公司 | High-hardness and super-wear-resistant UV transfer adhesive and preparation method thereof |
Also Published As
| Publication number | Publication date |
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| CN103666073B (en) | 2016-04-27 |
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Inventor after: He Yuankai Inventor before: Dong Liangqing |
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Effective date of registration: 20170307 Address after: 523430 Guangdong city in Dongguan Province town of Liaobu Fu Ling Industrial Zone Zhushan Basin Patentee after: Dongguan Haiya printing material Co. Ltd. Address before: South Taibai town 243161 Anhui city of Ma'anshan province Dangtu County Xintai white road Patentee before: Dangtu County Ke Hui commerce and trade Co., Ltd |
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