CN103666068A - Energy-saving and environment-friendly UV-cured printing ink - Google Patents
Energy-saving and environment-friendly UV-cured printing ink Download PDFInfo
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- CN103666068A CN103666068A CN201310602412.8A CN201310602412A CN103666068A CN 103666068 A CN103666068 A CN 103666068A CN 201310602412 A CN201310602412 A CN 201310602412A CN 103666068 A CN103666068 A CN 103666068A
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- printing ink
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- 238000007639 printing Methods 0.000 title abstract 3
- PQLMXFQTAMDXIZ-UHFFFAOYSA-N isoamyl butyrate Chemical compound CCCC(=O)OCCC(C)C PQLMXFQTAMDXIZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 11
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910021536 Zeolite Inorganic materials 0.000 claims abstract description 7
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229920003180 amino resin Polymers 0.000 claims abstract description 7
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims abstract description 7
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940094941 isoamyl butyrate Drugs 0.000 claims abstract description 7
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000010457 zeolite Substances 0.000 claims abstract description 7
- OOJBEQBXIJTMIN-UHFFFAOYSA-N europium 1,1,1-trifluoropentane-2,4-dione Chemical compound FC(C(=O)CC(C)=O)(F)F.[Eu] OOJBEQBXIJTMIN-UHFFFAOYSA-N 0.000 claims abstract description 4
- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000000976 ink Substances 0.000 claims description 24
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 238000003848 UV Light-Curing Methods 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000049 pigment Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims description 3
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 244000077995 Coix lacryma jobi Species 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- APZPSKFMSWZPKL-UHFFFAOYSA-N [3-hydroxy-2,2-bis(hydroxymethyl)propyl] 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC(CO)(CO)CO APZPSKFMSWZPKL-UHFFFAOYSA-N 0.000 claims description 3
- 229940022663 acetate Drugs 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 239000002904 solvent Substances 0.000 abstract description 5
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052737 gold Inorganic materials 0.000 abstract description 2
- 239000010931 gold Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 229910052709 silver Inorganic materials 0.000 abstract description 2
- 239000004332 silver Substances 0.000 abstract description 2
- ZDQNWDNMNKSMHI-UHFFFAOYSA-N 1-[2-(2-prop-2-enoyloxypropoxy)propoxy]propan-2-yl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COCC(C)OC(=O)C=C ZDQNWDNMNKSMHI-UHFFFAOYSA-N 0.000 abstract 1
- SVONRAPFKPVNKG-UHFFFAOYSA-N 2-ethoxyethyl acetate Chemical compound CCOCCOC(C)=O SVONRAPFKPVNKG-UHFFFAOYSA-N 0.000 abstract 1
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 abstract 1
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 abstract 1
- 239000000654 additive Substances 0.000 abstract 1
- 239000001099 ammonium carbonate Substances 0.000 abstract 1
- 239000012975 dibutyltin dilaurate Substances 0.000 abstract 1
- 125000005442 diisocyanate group Chemical group 0.000 abstract 1
- 239000012860 organic pigment Substances 0.000 abstract 1
- 238000007650 screen-printing Methods 0.000 abstract 1
- 240000001624 Espostoa lanata Species 0.000 description 2
- 235000009161 Espostoa lanata Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000011087 paperboard Substances 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000036211 photosensitivity Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000002211 ultraviolet spectrum Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses an energy-saving and environment-friendly UV-cured printing ink which is characterized by being prepared from the following raw materials in parts by weight:1-3 parts of an organic pigment, 20-23 parts of amino resin, 1-2 parts of ammonium bicarbonate, 1-2 parts of zeolite, 13-15 parts of ethylene glycol monoethyl ether acetate, 11-13 parts of isoamyl butyrate,12-14 parts of trimethylolpropane triacrylate, 1-1.1 parts of cobalt naphthenate, 1-2 parts of dibutyltin dilaurate, 10-12 parts of tripropylene glycol diacrylate, 5-8 parts of vinegar naphtha, 10-12 parts of UV epoxy acrylate, 4-8 parts of photoinitiator 1173, 4-5 parts of europium trifluoroacetylacetone, 5-6 parts of diisocyanate, and 4-5 parts of additives. The printing ink provided by the invention can be printed on a gold and silver cardboard or a PVC card at one step in a screen printing manner so as to improve production efficiency and save cost, and contains no solvent so as to reduce harm to a human body and environment pollution.
Description
Technical field
The present invention relates to a kind of ink and preparation method thereof, particularly a kind of energy-conserving and environment-protective UV curing inks and preparation method thereof.
Background technology
Ultraviolet light polymerization (UV) ink refers under uviolizing, utilizes the UV-light of different wave length and energy to make ink film forming and dry ink.Utilize different UV spectrum, can produce different-energy, the monomer polymerization in different ink vehicles is become to polymkeric substance, so the look film of UV ink has good machinery and chemical property.The major advantage of UV ink has: (1) is without solvent; (2) rate of drying is fast, and power consumption is few; (3) good luster, bright in luster; (4) water-fast, resistance to solvent, wear resisting property is good.In UV ink, light trigger is a kind of light activated compound that is subject to, and after absorb light is shone, is excited into free radical, and energy is transferred to photosensitivity molecule or photocrosslinking agent, makes UV China ink that photocuring reaction occur.UV China ink has become a kind of more ripe ink technology at present, and its pollutant emission is almost nil.UV curable ink due in system containing solvent, there is efficient, wide adaptability, economy, energy-conservation, environmental friendliness, become tool novel ink with broad prospects for development.
Summary of the invention
The object of this invention is to provide a kind of energy-conserving and environment-protective UV curing inks and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
An energy-conserving and environment-protective UV curing inks, is made by the raw material of following weight part: pigment dyestuff 1-3, aminoresin 20-23, bicarbonate of ammonia 1-2, zeolite 1-2, ethylene glycol ether acetate 13-15, isoamyl butyrate 11-13, Viscoat 295 12-14, cobalt naphthenate 1-1.1, dibutyl tin laurate 1-2, tri (propylene glycol) diacrylate 10-12, ethyl acetate 5-8, UV epoxy acrylate 10-12,1173 light trigger 4-8, trifluoroacetylacetone europium 4-5, vulcabond 5-6, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, double pentaerythritol methacrylate 10-12, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, linking agent TAC2-3, polyisobutene 2-3, silane coupling agent KH560 1-2, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Energy-conserving and environment-protective UV curing inks of the present invention, by following concrete steps, made: first add pigment dyestuff, aminoresin, bicarbonate of ammonia, zeolite, ethylene glycol ether acetate, isoamyl butyrate, Viscoat 295, cobalt naphthenate, dibutyl tin laurate stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1173 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1173 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The invention has the beneficial effects as follows: ink of the present invention can once be imprinted on it on gold and silver paperboard or PVC card by screen painting mode, has improved production efficiency, has saved the energy, and not containing solvent, alleviated the infringement of human body and environmental pollution.
Specific embodiments
Below by specific examples, the present invention is described in detail.
An energy-conserving and environment-protective UV curing inks, by following weight part (kilogram) raw material make: pigment dyestuff 1, aminoresin 20, bicarbonate of ammonia 1, zeolite 1, ethylene glycol ether acetate 13, isoamyl butyrate 11, Viscoat 295 12, cobalt naphthenate 1, dibutyl tin laurate 1, tri (propylene glycol) diacrylate 10, ethyl acetate 5, UV epoxy acrylate 10,1173 light triggers 4, trifluoroacetylacetone europium 4, vulcabond 5, auxiliary agent 4;
Described auxiliary agent by following weight part (kilogram) raw material be prepared from: nano diatomite powder 0.2, nano mica powder 0.2, double pentaerythritol methacrylate 10, neopentyl glycol 5, p-tert-butyl benzoic acid 1, linking agent TAC2, polyisobutene 2, silane coupling agent KH560 1, Tenox PG 2, coix seed oil 1; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
Energy-conserving and environment-protective UV curing inks of the present invention, by following concrete steps, made: first add pigment dyestuff, aminoresin, bicarbonate of ammonia, zeolite, ethylene glycol ether acetate, isoamyl butyrate, Viscoat 295, cobalt naphthenate, dibutyl tin laurate stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1173 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1173 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
The ink of gained, is used cross-hatching ox-hide tape stripping, draws compartment apart from 1mm, and 100% adheres to; Spirituous cotton balls is soaked in use, and 300 grams of pressure wipings 50 times, are as good as shape; Be soaked in salad oil (normal temperature) 8 hours, be as good as shape; Use is soaked with the cotton balls of salt solution, and 300 grams of pressure wipings 50 times, are as good as shape.
Claims (2)
1. an energy-conserving and environment-protective UV curing inks, it is characterized in that, by the raw material of following weight part, made: pigment dyestuff 1-3, aminoresin 20-23, bicarbonate of ammonia 1-2, zeolite 1-2, ethylene glycol ether acetate 13-15, isoamyl butyrate 11-13, Viscoat 295 12-14, cobalt naphthenate 1-1.1, dibutyl tin laurate 1-2, tri (propylene glycol) diacrylate 10-12, ethyl acetate 5-8, UV epoxy acrylate 10-12,1173 light trigger 4-8, trifluoroacetylacetone europium 4-5, vulcabond 5-6, auxiliary agent 4-5;
Described auxiliary agent is prepared from by the raw material of following weight part: nano diatomite powder 0.2-0.3, nano mica powder 0.2-0.3, double pentaerythritol methacrylate 10-12, neopentyl glycol 5-7, p-tert-butyl benzoic acid 1-2, linking agent TAC2-3, polyisobutene 2-3, silane coupling agent KH560 1-2, Tenox PG 2-3, coix seed oil 1-2; Its preparation method is by each mixing of materials, is heated to 60-70 ℃, and stirring reaction 30-40 minute, obtains.
2. energy-conserving and environment-protective UV curing inks according to claim 1, it is characterized in that, by following concrete steps, made: first add pigment dyestuff, aminoresin, bicarbonate of ammonia, zeolite, ethylene glycol ether acetate, isoamyl butyrate, Viscoat 295, cobalt naphthenate, dibutyl tin laurate stirring and evenly mixing, be heated to 80-90 ℃, stir 25-35 minute; Then add all the other remaining components except 1173 light triggers, stirring reaction 3-5 hour; Finally be cooled to 60-70 ℃, add 1173 light triggers, stirring reaction 40-50 minute, cooling after, grind and to obtain 20-40 μ m slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310602412.8A CN103666068B (en) | 2013-11-25 | 2013-11-25 | A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310602412.8A CN103666068B (en) | 2013-11-25 | 2013-11-25 | A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666068A true CN103666068A (en) | 2014-03-26 |
| CN103666068B CN103666068B (en) | 2016-03-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310602412.8A Active CN103666068B (en) | 2013-11-25 | 2013-11-25 | A kind of energy-conserving and environment-protective UV curing inks and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103666068B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104804522A (en) * | 2015-04-13 | 2015-07-29 | 郭小曼 | Environment-friendly ultraviolet-curing pad-printing ink |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
-
2013
- 2013-11-25 CN CN201310602412.8A patent/CN103666068B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1970656A (en) * | 2006-11-23 | 2007-05-30 | 北京印刷学院 | Thermoforming plastic printing ink adopting ultraviolet-infra red drying technology |
| CN103342921A (en) * | 2013-07-29 | 2013-10-09 | 中国科学院化学研究所 | Ink with high hiding rate for ink-jet printing and application thereof to preparation of flexible plate |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104804522A (en) * | 2015-04-13 | 2015-07-29 | 郭小曼 | Environment-friendly ultraviolet-curing pad-printing ink |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103666068B (en) | 2016-03-23 |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: An energy-saving and environmentally friendly UV curing ink and its preparation method Effective date of registration: 20231113 Granted publication date: 20160323 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231219 Granted publication date: 20160323 Pledgee: Shanghai Yudi Aviation Supplies Co.,Ltd. Pledgor: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980065339 |
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| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240103 Address after: Room 101, No. 165 Qiaoli Nanmen Road, Changping Town, Dongguan City, Guangdong Province, 523575 Patentee after: DONGGUAN HAOCAI INK TECHNOLOGY CO.,LTD. Address before: 244000 No. 3201, Cuihu Fourth Road, Tongling Economic Development Zone, Anhui Province Patentee before: TONGLING FOUNDER PLASTICS TECHNOLOGY Co.,Ltd. |